3. Results and Discussion
The basic descriptive statistics of all monitored quantities for woods of individual wood species are specified in
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7. Changes in the values of bending strength, impact strength and static and dynamic modulus of elasticity depending on the direction of loading are shown in
Table 8. In this table, the changes are given in percentage expression, where a change was monitored in the values of individual detected quantities in the radial direction against the values in the tangential direction. The following are detailed statements on the individual quantities, as well as graphical visualization or correlation dependencies between quantities.
The wood density of individual wood species was determined after air-conditioning of the test specimens. After the air-conditioning, absolute moisture was ascertained for the individual woods, namely 13.8% for spruce wood, 13.3% for larch, 11.9% for beech, 11.7% for birch, 10.2% for linden, 11.5% for oak and 12.0% for ash. The graph (
Figure 4) shows the determined values of wood density for individual examined wood species. The highest average density was recorded for larch wood, i.e., 760 kg/m
3 for samples that were tested under loading in the tangential direction. The lowest density was recorded for spruce wood, for which the same average density was found for both sets of samples (radial and tangential direction of loading), i.e., 463 kg/m
3. Statistically significant differences in mean values depending on the direction of loading were demonstrated for larch wood, and Duncan’s test (
Table A3) was used for multiple comparisons. Wood density is highly variable and depends on many factors [
5,
14]. This claim is evident in the case of larch density, which appears to be nonstandard compared to the values specified, for example, by Tsoumis [
5] or Wageführ [
33]. Other determined densities of individual wood species coincide with the range of densities reported in the literature [
5,
33,
34], except for oak wood, in which a slightly higher density was found, i.e., 719 or 722 kg/m
3.
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7 show the average widths of annual rings for individual wood species. The width and structure of the annual rings is highly variable and influenced by a large number of factors. The width of the annual ring changes both along the diameter of the trunk and along its length [
3,
5]. The largest width of the annual rings was found for ash wood, i.e., 2.9 mm, and the lowest for larch wood, 1.5 mm, which also showed the highest degree of variability. For birch wood with an average annual ring width of 2.4 mm, a nonstandard factor in the structure of annual rings was found after image analysis. The annual rings were markedly wavy in the cross section (
Figure 5d).
Figure 5 also shows examples of cross sections of wood of other wood species. All of the images are at 40× magnification.
Dinwoodie [
2] states in his work that bending strength is highly influenced by the occurrence of defects and the deviation of wood fibers from the longitudinal axis. However, in this work, great emphasis was placed on the quality of the tested material and the relative “homogeneity” of the test specimens was verified, which guaranteed the highest possible representative values of the investigated properties. This homogeneity was verified by the ultrasound and resonance methods. For clarity, the resonance method (
Figure 6) is specified, which monitored the time of passage of the sound wave in the test specimens on the basis of the tests they were subjected to. The measured time should be almost identical or similar without significant statistical differences. Only under this assumption were the errors eliminated, and the obtained values determining any of the properties had a more representative weight. After evaluating the data, the differences between the test samples, which followed each other within a specific test, were primarily monitored. Thus, in order to determine the static bending strength, the first two test samples in the lath (1 and 2) were compared, and to determine the dynamic strength (impact strength), the following test specimens, i.e., 3 and 4, were compared. It can be seen from the specified graph that this assumption was fulfilled, and the samples did not show any significant differences amongst themselves. A significant difference was observed for birch wood between samples 1 and 2, i.e., for wood samples in which annual ring corrugation was observed (
Figure 5d).
It is clear from the graphical representation (
Figure 7) that the highest values of static bending strength were achieved by birch wood when loading test specimens in the radial direction. The mean value of the bending strength limit in this case was 112.4 MPa. The lowest mean value was achieved by spruce wood under load in the radial direction, i.e., 87.1 MPa. Larch, beech and ash wood showed similar average values of static bending strength in both loading directions, i.e., in the range of 104.6 to 111.6 MPa. The mean value of bending strength for oak wood was 94.3 MPa in the tangential direction and 101.7 MPa in the radial direction of the load. All of the detected values of static bending strength for the selected wood species under load in the radial or tangential direction are given above in
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7. It is clear from the above tables that the highest degree of variability in the values of the bending strength limit was shown by oak wood, and the lowest degree of variability was observed in ash wood, in both directions.
Figure 7 also shows that the largest differences in the mean values of bending strength between the directions were achieved by oak wood, whilst lower differences were observed for linden and birch wood. Spruce, larch, beech and ash wood showed almost no differences in static bending strength values depending on the direction of the test specimen load.
Some authors state [
6,
13] that the ultimate strength of tangential bending can be 10% to 12% higher than that of radial bending in the wood of coniferous trees (softwoods). Požgaj et al. [
6] state in their work that for deciduous wood species (hardwoods), these differences in static bending are negligible in the range of 2% to 4%.
