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Article

Soft X-ray Lensless Imaging in Reflection Mode

1
Synchrotron SOLEIL, Saint-Aubin, B.P. 48, 91192 Gif-sur-Yvette, France
2
Centre de Sciences Nucléaires et Sciences de la Matière, CNRS-UMR 8609, Université Paris-Sud, Bât. 104, 91405 Orsay, France
3
Laboratoire de Chimie Physique-Matière et Rayonnement, CNRS-UMR 7614, Sorbonne Université, 75005 Paris, France
4
ELETTRA, Sincrotrone Trieste, Area Science Park, 34149 Basovizza, Trieste, Italy
5
Institut des Nanosciences de Paris, CNRS-UMR 7588, Sorbonne Université, 75005 Paris, France
*
Author to whom correspondence should be addressed.
Present address: Institut des Sciences Moléculaires d’Orsay, CNRS-UMR 8214, Université Paris-Saclay, Bât. 520, 91405 Orsay, France.
Photonics 2021, 8(12), 569; https://doi.org/10.3390/photonics8120569
Submission received: 16 November 2021 / Revised: 6 December 2021 / Accepted: 9 December 2021 / Published: 11 December 2021
(This article belongs to the Special Issue Extreme-Ultraviolet and X-ray Optics)

Abstract

:
We report on the development and implementation of methodologies dedicated to soft X-ray imaging by coherent scattering in reflection mode. Two complementary approaches are tested, based on Fourier transform holography and on ptychography. A new method for designing holographic masks has been developed. Our results represent a feasibility test and highlight the potential and limitations of imaging in reflection mode. Reflectivity is less efficient than transmission at soft X-ray wavelengths, hampering the acquisition of good quality images. Nonetheless, it has the potential to image a wider set of samples, notably those that are not transparent to soft X-rays. Although the images obtained so far are of modest quality, these results are extremely encouraging for continuing the development of coherent soft X-ray imaging in reflection mode.

1. Introduction

Interest in developing instrumentation and methods for soft X-ray imaging via coherent scattering is supported by a well-documented activity of modern X-ray sources, namely synchrotron, free-electron laser (FEL) and high-harmonic generation (HHG) facilities. In general, techniques relying on the elastic X-ray scattering, like resonant reflectivity, diffuse scattering, diffraction and lensless microscopy, which provide a rather unique tool-set for the investigation of timely and important topics relating to the ordering and to the dynamics of spin, charge and orbital moment in complex materials.
Tunable soft X-ray sources make it possible to select photon energies that match core resonances, merging the structural sensitivity of scattering with the element selectivity and sensitivity to electronic properties of a spectroscopic tool [1]. The soft X-ray range covers the relevant resonances of all the elements important for magnetic materials, notably the 2p→3d of 3d transition metals (TM) and the 3d→4f of rare-earths (RE). The polarization tunability introduces a well-defined and selectable symmetry on the X-ray probe that can be used to reveal and study specific symmetries of the sample. Resonant magnetic scattering of polarized X rays (XRMS) is a rather unique tool for studying both ferromagnetic (FM) and antiferromagnetic (AF) order, offering a view of the magnetic structure that is paralleled only by polarized neutron reflectivity. Resonant scattering in reflection mode (measuring the specular, diffuse or diffracted intensity) addresses the electronic properties, the microstructure [2,3], the magnetic structure [4,5,6,7,8,9,10], as well as the charge [11,12,13] and orbital [3,14] order with in-depth resolution [15,16].
Sources characterized by large transverse coherence can be used to produce X-ray images with high spatial resolution via scattering measurements. Over the last decade, several of the approaches to coherent imaging that were developed in the visible range have been extended successfully to the X-ray range, notably Fourier transform holography (FTH) [17,18] and ptychography [19,20,21]. Central to interest in imaging via coherent soft X-ray scattering is the study of magnetic structures (and of their dynamics), a topic of high impact in both fundamental research and applications [22].
Imaging by soft X-ray scattering takes full advantage of all the peculiar characteristics of modern X-ray sources, especially in terms of coherence and brilliance. Also, flux is a critical parameter, since low intensity can be a limiting factor for new developments in imaging techniques; as will become apparent in the following, this is particularly true in reflection mode.
From the very beginning [17] and up to now, soft X-ray FTH experiments have been performed intensely in transmission mode, and several complementary technical solutions have been developed: integrated [17,23] or separate [18,24] sample/mask approach, out-of-plane [24] or in-plane [25,26] magnetization analysis, use of circular (large majority of published works) or linear [27] polarization of the X rays. Many studies took advantage also of the optimized experimental conditions at FEL sources for two-color [28] or single-shot [29,30] magnetic imaging.
The transmission mode, however, suffers from one main limitation, i.e., the sample must be transparent. In the soft X-ray range this means a total thickness (i.e., including sample and substrate) of at most a few hundreds of nm, which hampers or even impedes the study of a large class of samples, notably single crystals and epitaxial thin films. The implementation of X-ray imaging in reflection mode has the potential to overcome constraints on the sample transparency, extending these imaging techniques to a wider class of materials.
Microscopy in reflection mode at extreme ultraviolet wavelengths has been performed by coherent diffraction imaging, relying on iterative phase retrieval algorithms. Examples were reported, for instance, at HHG sources, using 29 nm [31] and 42.6 nm [32] radiation.
Performing soft X-ray holography in reflection mode has been attempted at several synchrotron sources over the last 10 years, with scarce success. The simple idea of replacing the reference aperture (pin-hole) by a reference pin is hindered by the overwhelming contribution of diffuse scattering from the substrate. No significant result has been reported to date using this approach. The only published example of FTH in reflection used a holographic mask, placed after the sample surface and normal to it, that intercepts the scattered beam on its way to the detector [33]. This geometry limits severely the area that can be imaged to a fixed zone next to the sample edge. Moreover, since the mask is far from the X-ray impact spot, one has to rely on phase-retrieval algorithms for attaining an acceptable spatial resolution [34]. This first example of FTH in reflection [33] was a very important result of high impact, but the proposed configuration proved rather impractical and did not find many applications.
The objective of our work is to continue developing and testing new methods for reflection soft X-ray imaging using holography and ptychography. The former requires a very simple data treatment, but it is extremely photon-hungry since it relies on the intensity of a reference beam generated by a tiny aperture, the size of which limits the final spatial resolution [17]. The latter is simpler to implement experimentally, but requires using phase retrieval algorithms for image reconstruction [35,36,37]. Given the technical similarities of the two approaches, it is easy to implement both in a single experimental setup.

