J. Manuf. Mater. Process., Volume 6, Issue 4 (August 2022) – 24 articles

Additive manufacturing is a novel and breakthrough technology by which parts can be manufactured for various purposes and services. As in any production process, the desired properties of additively manufactured components, particularly in electron beam melting processes, ultimately depend on the manufacturing process parameters. Process parameters should be designed accordingly to manufacture parts with specific and desired characteristics. This study focuses on examining the effect of process parameters, such as beam current and velocity, focus offset, and line offset, at three different values each, on the properties of Ti-6Al-4V alloy. The study on the effect of the process parameters on the as-built material’s performance was performed using the Taguchi approach using an L₉ (3⁴) orthogonal array. The properties of printed parts (density, surface roughness, elastic moduli, hardness, tensile characteristics, fractography, and microstructure) were tested. A wide range of properties was obtained and analyzed; namely, porosity varied from 8% to almost fully dense materials with density higher than 99.9% and a range of yield and ultimate tensile strength values and brittle samples with less than 1% elongation to ductile samples with an elongation greater than 16%. The overall performance of printed parts was determined based on an evaluation criterion. Several parameter combinations were found and yielded the fabrication of parts with high density and relatively fine microstructure. The comparison of the best parameter combinations determined in this study and the parameters recommended by the machine manufacturer showed that improved results were obtained, and even when using the optimal parameters, they can be improved even more. This result highlights the ability of the proposed DOE method to further develop existing results and even for development of manufacturing parameters for new materials. Full article

The development of the simulation of refill friction stir spot welding (RFSSW) is critical to be able to predict the behavior of aluminum in the process under specific parameters. A two-dimensional axisymmetric thermo-mechanical model of the RFSSW process for 7075-T6 aluminum alloy sheet was developed and validated with experimental data. Welding temperatures and material flow, including defect formation, were accurately predicted by the model. While these results are encouraging, further development of bonding criteria is needed for simulation models, in order to enable the prediction of properties such as joint strength. The simulation was validated by a comparison of temperatures measured in the weld, which were demonstrated to be accurate at all positions in and around the weld nugget, within 10% of measured values. Additional validation of material flow was performed with post-weld optical microscopy where the simulation is shown to be able to predict the presence or absence of internal volumetric defects based on the variation in process parameters. Finally, the prediction of the tool process forces during the welding cycle were evaluated; however, both probe and shoulder forces were overestimated using the standard flow stress data for AA 7075-T6. Full article

The key priority of metallurgical industry development is expanding the range and improving the quality of bar products and their major component, steel wire. Continuous wire rod mills with multi-roll passes have been developed and implemented over the past decades. These include mills with four-roll passes with mutually perpendicular rolls. The specific feature of mills with complex passes is the impossibility of conduct and the direct measurement of the workpiece dimensions in several directions during rolling. The paper studies the development of a system for indirect control over complex section geometry by adjusting the interstand space tension with simultaneous compensation for changes in rolling forces. The paper contribution is the first justification of a technique for the control over the indirect rolled product section on mills with multi-roll passes based on theoretical and experimental research. Analytical and experimental dependencies between the metal pressure on the rolls and the semifinished rolled product temperature, rolling speed, and single drawing have been obtained for various steel grades. The impact of process factors on the rolled product section geometry when rolling in stands with four-roll passes has first been studied. The automated control system implementing the proposed technique has passed pilot tests on a continuous five-stand mill. The processes occurring in closed-loop speed and torque control systems under controlling and disturbing effects have been experimentally studied. Implementing the proposed algorithms indirectly confirmed the reduced impact of tension and pressure on the section geometry. Full article

