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Molecules
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Organic Electrosynthesis
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Organic Electrosynthesis

A special issue of Molecules (ISSN 1420-3049).

Deadline for manuscript submissions: closed (31 May 2011) | Viewed by 13631

Special Issue Editors

Prof. Dr. Luis Echegoyen

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Guest Editor
Division of Chemistry, National Science Foundation, 4201 Wilson Boulevard, Arlington, VA 22230, USA
Interests: fullerene chemistry; electrochemistry; supramolecular chemistry
Dr. Andrew P. Doherty

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Guest Editor
School of Chemistry and Chemical Engineering, The Queen's University of Belfast, Belfast, County Antrim, Northern Ireland, UK
Interests: electrochemistry in organised media; structural evolution of mesophase liquids; electrocatalysis, electrosynthesis; nano-particle electrochemistry

Keywords

  • electrosynthesis
  • electrolysis
  • preparative scale
  • physical electrochemistry
  • mechanisms
  • reactor engineering
  • green technology

Published Papers (2 papers)

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Research

440 KiB  
Article
Synthetic Organic Electrochemistry in Ionic Liquids: The Viscosity Question
by Steven Bornemann and Scott T. Handy
Molecules 2011, 16(7), 5963-5974; https://doi.org/10.3390/molecules16075963 - 18 Jul 2011
Cited by 15 | Viewed by 7158
Abstract
Ionic liquids are obvious candidates for use in electrochemical applications due to their ionic character. Nevertheless, relatively little has been done to explore their application in electrosynthesis. We have studied the Shono oxidation of arylamines and carbamates using ionic liquids as recyclable solvents [...] Read more.
Ionic liquids are obvious candidates for use in electrochemical applications due to their ionic character. Nevertheless, relatively little has been done to explore their application in electrosynthesis. We have studied the Shono oxidation of arylamines and carbamates using ionic liquids as recyclable solvents and have noted that the viscosity of the medium is a major problem, although with the addition of sufficient co-solvent, good results and excellent recovery and recycling of the ionic liquid can be achieved. Full article
(This article belongs to the Special Issue Organic Electrosynthesis)
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251 KiB  
Communication
An Electrochemical Synthesis of Functionalized Arylpyrimidines from 4-Amino-6-Chloropyrimidines and Aryl Halides
by Stéphane Sengmany, Erwan Le Gall and Eric Léonel
Molecules 2011, 16(7), 5550-5560; https://doi.org/10.3390/molecules16075550 - 29 Jun 2011
Cited by 17 | Viewed by 6031
Abstract
A range of novel 4-amino-6-arylpyrimidines has been prepared under mild conditions by an electrochemical reductive cross-coupling between 4-amino-6-chloro-pyrimidines and functionalized aryl halides. The process, which employs a sacrificial iron anode in conjunction with a nickel(II) catalyst, allows the formation of coupling products in [...] Read more.
A range of novel 4-amino-6-arylpyrimidines has been prepared under mild conditions by an electrochemical reductive cross-coupling between 4-amino-6-chloro-pyrimidines and functionalized aryl halides. The process, which employs a sacrificial iron anode in conjunction with a nickel(II) catalyst, allows the formation of coupling products in moderate to high yields. Full article
(This article belongs to the Special Issue Organic Electrosynthesis)
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