2. Materials and Methods

We have developed a setup for X-ray imaging in reflection mode based on the separate mask/sample scheme, making it possible to bring any part of the sample into the field of view. We installed the new set-up in the IRMA-2 scattering chamber [38] and we tested it at the SEXTANTS beamline [39] of the SOLEIL synchrotron. The X-ray transverse coherence was defined by selecting the central part of the undulator emission cone via a four-jaws device, a configuration already characterized [38] and tested in previous experiments [26,27]. Additionally, the incoming beam was skimmed by placing a 20 µm guard-hole ~10 mm before the mask/sample setup in order to limit the irradiated mask area. The two-dimensional detector was a 27.6 × 27.6 mm2 charge-coupled device (CCD) with 2048 × 2048 pixels. A 100 nm-thick aluminum filter protected the detector from the stray visible light generated by the in-vacuum encoders. The CCD could be mounted on fixed flanges at either 30° or 90° from the incoming beam axis in order to collect the specular and the diffuse intensity from the sample set at either ω = 15° or ω = 45° incidence. In both cases, the detector was positioned at 470 mm from the sample, collecting ±1.6° along the two directions in the YZ’ plane normal to the specular beam axis. Since the projection of the scattering vector Q on the sample surface depends on ω in the Z’ direction but not in the Y direction, a square detector covers different ranges of QY and QZ’ in the reciprocal space, the difference increasing for lower ω values.
Test samples were arrays of sub-micron objects of different materials, namely an 80 nm thick Fe20Ni80 (permalloy, or Py) layer, a 50 nm thick FeRh layer, and a (Co11nm/Cu20nm)20 multilayer. The patterns consisted of squares, of rectangles, and of triangular holes. The Py and Co/Cu objects were prepared on Si substrates using X-ray lithography in combination with sputter deposition and lift-off according to the process described in [40]. The FeRh film was sputter-deposited on MgO and patterned using optical lithography and ion etching.
We used two different kinds of masks for holography and ptychography, both prepared by etching X-ray opaque supports (1.2 µm of AuCr0.2 on 100 nm thick Si3N4 membranes) using focused ion beam (FIB) milling. The final set-up for the synchrotron experiment is sketched in Figure 1: a 20 µm pin-hole delimits the size of the beam reaching the mask and impinging on the sample, tilted at the desired angle (45° in the picture for holography).
An ensemble of 11 encoded translation and rotation tables, driven by either stepper or piezoelectric motors, provided all the required degrees of freedom to the guard-hole (TxTyTz), holographic or ptychographic mask (TxTyTzRy) and sample (TxTyTzRy), as sketched in Figure 1. A preliminary alignment of all parts was performed in air prior to the experiment, using the synchrotron visible light for autocollimation.