The scope of this work is to provide an overview of the influences of process parameters, print orientation, and post-process treatments of Ti6AlV4 processed by laser powder bed fusion on its microstructure and physical and mechanical properties and their anisotropic behavior. To avoid the influence of changes in powder quality and ensure comparability, experiments were carried out using a single batch of virgin powder. First, characterization of the density and surface roughness was performed to optimize the process parameters utilizing design of experiment. Tensile, notched bar impact and compression test specimens were built in three different orientations: vertically, horizontally, and inclined at 45° to the build plate. Later, the influence of the staircase effect and the possible course of anisotropy from vertical to horizontal were investigated. Subsequently, heat treatments for stress relief, furnace annealing, and hot isostatic pressing were performed. In addition to as-built samples, mechanical machining and a two-step electrochemical polishing surface treatment were applied to investigate the influence of the surface roughness. With parameter optimization, a relative density of 99.8% was achieved, and surface roughness was improved over default parameters, reducing Ra by up to 7 µm. Electrochemical polishing is a viable way to decrease the surface roughness. An Ra value of 1 µm and an Rz value of 4 µm can be achieved for 45° downskin surfaces with as-built surface roughness values of Ra 24 µm and Rz 117 µm. As-built and stress-relieved conditions show little anisotropy in their yield and tensile strength (max 2.7%), but there is a strong influence of the build orientation on necking, and brittle fracture behavior is shown due to the martensitic microstructure (up to 70%). Heat treatment can increase the ductility and further decrease the strength anisotropy with both furnace annealing and hot isostatic pressing delivering similar results for tensile properties, while angled samples exhibit behavior that is closer to vertical than horizontal, indicating a non-linear change in break behavior. Electrochemical polishing increases fracture necking, and its isotropy drastically increases from 4% to over 30% compared with as-built parts, which is close to the level of the machined specimen. Full article

Powder-bed binder jet 3D printing is a flexible method for producing magnesium oxychloride (MOC)-based articles. Despite the great potential of this additive manufacturing technology for producing free-form MOC cement-based components, the influence of processing factors on final material performance has not yet been investigated and no general models exist for the selection of proper parameters with the desired quality. In the present work, the effect of six key manufacturing factors on the modulus of rupture of MOC cement-based components was studied, using an analysis of variance. The parametric analysis revealed that the material’s strength was strongly influenced by three process inputs: particle size, the amount of binder, and layer thickness. The amount of binder was determined by the “rate of voxel” and the “powder-bed density” and required precise control during the printing process. The introduced quadratic regression model can assist operators in selecting a combination of binder jet process inputs to achieve predetermined final material performance. Full article

The microstructure, static, and fatigue mechanical properties of laser powder bed fused (LPBF) Ti-6Al-4V components subjected to three different post-processing treatments (PTs) are compared. The first treatment includes stress relief (SR) and beta-phase annealing (BA) heat treatments, the second one includes SR, beta-solution (BST) and over aging (OA) heat treatments, and the third procedure is a combination of hot isostatic pressing (HIP) and BST + OA. It was demonstrated that the three PTs led to the decomposition of α’ martensite inherited from the LPBF process and the formation of variable α + β structures. The SR + BA treatment forms a basket weave structure having an average α lamellae width of ~3 µm and surrounded by ~1 µm-sized zones of segregated β phase (4.6–5.2% β phase content) and globalized α phase (~10 µm in size) inside prior columnar β grains (~100 µm in width). The SR + BST + OA treatment forms semi-equiaxed α grains (~300 µm) containing colonies (~50 µm) of parallel-oriented α plates (~6 µm), and β phase (5.8–7.5%) in the interplate spacing. The HIP + BST + OA treatment leads to the formation of large grains (~500 µm) with both basket weave and colony (~40 µm) α structures containing α plates (1.1–4.2 µm) and β phase (5–7.1%). To compare the impact of these PTs on the mechanical properties of LPBF components, they were subjected to static and fatigue tensile testing at room temperature. The best combination of mechanical properties (yield strength ~920 MPa, ultimate strength ~1000 MPa, elongation to break ~22.5%, and fatigue strength ~600 MPa, 10⁷ cycles) was obtained in the case of SR + BA specimens. These results demonstrate that an adequate thermal treatment, such as SR + BA, of the LPBF Ti64 components, could be a valuable and less expensive alternative to the established HIP + BST + OA treatment procedure when fatigue life is the main concern. Full article

This article presents a cost-effective and reliable method for welding 30 mm thick sheets of shipbuilding steel EH36. The method proposes to perform butt welding in a two-run technique using hybrid laser arc welding (HLAW) and submerged arc welding (SAW). The HLAW is performed as a partial penetration weld with a penetration depth of approximately 25 mm. The SAW is carried out as a second run on the opposite side. With a SAW penetration depth of 8 mm, the weld cross-section is closed with the reliable intersection of both passes. The advantages of the proposed welding method are: no need for forming of the HLAW root; the SAW pass can effectively eliminate pores in the HLAW root; the high stability of the welding process regarding the preparation quality of the weld edges. Plasma cut edges can be welded without lack of fusion defects. The weld quality achieved is confirmed by destructive tests. Full article

