Characterization and Antibacterial Properties of Polyetherketoneketone Coated with a Silver Nanoparticle-in-Epoxy Lining
Abstract
:1. Introduction
2. Materials and Methods
2.1. Preparation and Characterization of AgNPs
2.2. Characterization of Specimens Coated with an AgNP-in-Epoxy Lining
2.3. Bacteriostatic Assays In Vitro
3. Results
3.1. Characterization of the Synthesized AgNPs
3.2. Characterization of Specimens Coated with the AgNP-in-Epoxy Lining
3.3. Antibacterial Properties of Specimens Coated with the AgNP-in-Epoxy Lining
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Surface Roughness | ||
---|---|---|
Ra (nm) | RMS (nm) | |
PEKK | 120.262 | 148.744 |
0.25% Ag-PEKK | 2.914 | 4.825 |
0.5% Ag-PEKK | 1.391 | 2.002 |
PEEK | 115.988 | 149.957 |
0.25% Ag-PEEK | 4.939 | 6.950 |
0.5% Ag-PEEK | 2.555 | 4.743 |
Peak Location (cm−1) | Bond Type | Specimen |
---|---|---|
918 | Diphenyl ketone group | PEKK, PEEK |
1033 | C-O-C stretching vibrations in ether groups | Ag-PEKK and Ag-PEEK |
1150 | Asymmetric stretching vibration of C−O−C bonds in diaryl groups | PEKK, PEEK |
1182 | Diphenylether group | PEEK |
1215 | Diphenylether group | PEEK |
1220 | Asymmetric stretching vibrations of C−O−C bonds in diaryl groups | PEKK, PEEK |
1232 | C-O-C stretching vibrations in ether groups | Ag-PEKK and Ag-PEEK |
1485 | Phenyl rings of diphenylether group | PEEK |
1492 | Diphenyl ketone group | PEKK, PEEK |
1507 | Aromatic carbon | Ag-PEKK and Ag-PEEK |
1583 | C = C stretching vibrations in benzene ring bands | PEKK, PEEK |
1594 | Phenyl rings | PEEK |
1647 | Diphenyl ketone group | PEKK, PEEK |
1722 | Carbonyl stretching mode | Ag-PEKK and Ag-PEEK |
PEEK | 0.25% Ag-PEEK | 0.5% Ag-PEEK | PEKK | 0.25% Ag-PEKK | 0.5% Ag-PEKK | |
---|---|---|---|---|---|---|
Porphyromonas gingivalis (CFU) | 1411.6 ± 68.2 | 538.6 ± 30.2 | 358.3 ± 38.2 | 641.7 ± 34.0 | 500.3 ± 29.6 | 233.3 ± 30.6 |
Antibacterial rate (%) | - | 61.87 | 74.63 | 54.57 | 64.56 | 83.47 |
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Lee, W.-F.; Wang, L.-Y.; Renn, T.-Y.; Yang, J.-C.; Fang, L.-S.; Lee, Y.-H.; Peng, P.-W. Characterization and Antibacterial Properties of Polyetherketoneketone Coated with a Silver Nanoparticle-in-Epoxy Lining. Polymers 2022, 14, 2906. https://doi.org/10.3390/polym14142906
Lee W-F, Wang L-Y, Renn T-Y, Yang J-C, Fang L-S, Lee Y-H, Peng P-W. Characterization and Antibacterial Properties of Polyetherketoneketone Coated with a Silver Nanoparticle-in-Epoxy Lining. Polymers. 2022; 14(14):2906. https://doi.org/10.3390/polym14142906
Chicago/Turabian StyleLee, Wei-Fang, Lu-Ying Wang, Ting-Yi Renn, Jen-Chang Yang, Lih-Sheng Fang, Yi-Huan Lee, and Pei-Wen Peng. 2022. "Characterization and Antibacterial Properties of Polyetherketoneketone Coated with a Silver Nanoparticle-in-Epoxy Lining" Polymers 14, no. 14: 2906. https://doi.org/10.3390/polym14142906