2.1. Holographic Mask

The preparation of the holographic mask relied on an original process developed at CSNSM [41] and used also for kirigami [42,43], which is illustrated in Figure 2. First, the object and reference apertures are opened in the direction perpendicular to the Au-coated and X-ray opaque Si3N4 membrane by FIB milling (Figure 2a). Then an area of ~50 × 50 µm2 containing the apertures is delimited and three of its sides are sliced by FIB (Figure 2b). Finally, the sliced area containing the holography apertures is lifted to the desired angle, at 45° in our case (Figure 2c). Figure 2d shows that several of such masks, lifted at either +45° or –45°, can be prepared on a single Si3N4 multi-membrane Si substrate. Finally, Figure 2e shows an alternative mask design, comprising a line-reference aperture (30 nm wide in its narrowest part and 8 µm long) for HERALDO data processing [44,45,46], an approach that was used already at the SEXTANTS beamline in transmission mode [47,48,49]. Data reported below make use of this mask.
A precise parallel positioning of the sample and mask surfaces (Figure 1) makes it possible to bring them in close contact, as in the transmission case [18,24,26,27], gaining stability and avoiding (or at least reducing to a minimum) the need for back-propagation corrections [34].
For the top two masks shown in Figure 2d, X-rays go through the lifted mask first, impinge at 45° on the sample positioned behind the mask, and are scattered towards the CCD detector placed at 90°. For the lower masks of Figure 2d, X rays enter the 50 µm opening first, impinge on the sample at 45°, and the scattered beam goes through the holographic mask before reaching the detector. Data shown in Figure 3 were collected using this configuration, which also corresponds to the sketch of Figure 1.

2.2. Ptychographic Mask

The preparation of the ptychographic masks followed the standard procedure of FIB milling of the same X-ray opaque membranes. Several apertures, either square (1.7 μm and 2.4 μm) or circular (from 0.6 to 3 μm in diameter) were prepared on the same multi-membrane Si support. Only one aperture was illuminated at a time, selected by positioning it behind the 20 µm guard-hole (Figure 1). By an appropriate shaping of the Si support, each mask could be aligned normal to the incident beam and positioned as close as 1.5 mm along the X direction from the point where the photons impinge on the sample surface. The sample position behind the mask was scanned in sub-μm (100 to 400 nm) steps along both Y and Z’ directions within the sample surface (see Figure 1), using encoded piezoelectric motors. In this way several overlapping sample areas were illuminated and, for each sample position, the 2D map of the scattered intensity was collected by the CCD detector. One complete acquisition typically consisted of 40 to 120 steps. The entire data set was then treated by means of a phase retrieval algorithm that allows the reconstruction of the sample image over the whole probed area [50].

3. Results

3.1. Holography

Figure 3a shows the 2D diffraction pattern of the soft X-ray beam being scattered by the Co/Cu sample (700 × 300 nm2 rectangles on a 880 × 540 nm2 mesh) and going through the holographic mask.
The photon energy is tuned to 776 eV, corresponding to the Co 2p3/2 resonance. In this reciprocal space image, one can clearly identify contributions from the array of rectangles (horizontal/vertical intensity spots), from the 45° tilted square holographic object aperture (intensity along ±45° axes), and from the horizontal line-reference aperture (intensity scattered along the vertical line through the center of the figure). One can also observe fine modulations of the intensity corresponding to interference between these different contributions. Figure 3b shows the Fourier transform of the scattered intensity providing a real space image, with the autocorrelation of the object aperture dominating its central part. The holographic mask design produces cross-correlations between object and reference apertures that are well separated from the autocorrelation. The cross-correlations between the object and point-reference apertures and between the object and line-reference apertures are indicated by arrows in Figure 3b. They are accompanied by conjugate images, symmetric with respect to the center of the figure [17]. Although Figure 3 suggests that we have appropriate conditions for achieving soft X-ray imaging by FTH in reflection mode, the high scattering angle implies that only a very low intensity goes through the holographic mask, especially through the point-reference aperture.
Figure 4 shows the details of the FT reconstructions obtained at 776 eV using either the point-reference (Figure 4b) or the line-reference (Figure 4c,d), and compares the results with an image of the array of Co/Cu rectangles obtained by scanning electron microscopy (SEM, Figure 4a).
In all the holographic images the objects can be identified, as highlighted also by the line profiles shown in Figure 4e,f. Due to the low signal to noise ratio (SNR), however, we can hardly claim to have obtained a clear image of the objects.