Selective laser melting is an additive manufacturing technology used to fabricate metal parts characterized by complex geometries that are difficult or impossible to produce with conventional production methods. One of the major drawbacks of laser melting is the poor surface quality that typically is not satisfactory for functional applications. The aim of this work is to use areal analysis to characterize selective laser melting surfaces. The results highlight a marked variability and anisotropy that cannot be evaluated through traditional measurement. The building orientation and secondary finishing operations are analyzed and discussed. Findings demonstrate how areal analysis can be used to determine how to implement barrel finishing with the aim of reducing anisotropy and increasing surface quality. Full article

A known problem of additive manufactured parts is their poor surface quality, which influences product performance. There are different surface treatments to improve surface quality: blasting is commonly employed to improve mechanical properties and reduce surface roughness, and electropolishing to clean shot peened surfaces and improve the surface roughness. However, the final surface roughness is conditioned by multiple parameters related to these techniques. This paper presents a prediction model of surface roughness (Ra) using an Artificial Neural Network considering two parameters of the SLM manufacturing process and seven blasting and electropolishing processes. This model is proven to be in agreement with 429 experimental results. Moreover, this model is then used to find the optimal conditions to be applied during the blasting and the electropolishing in order to improve the surface roughness by roughly 60%. Full article

This paper analyzes the surface grinding of unfilled and glass-filled polyamides. The process is performed by varying the workpiece velocities to evaluate applied practical applications in the industry while being energy efficient. During the machining, the temperatures, normal forces, tangential forces, and spindle power were collected, and the surface quality was evaluated by a scanning electron microscope (SEM), helping to determine material removal mechanisms and study their behavior under grinding. One of the primary outcomes of the present research was that, different from most metallic and ceramic materials, polyamides benefited from the material removal rate increase. We had higher quality material removed efficiently. Also, the specific energy of both materials converged to previously demonstrated values, showing once again that it is highly dependent on the matrix. Moreover, the time-dependent mechanical properties of the material during processing were identified. The fast application of the force at high speed gave less time to respond to the mechanical strain, determining an improvement in the surface quality of the samples. Consequently, the surface quality of the final product improved with a speed increase, leading to low roughness values. Full article

Friction stir welding (FSW) is an advantageous solid-state joining process that is suitable for many materials in multiple industries. In an industrial setting, manufacturers are actively seeking faster welding speeds to increase throughput. Increasing welding speed limits the size of defect-free parameter windows, which may increase the frequency of defects. The push for faster welding speeds emphasizes the need for economical non-destructive evaluation (NDE) for FSW, like any other type of welding. This work introduces a generalized defect detection method that recognizes the stochastic nature of the FSW process, and that can be generally applied to FSW of a material across a dynamic range of process parameters and welding conditions. When applied to aluminum friction stir-welded blanks at speeds ranging from 1500 to 3000 mm/min with varying ranges of tool tilts, the methodology proved 100% effective at positive detection when defects were present with zero scrap rate. Furthermore, additional development demonstrated the proposed stochastic approach can be used to detect the spatial location of a defect within a weld with 94% detection accuracy and a 4.2% scrap rate. Full article

This study investigates the application of centrifugal force for the compaction of metal powder. Previous studies using the centrifugal force for manufacturing the green bodies were focused on fine powders with narrow particle size distribution or binary mixtures. This study explores the particle packing of multi-sized powder. Aluminum alloy powder with a particle size less than 100 µm and polymer binder were admixed and compacted in the centrifugal casting with ranging magnitudes of centripetal acceleration. Three different centrifugal forces were tested: 700, 1800, and 3700 G. The microstructure of the green bodies was then observed on the SEM micrographs. The obtained green bodies had high packing densities ranging from 62 to 69%. The packing density and median particle size increase at the positions further away from the center of rotation of the centrifuge with an increase of centrifugal force. The effect of centrifugal force on the segregation of particles was investigated through the quasi-binary segregation index. The segregation phenomena was not observed at 700 G, but clear particle segregation was found at higher centrifugal forces. The increase of the centrifugal force resulted in higher segregation with finer particles moving to the inner part of the spinning mold, with a significant change in the size of particles located closer to the center of rotation. Overall, the centrifugal process was found to produce highly compacted green bodies while yielding a segregation effect due to wide particle size distribution. Full article