Table 8 shows the differences in the mean values of static bending strength for wood of selected wood species depending on the direction of loading. These differences are expressed as a percentage and are related to how the mean values of static bending strength at radial load have changed from the values found in the tangential direction. The table shows that the largest difference was recorded for oak wood, i.e., 7.9%, while minor differences were found for linden wood, 6.6%, and birch, 4.7%, and for spruce, larch, beech and ash wood, these differences are negligible. Statistically significant differences in mean values between loading directions were demonstrated for oak and linden wood, and Duncan’s test was used for multiple comparisons (see
Appendix A Table A1).
It is evident from the above that for woods of certain deciduous wood species (oak, linden), higher and statistically significant differences in mean values of the limit bending strength depending on the direction of loading were achieved than those reported by Požgaj et al. [
6]. Despite this fact, these differences are considered negligible, and in their works, some authors [
5,
6,
34] report only the values of static bending strength, which were obtained by standardized procedures, i.e., in the tangential direction.
The determined values of static bending strength under load in the tangential direction (
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7) for woods of selected wood species coincide with the range of values specified in [
5,
6,
34], except for Linden wood, for which the mean value of the strength limit in static bending was significantly higher. Similarly, Pelit et al. [
35] state in their work that their ascertained value of static bending strength for linden wood is 60.9 MPa, which is also significantly lower than the value determined in our research.
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7 further show that the highest values of static modulus of elasticity were achieved by birch wood when loading test specimens in the radial direction. The mean value of the static modulus of elasticity in this case was 11,643 MPa. Linden wood achieved the lowest mean value under load in the tangential direction, i.e., 9332 MPa. Other mean values of the static modulus of elasticity depending on the direction of load in the investigated wood species obtained values between the maximum and minimum mean value given above. The highest degree of variability in the values of static modulus of elasticity was shown by oak wood, whilst the lowest degree of variability was observed in ash wood. In both cases, this variability was demonstrated in both the radial and tangential directions of loading. The determined values of the static modulus of elasticity had a similar trend depending on the direction of loading as in bending strength, except for ash wood, where the opposite trend was observed. The static modulus of elasticity values in the woods of the studied wood species are similar to those reported by some authors in their works [
1,
3,
6]. The only exception is birch wood, for which lower values were found compared to the values reported by these authors.
For comparison, dynamic modules of elasticity are also specified in
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7. It turned out that in all of the methods, the highest mean values of dynamic modulus of elasticity were achieved by birch wood, i.e., in the range of 16,883 to 18,808 MPa. The lowest mean values were achieved by spruce wood in all of the methods, i.e., in the range of 7748 to 10,367 MPa. For larch wood, the greatest degree of variability was demonstrated using the ultrasound method (from the fronts), and for the remaining two methods, oak wood had the greatest degree of variability. Ash wood generally showed the lowest degree of variability. Furthermore, it is also evident that the highest mean values of the dynamic modulus of elasticity were achieved in almost all of the examined wood species using the ultrasound method, where piezoelectric sensors were applied to the sample surfaces, except for larch wood, where the opposite trend prevailed. The lowest mean values were achieved with the second ultrasound method (sensors were applied to the end faces of the samples), except for beech and larch wood. Dynamic modules determined via the resonance methods were slightly higher, except for spruce, larch and beech wood, where the opposite trend prevailed. In their work, Oberhofnerová et al. [
21] determined the dynamic modulus of elasticity for spruce and oak wood via the ultrasound method (piezoelectric sensors were applied to the test specimen surfaces) and the resonance method, and there were similar differences between the mean values of the dynamic modulus of elasticity in oak wood as in this work. However, for spruce wood, such high differences were not recorded depending on the method used, as is also the case in this work. Holeček et al. [
20] also found small differences in spruce wood depending on the method used. Based on these facts, it can be concluded that deciduous wood species have larger differences in the values of the dynamic modulus of elasticity depending on the method used than in coniferous trees. This can be explained by the fact that coniferous trees have a simpler anatomical structure than deciduous woods, and the propagation of the sound wave is to some extent influenced by this anatomical structure.
Compared to static modules of elasticity, dynamic modules of elasticity are largely overestimated. In the case of the examined coniferous tree wood, these differences were monitored up to 20%. For wood species with a scattered porous wood structure, these differences were more pronounced, i.e., in the range of 36% to 68%, and for wood species with a circularly porous structure in the range of 21% to 44%.