3.2. Ptychography

Concerning ptychography, the function of the mask is to define the X-ray source that illuminates a certain sample area. Several diffraction patterns are collected by moving with high precision the sample with respect to the mask, illuminating overlapping areas. Finally, an iterative algorithm for phase retrieval [50] treats the ensemble of the diffraction patterns to reconstruct a real space image of the amplitude and phase contrast corresponding to the probed area. Fairly good results have been obtained already at the SEXTANTS beamline using this approach in transmission mode [49].
A first set of data was recorded with the detector positioned at 90° with respect to the incoming beam, measuring the scattering from a pattern of triangular holes in a permalloy film (Figure 5a), using a photon energy of 707 eV (Fe 2p resonance). The mask had a 2 μm diameter aperture and was set normal to the incident beam, 1.5 mm away from the sample. Figure 5b shows the amplitude image obtained, after 1300 iterations, from the analysis of 40 diffraction patterns. Next, the CCD was placed at 30° with respect to the incoming beam, with a gain in scattered intensity that allowed us to speed up the acquisition and to increase the number of steps in the ptychography measurement. Figure 5c shows the image of the reconstructed amplitude (60 diffraction patterns, 1241 iterations) for the array of triangles. In spite of the gain in intensity, we obtained an image of worse quality at more grazing incidence, the reasons for that becoming apparent in the analysis of the data below.
Figure 6a shows the amplitude image of FeRh 400 nm squares, based on the analysis of 10 frames measured in reflection ptychography at grazing incidence (ω = 15°) and at 707 eV photon energy. The total acquisition time was ~15′, and the reconstruction relied on 5000 iterations. Figure 6b shows the horizontal profile (Y direction) of the intensity. The analysis of the intensity steps corresponding to the edges of the FeRh objects shows that they extend over 110 ± 10 nm, setting an upper limit to the spatial resolution in the Y direction. Along the Z’ direction, corresponding to the intersection between the incidence plane and the sample surface, the effective pixel size is enlarged by a factor ~3.2 due to the reduced QZ’ range covered by the detector for ω = 15° grazing incidence of the X rays. As a result, it is not possible to discern any intensity plateau associated with the 400 nm objects in Figure 6c. Therefore, the intensity gained by setting the detector at 30° is counterbalanced by a loss of spatial resolution in the vertical direction with an overall degradation of the image quality, as shown also in Figure 5.