To verify the mathematical model of the water-jet cooling of steel plates developed by the authors, previously performed experimental studies of the temperature of the test plates in a roller-quenching machine (RQM) were used. The calculated temperature change in the metal as it moved in the RQM was compared with the readings of thermocouples installed at the center of the test plate and near its surface. The basis of the model is the dependence of the temperatures of the film, transition and nucleate boiling regimes on the thickness of the oxide scale layer on the cooled surface. It was found that the model correctly accounts for the oxide scale on the sheet surface, the flow rates and combinations of the RQM banks used, the water temperature, and other factors. For all tests, the calculated metal temperature corresponded well with the measured one. In the experiments with interrupted cooling, the calculated temperature plots repeated the characteristic changes in the experimental curves. The main uncertainty in the modeling of cooling over a wide temperature range can be attributed to the random nature of changes in the oxide scale thickness during water cooling. In this regard, the estimated thickness of the oxide scale layer should be considered the main parameter for adapting the sheet temperature-control process. The data obtained confirm the possibility of effective application of the model in the ACS of industrial TMCP (Thermo-Mechanical Controlled Process) systems. Full article

In this work, the expansion of friction stir welding (FSW) in parts made via material extrusion (MEX) 3D printing was investigated. Poly(methyl methacrylate) (PMMA) plates were joined in a full factorial experimental design. The effects of three FSW parameters (weld tool pin geometry, rotating speed, and travel speed) on the weld results were studied. The tensile strength was investigated using statistical modeling tools. A morphological characterization study was also conducted on the weld zone, with microscopy. The state of the material during the FSW process was monitored via real-time temperature measurements. The feasibility of the process was verified. The results show high industrial merit for the process. The highest tensile strength was reported for the sample welded with the frustum tool, at 1400 rpm and a 9 mm/min travel speed (the highest studied), with a welding efficiency > 1. This can be attributed to the reduced porosity of the weld area compared to the 3D printed structure, and indicates a high potential for joining 3D-printed PMMA sheets via the FSW process. Full article

Flange wrinkling is often seen in deep-drawing process when the applied blankholding force is too small. This paper investigates the plastic wrinkling of flange under a constant blankholding force. A series of deep-drawing experiments of AA1100-O blanks are conducted with different blankholding forces. The critical cup height and wrinkling wave numbers for each case is established. A reduced-order model of flange wrinkling is developed using the energy method, which is implemented to predict the flange wrinkling of AA1100-O sheet by incrementally updating the flange geometry and material hardening parameters during the drawing process. A deep-drawing finite element model is developed in ABAQUS/standard to simulate the flange wrinkling of AA1100-O blanks under constant blankholding force. The predicted cup height and wave numbers from the finite element model and reduced-order model are compared with the experimental results, which demonstrates the accuracy of the reduced-order model, and its potential application in fast prediction of wrinkling in deep-drawing process. Full article

Pallet racking is a fundamental component within the manufacturing, storage, and distribution centers of companies around the World. It requires continuous inspection and maintenance to guarantee the protection of stock and the safety of personnel. At present, racking inspection is manually carried out by certified inspectors, leading to operational down-time, inspection costs and missed damage due to human error. As companies transition toward smart manufacturing, we present an autonomous racking inspection mechanism using a MobileNetV2-SSD architecture. We propose a solution that is affixed to the adjustable cage of a forklift truck, enabling adequate coverage of racking in the immediate vicinity. Our proposed approach leads to a classifier that is optimized for deployment onto edge devices, providing real-time alerts of damage to forklift drivers, with a mean average precision of 92.7%. Full article

