Do Chemical-Based Bonding Techniques Affect the Bond Strength Stability to Cubic Zirconia?
Abstract
:1. Introduction
2. Materials and Methods
2.1. Study Design
2.2. Specimens Preparation
2.3. Shear-Bond Strength Test
2.4. Statistical Analysis
3. Results
4. Discussion
5. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Adesive Protocols | Material | Type of Material | Manufacturer | Application Procedure |
---|---|---|---|---|
Tribochemical treatment (GROUP 1) | Cojet Sand | Tribochemical silica-coating particles, 30 µm | 3M, Seefeld, Germany | 1. air-abrasion with silica particles for 10 s. 2. wash for 30 s |
Silane Primer | silane | 3M | 3. apply 1 coat 4. air-dry for 10 s | |
Optibond FL, Bonding | ethyl alcohol, dimethacrylate monomers, barium alumino-borosilicate glass, fumed silica, sodium hexafluorosilicate | Kerr Corp., Orange, CA, USA | 5. apply 1 coat 6. gently air-dry 7. light-cure for 20 s. | |
Signum (GROUP 2) | Signum Zirconia Bond | Bond I: acetone, 10-mdp, acetic acid Bond II: Methyl–methacrylate, diphenyl(2,4,6-trimethylbenzoyl) phosphinoxide | Kulzer, Hanau, Germany | 1. apply 1 coat of Bond I 2. air-dry for 10 s 3. apply 1 coat of Bond II 4. air-dry for 10 s 5. light-cure for 20 s |
Z-Prime (GROUP 3) | Z-Prime Plus | Organophosphate monomer (MDP), carboxylic acid monomer (BPDM), HEMA, ethanol | Bisco, Inc., Schaumburg, IL, USA | 1. apply 1 coat 2. air-dry for 10 s |
Universal Adhesive (GROUP 4) | All-Bond Universal | Organophosphate monomer (MDP), BisGMA, HEMA, ethanol, water, initiators | Bisco, Inc., Schaumburg, IL, USA | 1. apply 1 coat 2. air-dry for 10 s 3. light-cure for 20 s |
Study Groups | Not Thermocycled | Thermocycled | ||
---|---|---|---|---|
Bond Strength (MPa) ± SD | Type of Fracture | Bond Strength (MPa) ± SD | Type of Fracture | |
Group 1 | 21.99 Aa ± 4.98 | 16.67% ACE 83.33% ACO | 8.20 Cb ± 1.86 | 18.75% ACE 75% ACO 6.25% AM |
Group 2 | 25.21 Aa ± 5.45 | 100% ACO | 14.53 Bb ± 4.23 | 91.67% ACO 8.33% AM |
Group 3 | 25.73 Aa ± 5.05 | 100% ACO | 9.31 Cb ± 4.31 | 100% ACO |
Group 4 | 23.12 Aa ± 5.14 | 100% ACO | 8.08 Cb ± 1.45 | 83.33% ACO 16.67% AM |
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Comba, A.; Baldi, A.; Tempesta, R.M.; Carossa, M.; Perrone, L.; Saratti, C.M.; Rocca, G.T.; Femiano, R.; Femiano, F.; Scotti, N. Do Chemical-Based Bonding Techniques Affect the Bond Strength Stability to Cubic Zirconia? Materials 2021, 14, 3920. https://doi.org/10.3390/ma14143920
Comba A, Baldi A, Tempesta RM, Carossa M, Perrone L, Saratti CM, Rocca GT, Femiano R, Femiano F, Scotti N. Do Chemical-Based Bonding Techniques Affect the Bond Strength Stability to Cubic Zirconia? Materials. 2021; 14(14):3920. https://doi.org/10.3390/ma14143920
Chicago/Turabian StyleComba, Allegra, Andrea Baldi, Riccardo Michelotto Tempesta, Massimo Carossa, Letizia Perrone, Carlo Massimo Saratti, Giovanni Tommaso Rocca, Rossella Femiano, Felice Femiano, and Nicola Scotti. 2021. "Do Chemical-Based Bonding Techniques Affect the Bond Strength Stability to Cubic Zirconia?" Materials 14, no. 14: 3920. https://doi.org/10.3390/ma14143920