4. Discussion

We consider that the reflection holography and ptychography experiments reported here prove the technical feasibility of this method, and that the results achieved are positive and encouraging. Although the quality of the images obtained so far is, admittedly, rather poor, they represent nonetheless a first achievement in the process of developing a new experimental approach.
Beyond providing a reasonable proof of feasibility, this experiment also allowed us to introduce a new and original approach to the mask fabrication process. Concerning holography, the new mask design represents a major step forward with respect to attempts made in the past. By moving the sample laterally, different sample areas can be brought into the field of view, and this approach makes it possible to extend the capabilities of the separate mask/sample FTH technique, already developed in transmission [18,24,27], to the reflection mode. Although the images we obtained so far are of rather modest quality, these results are extremely encouraging for continuing the development of reflection X-ray holography.
Ptychography poses less severe constraints than holography in terms of signal-to-noise ratio. These first attempts in reflection mode have yielded already better results, although not yet completely satisfactory in terms of image contrast and spatial resolution. In the case of the FeRh sample, the ion etching process may affect the X-ray reflectivity near the edges of the etched regions, with a negative influence on the image reconstruction of Figure 6. We cannot really quantify this effect for our measurements and, anyway, a similar observation would not apply to the permalloy sample of Figure 5.
Overall, the results achieved allow us to identify in the signal intensity the main limiting factor that has to be addressed in future reflection soft X-ray imaging experiments. This is particularly true for holography: even at an optimized synchrotron source, the intensity of the reference soft X-ray wave scattered at high angle through a ~20–40 nm aperture requires extremely long exposure times, exacerbating noise and stability problems. Working at lower photon energy, e.g., at the 3p resonances of 3d-TM (around 40–70 eV), is an interesting option for overcoming the reflected intensity problem and for achieving a better SNR. We could not explore this option in the present experiment because the fixed sample-detector distance of 470 mm implies covering a much-reduced Q-space at lower photon energy, producing very large pixels (~300 nm) in the FTH images. A different setup, with the CCD set closer to the sample (50–100 mm), will be required for exploring the possibility of working in reflectivity at the 3p resonances. Another approach, already tested in transmission [18,51], consists in the implementation of multiple reference apertures forming independent images that can be summed up to improve the SNR ratio.
We conclude by pointing out that all the ongoing upgrade projects at synchrotron sources have as a clear and declared objective the optimization of the coherent flux, therefore providing much improved conditions for lensless imaging techniques. Also, the high intensity per pulse offered by the X-ray FEL sources will represent a major asset for a drastic improvement of the SNR and for taking a decisive step forward in the development of soft X-ray imaging in reflection mode.

Author Contributions

Conceptualization, H.P., F.F., C.S., M.S.; methodology, H.P., F.F., R.D., C.S.; software, H.P.; investigation, all authors; data curation, H.P., M.S.; writing—original draft preparation, M.S.; writing—review and editing, all authors. All authors have read and agreed to the published version of the manuscript.

Funding

This research received no external funding.

Data Availability Statement

The data that support the findings of this study are available from the corresponding author upon reasonable request.

Acknowledgments

We acknowledge SOLEIL for provision of synchrotron radiation facilities. We thank K. Medjoubi (Synchrotron SOLEIL) for assistance in installing the phase retrieval computer code. We acknowledge the use of the SEM-FIB facility of the Institut des Sciences Moléculaires d’Orsay for mask preparation.

Conflicts of Interest

The authors declare no conflict of interest.