This paper presents a new mechanical joining process to assemble aluminum busbars in energy distribution systems. The process is based on the extension of injection lap riveting to the connection of busbars made from the same material as the rivets and requires redesigning the joints to ensure complete filling with good mechanical interlocking and appropriate contact pressures on the overlapping area. The experimental work was carried out in unit cells and involved the fabrication of the riveted joints and the evaluation of their electrical resistance at different service temperatures. Comparisons with the bolted joints that were fabricated and tested for reference purposes show that injection riveted joints provide lower values of electrical resistance and require much less space for assembly due to the absence of material protrusions above and below their surfaces. Numerical simulation with finite elements allows the relating of the reduction in electrical resistance with the changes in the electric current flow when the bolts are replaced by the new type of rivets. The experimental and numerical predictions revealed that the new type of rivets experience an increase in electrical resistance of up to 6 μΩ (30%) when the service temperature approaches 105 °C. Still, the resistance at this temperature (26.2 μΩ) is more than 3 times smaller than that of the bolted joints (80.5 μΩ). Full article

Additive Manufacturing (AM) appears to be the best candidate to manufacture random architected materials, as it offers significant freedom in the design of hollowed parts with complex geometry. However, when these structures are needed with thins walls and struts, AM processes may encounter difficulties in properly manufacturing these structures due to their capability limits. This study proposes to characterize the manufacturing of random architected structures to see firstly their fabricability and the capability of the additive manufacturing processes used, such as vat photopolymerization (Stereolithography process (SLA)), material extrusion (Fused Filament Fabrication process (FFF)) and powder bed fusion (Selective Laser Sintering process (SLS)) through tomographic, dimensional, and mass analysis. Several defects specific to each process were identified. A higher predominance of porosities, lack of printing and excess of material manifests as trapped or partially fused powder for SLS and angel hair for FFF. These defects strongly affect the dimensional and geometric accuracy of the struts and, thus, the final mass of the structure obtained with these two processes. The SLA process makes it possible to print thinner details of random architected structures with better material quality and good dimensional and geometric accuracy, under the conditions and protocol used in this study. Full article

Laser additively manufactured duplex stainless steels contain mostly ferrite in the as-built parts due to rapid solidification of the printed layers. To achieve duplex microstructures (ferrite and austenite in roughly equal proportions) and, thus, a good combination of mechanical properties and corrosion resistance, an austenitic stainless steel powder (X2CrNiMo17-12-2) and a super duplex stainless steel powder (X2CrNiMoN25-7-4) were mixed in different proportions and the powder mixtures were processed via PBF-LB/M (Laser Powder Bed Fusion) under various processing conditions by varying the laser power and the laser scanning speed. The optimal process parameters for dense as-built parts were determined by means of light optical microscopy and density measurements. The austenitic and ferritic phase formation of the mixed alloys was significantly influenced by the chemical composition adjusted by powder mixing and the laser energy input during PBF-LB/M. The austenite content increases, on the one hand, with an increasing proportion of X2CrNiMo17-12-2 in the powder mixtures and on the other hand with increasing laser energy input. The latter phenomenon could be attributed to a slower solidification and a higher melt pool homogeneity with increasing energy input influencing the phase formation during solidification and cooling. The desired duplex microstructures could be achieved by mixing the X2CrNiMo17-12-2 powder and the X2CrNiMoN25-7-4 powder at a specific mixing ratio and building with the optimal PBF-LB/M parameters. Full article

Non-destructive testing (NDT) is a quality control measure designed to ensure the safety of products according to established variability thresholds. With the development of advanced technologies and a lack of formalised knowledge of the state-of-the-art, the National Composites Centre, Bristol, has identified that the increasing complexity of composite products will lead to some severe inspection challenges. To address the apparent knowledge gap and understand system complexity, a formulaic approach to introduce intelligence and improve the robustness of NDT operations is presented. The systemic development of a high-fidelity knowledge base (KB) involves the establishment of a capability matrix that maps material, component, and defect configuration to the capabilities and limitations of selected detection methods. Population and validation are demonstrated through the experimental testing of reference standards and evaluated against an assessment criteria. System complexity in ultrasonic testing operations focusses on capturing the inherent risks in inspection and the designation of evidence-based path plans for automation platforms. Anticipated deployment of the validated applicability data within the KB will allow for road-mapping of the inspection technique development and will provide opportunities for knowledge-based decision making. Moreover, the KB highlights the need for Design for Inspection, providing measurable data that the methodology should not be ignored. Full article