The graphical representation (
Figure 8) shows that the highest values of impact (dynamic) strength were achieved by birch wood when loading test specimens in the tangential direction. The mean value of impact strength in this case was 10.0 J/cm
2. The lowest mean value was achieved by oak wood in the tangential direction i.e., 4.5 J/cm
2. For linden wood, almost no difference was observed in the average values of impact strength depending on the direction of loading, with a mean value of 6.5 J/cm
2. The largest differences in the average values of dynamic toughness were recorded for spruce wood, which were 9.8 J/cm
2 in the radial direction and 6.5 J/cm
2 in the loading tangential direction. All of the ascertained values are specified in
Table 1,
Table 2,
Table 3,
Table 4,
Table 5,
Table 6 and
Table 7. It is clear from the above tables that the highest degree of variability in the values of dynamic toughness was shown by spruce wood under load in the radial direction and the lowest degree of variability was observed in ash wood, i.e., both in the loading tangential and radial direction. It was also found that the mean values of impact strength depend on both the type of wood species and the direction of loading of the test specimens. There were significant differences depending on the direction of loading in spruce wood, larch, beech, oak, birch and ash. In their work, Požgaj et al. [
6] state that for wood with a significant difference between spring and summer wood, i.e., for coniferous and deciduous wood species with a circularly porous structure, the work consumed for rupturing the test specimen (impact strength) is higher, in the range of 25% to 50%, in the radial than in the tangential direction of loading. Požgaj et al. [
6] did not notice any significant differences in the wood of deciduous wood species with a scattered porous wood structure. It is clear from
Table 8 that this claim agrees for coniferous tree wood and wood species with a circularly porous wood structure, but this is not the case for scattered porous wood species. The table shows that the largest difference in mean values was recorded for spruce wood, i.e., 50.3%, and slightly smaller differences were observed for larch wood 41.2%. Smaller differences of about 20% were recorded for beech, ash and oak wood. For birch wood, a difference was recorded with the opposite trend than for the woods mentioned above, i.e., −9.5%. This peculiarity can be explained by the fact that despite careful selection of the material and verification of its relative “homogeneity”, it was found after image analysis that birch wood shows a significant, but slight ripple in the annual ring that cannot be seen with the human eye (
Figure 5d). It can be concluded from this that this ripple greatly affected the impact strength values. Linden wood showed almost no difference, and this difference (−0.8%) can be considered negligible. Duncan’s test (
Table A2) was used for multiple comparisons. Statistically significant differences in the mean values of impact strength depending on the direction of loading were demonstrated in spruce, larch, beech, birch, oak and ash wood, and in linden wood, no statistically significant difference was demonstrated.
Overall, it can be concluded that the impact strength values between the individual studied wood species and directions of loading are highly influenced by the anatomical structure of the wood of individual wood species and the percentage representation of basic building elements (vessels, tracheids, parenchymal cells, libriform fibers, etc.). Furthermore, it can be concluded that the anatomical structure and the percentage of individual building elements are more pronounced in the determination of dynamic toughness and contribute to the difference in values in the radial and tangential directions of loading than in the case of bending strength under static loading. The values will also be influenced both by the submicroscopic structure of wood (fibrillar structure) and by the representation of basic building biopolymers of wood (cellulose, hemicelluloses, lignin) in individual anatomical elements of wood. In their work, Conrad el. al. [
36] addressed the results of several authors and came to the conclusion that in the case of wood failure, there is a different crack propagation at the microscopic and submicroscopic level of wood depending on the direction of loading, from which it can be deduced that different crack propagation in wood from various selected wood species will also affect the resulting dynamic toughness values. The same can be assumed for static loads in bending (see
Figure 9 and
Figure 10). Furthermore, it can be concluded that with dynamic loading of wood in the radial direction, there is a higher resistance of the material, because the impact energy must alternately pass through the spring and summer wood, which does not occur with loading in the tangential direction.
It is clear that various methodologies can be used to determine the bending characteristics of wood, often using nondestructive principles, such as Near-Infrared Spectroscopy [
37]. However, the standardized methodologies can be said to be, from a principle point of view and in compliance with the conditions of the experiments, still the most accurate methods, especially from the point of view of the validity of the obtained results.
With regard to the investigated wood species, it is often possible to observe dependencies between the individual obtained quantities or properties. Based on this fact, correlation matrices were created (see
Table A4,
Table A5,
Table A6,
Table A7,
Table A8,
Table A9 and
Table A10), by means of which the obtained quantities of wood of individual wood species were compared and, if possible, also depending on the direction of loading. As an example, some of the correlations were converted to graphical form (linear regression, see
Figure 11). From the above graphs and tables, it is clear that relatively strong dependencies were observed between some variables, i.e., in particular in the case of oak wood, where dependence was proven in almost all cases. Dependence was not proven between impact toughness (tangential direction) and bending strength (radial direction), which is of course one of the dependencies without any significant justification. Furthermore, the dependence between impact strength and the dynamic modulus of elasticity was not demonstrated for oak wood. In this case, a statistically significant dependence was demonstrated only between the impact strength (radial direction) and the dynamic modulus of elasticity (radial direction) with a correlation coefficient of r = 0.314. In all other cases, statistically significant dependencies were demonstrated, with higher correlation coefficients than in the previous case. It is evident from the graphical expression (
Figure 11a,b) that a medium–strong dependence (r ≅ 0.50 ÷ 0.75) was demonstrated between bending strength and impact strength, as well as between impact strength and static modulus of elasticity (
Figure 11d). Similar statistically significant dependencies were also observed in oak wood in other cases. Very strong dependences (r > 0.75) were demonstrated between bending strength and static modulus of elasticity (
Figure 11c), between bending strength and density (
Figure 11f) and between the static modulus of elasticity and density (
Figure 11g), as shown, for example, by Dinwoodie [
2]. All of the other investigated dependencies, both for oak and the wood of other investigated wood species, are specified in
Table A4,
Table A5,
Table A6,
Table A7,
Table A8,
Table A9 and
Table A10.