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Figure 1. Sketch of the experimental set-up (side view) for holography (left) and ptychography (right), showing the three main elements (guard-hole, mask and sample) and their respective in-vacuum motorized translations (T) and rotations (R). The Z’ axis depends on ω, the angle of grazing incidence (ω = 45° for holography, ω = 15° and 45° for ptychography). The Y axis, common to all elements, is perpendicular to the drawing.
Figure 1. Sketch of the experimental set-up (side view) for holography (left) and ptychography (right), showing the three main elements (guard-hole, mask and sample) and their respective in-vacuum motorized translations (T) and rotations (R). The Z’ axis depends on ω, the angle of grazing incidence (ω = 45° for holography, ω = 15° and 45° for ptychography). The Y axis, common to all elements, is perpendicular to the drawing.
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Figure 2. Scanning electron microscopy (SEM) images of the holographic mask fabrication process by focused ion beam milling. (a) Normal incidence etching of the holographic mask in the gold coated Si3N4 membrane, with a square object aperture and five point-reference apertures. (b) Three-side cutting of a 50 × 50 μm2 area containing the holography apertures (view at 45° from the surface). (c) The cut area containing the apertures is lifted at 45° with respect to the membrane surface. (d) View of the four-membrane Si substrate, showing two masks lifted at +45° and two others at −45°. (e) Mask design alternative to (a), comprising a 2.4 μm square object aperture, plus two point-reference and one line-reference apertures.
Figure 2. Scanning electron microscopy (SEM) images of the holographic mask fabrication process by focused ion beam milling. (a) Normal incidence etching of the holographic mask in the gold coated Si3N4 membrane, with a square object aperture and five point-reference apertures. (b) Three-side cutting of a 50 × 50 μm2 area containing the holography apertures (view at 45° from the surface). (c) The cut area containing the apertures is lifted at 45° with respect to the membrane surface. (d) View of the four-membrane Si substrate, showing two masks lifted at +45° and two others at −45°. (e) Mask design alternative to (a), comprising a 2.4 μm square object aperture, plus two point-reference and one line-reference apertures.
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Figure 3. X-ray holography in reflection mode. (a) Hologram collected at 776 eV and 90° scattering angle from an array of sub-µm Co/Cu dots, using the holographic mask shown in Figure 2e, which comprises both line- and point-references. (b) Fourier transform of (a). The object autocorrelation is at the center of the image. The object/point-reference and object/line-reference cross-correlations are indicated by arrows in the lower half of the picture. Conjugate images appear in the upper half.
Figure 3. X-ray holography in reflection mode. (a) Hologram collected at 776 eV and 90° scattering angle from an array of sub-µm Co/Cu dots, using the holographic mask shown in Figure 2e, which comprises both line- and point-references. (b) Fourier transform of (a). The object autocorrelation is at the center of the image. The object/point-reference and object/line-reference cross-correlations are indicated by arrows in the lower half of the picture. Conjugate images appear in the upper half.
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Figure 4. Reflection holography with point- and line-references. (a) SEM image of the Co/Cu patterned sample. The yellow square highlights an area equivalent to the object aperture of the holographic mask. (b) Cross-correlation image with the point-reference, where one can identify the sub-micron structures. (c,d) Images obtained by the HERALDO analysis [44,45] of the object/line-reference cross correlation. Two images are generated, with inverse contrast. (e,f) Comparison of vertical (e) and horizontal (f) line profiles obtained from images (b,c).
Figure 4. Reflection holography with point- and line-references. (a) SEM image of the Co/Cu patterned sample. The yellow square highlights an area equivalent to the object aperture of the holographic mask. (b) Cross-correlation image with the point-reference, where one can identify the sub-micron structures. (c,d) Images obtained by the HERALDO analysis [44,45] of the object/line-reference cross correlation. Two images are generated, with inverse contrast. (e,f) Comparison of vertical (e) and horizontal (f) line profiles obtained from images (b,c).
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Figure 5. (a) SEM image of the permalloy pattern. Amplitude contrast images of the sample reconstructed from diffraction patterns acquired by ptychography at a grazing incidence ω = 45° (b) and ω = 15° (c). Reconstructions based on 40 and 60 diffraction patterns in (b,c), respectively. The photon energy was 707 eV (Fe-2p resonance).
Figure 5. (a) SEM image of the permalloy pattern. Amplitude contrast images of the sample reconstructed from diffraction patterns acquired by ptychography at a grazing incidence ω = 45° (b) and ω = 15° (c). Reconstructions based on 40 and 60 diffraction patterns in (b,c), respectively. The photon energy was 707 eV (Fe-2p resonance).
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Figure 6. (a) Amplitude contrast image of the ~400 nm FeRh squares on a 600 × 800 nm2 mesh, reconstructed from 10 diffraction patterns acquired by ptychography at a grazing incidence ω = 15° and at a photon energy of 707 eV. The size of the reconstructed pixel is 34.4 × 109.1 nm2. Horizontal (b) and vertical (c) line profiles are also shown.
Figure 6. (a) Amplitude contrast image of the ~400 nm FeRh squares on a 600 × 800 nm2 mesh, reconstructed from 10 diffraction patterns acquired by ptychography at a grazing incidence ω = 15° and at a photon energy of 707 eV. The size of the reconstructed pixel is 34.4 × 109.1 nm2. Horizontal (b) and vertical (c) line profiles are also shown.
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Popescu, H.; Fortuna, F.; Delaunay, R.; Jaouen, N.; Spezzani, C.; Sacchi, M. Soft X-ray Lensless Imaging in Reflection Mode. Photonics 2021, 8, 569. https://doi.org/10.3390/photonics8120569

AMA Style

Popescu H, Fortuna F, Delaunay R, Jaouen N, Spezzani C, Sacchi M. Soft X-ray Lensless Imaging in Reflection Mode. Photonics. 2021; 8(12):569. https://doi.org/10.3390/photonics8120569

Chicago/Turabian Style

Popescu, Horia, Franck Fortuna, Renaud Delaunay, Nicolas Jaouen, Carlo Spezzani, and Maurizio Sacchi. 2021. "Soft X-ray Lensless Imaging in Reflection Mode" Photonics 8, no. 12: 569. https://doi.org/10.3390/photonics8120569

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