Thin-walled features can be difficult to produce with traditional machining methods which often rely on excess stock material for stiffness. This challenge is increased in hybrid manufacturing where the feature is already near net shape before machining. Significant workpiece deflection can result in poor geometric and surface finish tolerances on the finished part. A potential solution to this problem is to implement sacrificial support structures to the as-printed geometry. The supports are then machined away during the finishing portion of the hybrid process. In the present work, several different design parameters for these sacrificial supports were evaluated to determine their impact on the quality of representative thin wall geometry samples. The angle, height, and spacing of triangular support structures were varied for each sample and then machined and examined. The addition of these supports relative to an unsupported configuration provided a deflection reduction of around 0.2 mm. Surface roughness was improved by approximately 1.5 µm. Increasing values of support height were found to correspond to reduced wall deflection. Similarly, decreasing values of support angle and support spacing improved geometric accuracy. Efficiency comparisons showed that increases in print time corresponded to rapidly diminishing gains in geometric accuracy but continued to improve surface roughness. Implications for hybrid finishing of additively manufactured thin-walled structures is briefly discussed. Full article

Waste-derived materials obtained from the recovery and recycling of electronic waste (e-waste) such as batteries and printed circuit boards have attracted enormous attention from academia and industry in recent years, especially due to their eco-friendly nature and the massive increment in e-waste due to technological development. Several investigations in the literature have covered the advances achieved so far. Meanwhile, photocatalytic applications are especially of interest since they maintain mutual benefits and can be used for H₂ production from solar water splitting based on semiconductor processing as a proper environmentally friendly technique for solar energy conversion. In addition, they can be utilized to degrade a variety of organic and non-organic contaminations. Nonetheless, to the best of the authors’ knowledge, there has not been any comprehensive review that has specifically been focused on e-waste-derived photocatalytic materials. In this regard, the present work is dedicated to thoroughly discussing the related mechanisms, strategies, and methods, as well as the various possible photocatalysts synthesized from e-wastes with some critiques in this field. This brief overview can introduce modern technologies and promising possibilities for e-waste valorization, photocatalytic processes, and new photocatalytic degradation methods of eco-friendly nature. This paper discusses various e-waste-obtained photocatalytic materials, synthesis procedures, and applications, as well as several types of e-waste, derived materials such as TiO₂, ZnO, indium tin oxide, and a variety of sulfide- and ferrite-based photocatalytic materials. Full article

In this work, a finite-element model was elaborated to simulate the thermomechanical behavior of 6061 aluminum alloy during friction-stir welding (FSW). It was shown that FSW-induced deformation is a two-stage process. In addition to the stirring action exerted by the rotating tool probe, the material in the near-surface area of the stir zone also experienced a secondary deformation by the shoulder edge after passage of the welding tool. Both deformation steps were found to be comparable in terms of temperature and strain, but the secondary deformation was primarily concentrated in the near-surface layer. The effects of tool rotation and translation rates on FSW temperature and strain were also systematically examined. Depending on particular welding conditions, the peak welding temperature was predicted to vary from 360 to 500 °C, while the cumulative effective strain was from 12 to 45. Full article

The circular economy promotes plastic recycling, waste minimization, and sustainable materials. Hence, the use of agricultural waste and recycled plastics is an eco-friendly and economic outlook for developing eco-designed products. Moreover, new alternatives to reinforce recycled polyolefins and add value to agroindustrial byproducts are emerging to develop processable materials with reliable performance for industrial applications. In this study, post-consumer recycled high-density polyethylene (rHDPE) and ground rice husk (RH) of 20% w/w were blended in a torque rheometer with or without the following coupling agents: (i) maleic anhydride grafted polymer (MAEO) 5% w/w, (ii) neoalkoxy titanate (NAT) 1.5% w/w, and (iii) ethylene–glycidyl methacrylate copolymer (EGMA) 5% w/w. In terms of processability, the addition of RH decreased the specific energy consumption in the torque experiments with or without additives compared to neat rHDPE. Furthermore, the time to reach thermal stability in the extrusion process was improved with EGMA and MAEO compatibilizers. Tensile and impact test results showed that using coupling agents enhanced the properties of the RH composites. On the other hand, thermal properties analyzed through differential scanning calorimetry and thermogravimetric analysis showed no significant variation for all composites. The morphology of the tensile fracture surfaces was observed via scanning electron microscopy. The results show that these recycled composites are feasible for manufacturing products when an appropriate compatibilizer is used. Full article