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Correction to Toxins 2021, 13(12), 883.
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Correction

Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883

by
Luis G. Addante-Moya
1,
Antonio Abad-Somovilla
1,
Antonio Abad-Fuentes
2,
Consuelo Agulló
1 and
Josep V. Mercader
2,*
1
Department of Organic Chemistry, University of Valencia, Doctor Moliner 50, 46100 Burjassot, Valencia, Spain
2
Spanish Council for Scientific Research, Institute of Agrochemistry and Food Technology, Agustí Escardino 7, 46980 Paterna, Valencia, Spain
*
Author to whom correspondence should be addressed.
Toxins 2023, 15(2), 162; https://doi.org/10.3390/toxins15020162
Submission received: 9 February 2023 / Accepted: 9 February 2023 / Published: 16 February 2023
(This article belongs to the Special Issue Application of Novel Methods for Mycotoxins Analysis)
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Versions Notes

Misplace of Schemes

In the original publication [1], Scheme 1 and Scheme 2 are misplaced due to mistakes in the publication process. Scheme 1 should be placed in the position of Scheme 2 and vice versa.
The correct schemes should be as follows:
Toxins 15 00162 sch001 550
Scheme 1. Synthesis of ALa-NHS ester. Reagents and conditions: (a) Br(CH2)4CO2CH3, K2CO3, KI, Bu4NBr, acetone, reflux, 16 h, 75% of 3. (b) Tf2O, pyridine, 0 °C to rt, 20 h, 91%. (c) i. n-BuLi, THF, −78 °C, 40 min; ii. B(OiPr)3, −78 °C to 0 °C, 1.5 h, 93%. (d) Pd(PPh3)4, K2CO3, DMF, 93 °C, 24 h, 75%. (e) i. HCl, MeOH, rt, 22 h; ii. TFA, CH2Cl2, rt, 20 h, 97%. (f) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 93%. (g) EDC·HCl, NHS, DMF, rt, overnight, 99% of crude product.
Scheme 1. Synthesis of ALa-NHS ester. Reagents and conditions: (a) Br(CH2)4CO2CH3, K2CO3, KI, Bu4NBr, acetone, reflux, 16 h, 75% of 3. (b) Tf2O, pyridine, 0 °C to rt, 20 h, 91%. (c) i. n-BuLi, THF, −78 °C, 40 min; ii. B(OiPr)3, −78 °C to 0 °C, 1.5 h, 93%. (d) Pd(PPh3)4, K2CO3, DMF, 93 °C, 24 h, 75%. (e) i. HCl, MeOH, rt, 22 h; ii. TFA, CH2Cl2, rt, 20 h, 97%. (f) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 93%. (g) EDC·HCl, NHS, DMF, rt, overnight, 99% of crude product.
Toxins 15 00162 sch001
Toxins 15 00162 sch002 550
Scheme 2. Synthesis of ALb-NHS ester. Reagents and conditions: (a) Pd(PPh3)4, K2CO3, DMF, 95 °C, 19 h, 77%. (b) NaH2PO4·H2O, NaClO2, tBuOH-H2O (5:1), rt, 5 h, 96%. (c) iPrOH, THF, conc HCl, 55 °C, 24 h, 98%. (d) Br(CH2)4CO2CH3, Cs2CO3, DMF, 94%. (e) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 99%. (f) EDC·HCl, NHS, DMF, rt, overnight. (g) 5% Pd/C, acetone, H2 (1.5 atm), rt, 19 h, 95% of crude product from 14.
Scheme 2. Synthesis of ALb-NHS ester. Reagents and conditions: (a) Pd(PPh3)4, K2CO3, DMF, 95 °C, 19 h, 77%. (b) NaH2PO4·H2O, NaClO2, tBuOH-H2O (5:1), rt, 5 h, 96%. (c) iPrOH, THF, conc HCl, 55 °C, 24 h, 98%. (d) Br(CH2)4CO2CH3, Cs2CO3, DMF, 94%. (e) Lipase acrylic resin, THF-PB 100 mM, rt, 20 h, 99%. (f) EDC·HCl, NHS, DMF, rt, overnight. (g) 5% Pd/C, acetone, H2 (1.5 atm), rt, 19 h, 95% of crude product from 14.
Toxins 15 00162 sch002
The authors state that the scientific conclusions are unaffected. The original publication has also been updated.

Reference

  1. Addante-Moya, L.G.; Abad-Somovilla, A.; Abad-Fuentes, A.; Agulló, C.; Mercader, J.V. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. [Google Scholar] [CrossRef]
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MDPI and ACS Style

Addante-Moya, L.G.; Abad-Somovilla, A.; Abad-Fuentes, A.; Agulló, C.; Mercader, J.V. Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. Toxins 2023, 15, 162. https://doi.org/10.3390/toxins15020162

AMA Style

Addante-Moya LG, Abad-Somovilla A, Abad-Fuentes A, Agulló C, Mercader JV. Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883. Toxins. 2023; 15(2):162. https://doi.org/10.3390/toxins15020162

Chicago/Turabian Style

Addante-Moya, Luis G., Antonio Abad-Somovilla, Antonio Abad-Fuentes, Consuelo Agulló, and Josep V. Mercader. 2023. "Correction: Addante-Moya et al. Assessment of the Optimum Linker Tethering Site of Alternariol Haptens for Antibody Generation and Immunoassay Development. Toxins 2021, 13, 883" Toxins 15, no. 2: 162. https://doi.org/10.3390/toxins15020162

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