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Article
Peer-Review Record

Experimental Investigation and Computational Fluid Dynamic Simulation of Hydrodynamics of Liquid–Solid Fluidized Beds

ChemEngineering 2022, 6(3), 37; https://doi.org/10.3390/chemengineering6030037
by Amer A. Abdulrahman 1, Omar S. Mahdy 1, Laith S. Sabri 1,2,*, Abbas J. Sultan 1,2, Hayder Al-Naseri 2,3, Zahraa W. Hasan 1, Hasan Shakir Majdi 4 and Jamal M. Ali 1
Reviewer 1: Anonymous
Reviewer 2: Anonymous
Reviewer 3: Anonymous
Reviewer 4: Anonymous
ChemEngineering 2022, 6(3), 37; https://doi.org/10.3390/chemengineering6030037
Submission received: 1 March 2022 / Revised: 3 May 2022 / Accepted: 9 May 2022 / Published: 12 May 2022

Round 1

Reviewer 1 Report

This paper deals with an experimental and modelling study of the fluid dynamics of solid-liquid fluidised beds. The applications are very important such as fluid catalytic cracking (FCC) and fluidised bed combustion (FBC) in the oil industry, granulation in the pharmaceutical industry, chlorination in the semiconductor industry, hydrometallurgy, food technology, biochemical treatment and water treatment.
For this reason, this work may be of interest to readers of the Journal.
Authors should make some revisions prior to publication:

1. Why did you use glass beads of 3 different sizes? Did you want to simulate the presence of particular solids used for example in the processes listed above or did they have another role? Then it would be better to justify, give a reason why these elements have been used and especially the characteristic dimensions and their density.

2. Equations and numbering should be reported according to the Journal standard. In addition some equations should be better written: for example see the 5

3. All parameters in the equations should be described along with the dimensional units: review Eq 11 and 12, they should not go in a table like this. After Eq 11, you will have to say that some parameters like A B etc are given as a function of another parameter etc etc.

4. In the results, when you present a new Figure, the discussion of the results should be inserted after the Figure.

5. You could choose a symbol to indicate the minimum fluidization rate. Also, you could better discuss Figure 3, no details have been added.

6. In Figure 5, you should add the parametric of the last diameter in the caption. Same for Figure 6.

7. The table of symbols in the Conclusions section should be removed. Follow the Journal standards to list the parameters.

Author Response

Why did you use glass beads of 3 different sizes? Did you want to simulate the presence of particular solids used for example in the processes listed above or did they have another role? Then it would be better to justify, give a reason why these elements have been used and especially the characteristic dimensions and their density

 We appreciate the reviewer’s comments very much. As you commented, The particle size distribution (PSD) is an important property that can influence the hydrodynamics and chemical conversion in fluidized bed system. The objective of this study is to investigate the effect of PSDs of particle on pressure drop (ΔP), minimum fluidization velocity (Umf) and individual phase hold-up. As a research team, we are working on the use of catalyst with diameters ranging from 2 mm to 6 mm, and therefore we need to study these dimensions because there are subsequent studies on the heat and mass transfer coefficient.

Equations and numbering should be reported according to the Journal standard. In addition, some equations should be better written: for example see the 5

As suggested by the reviewer, Equations and numbering have been corrected according to the journal standard.

All parameters in the equations should be described along with the dimensional units: review Eq 11 and 12, they should not go in a table like this. After Eq 11, you will have to say that some parameters like A B etc are given as a function of another parameter etc.

 As the reviewer commented, the equations have been corrected

In the results, when you present a new Figure, the discussion of the results should be inserted after the Figure

As commented by the reviewer, this note has been corrected

 

. You could choose a symbol to indicate the minimum fluidization rate. Also, you could better discuss Figure 3, no details have been added

As suggested by the reviewer,  this note has been corrected

In Figure 5, you should add the parametric of the last diameter in the caption. Same for Figure 6.

As suggested by the reviewer, this note has been corrected

The table of symbols in the Conclusions section should be removed. Follow the Journal standards to list the parameters

As commented by the reviewer, this note has been corrected

Author Response File: Author Response.docx

Reviewer 2 Report

  1. LSFB abbreviation from the abstract section is not a common one. Please express the idea in extenso and then use the abbreviations.
  2. In this paragraph “Liquid-solid fluidized beds (LSFBs) have several advantages including; high mixture rates (temperature homogeneity and efficient solid mixing), greater surface area, and a high fluid/solid relative velocity [2].”, is not very clear what “high mixtures rates” is referring to. If is probably related with the velocity of a liquid-solid mixture in a fluidized bed, it must be expressed accordingly. Please rephrase.
  3. The introduction does not state properly the novelty of the results emphasized in the manuscript.
  4. The way equations (5) and (6) are presented is not clear. Please rearrange.
  5. Equation (8) should include a partial derivative on the left side of the equal sign. Please correct.
  6. In order to make the simulation section clearer, please provide the minimum configuration of the system on which the calculations were carried out as well as the software used for these calculations.
  7. Titles of the figures should start with capital letters.
  8. Measurement units representation in table with the symbols should be corrected (i.e. Pa.s is not the right unit for fluid dynamic viscosity).
  9. No clear comparison between modeling and experimental results is provided in the results section, based on numerical results.
  10. The quality of the figures should be drastically improved.
  11. The structure of the manuscript should be improved (Tables interlapping with text sections, equations without proper numbering, several typing errors).

Author Response

No.

Comments

Response to the reviewer

1.

LSFB abbreviation from the abstract section is not a common one. Please express the idea in extenso and then use the abbreviations.

 We appreciate the reviewer’s comments very much. As you commented, this note has been corrected (red color)

 

2.

In this paragraph “Liquid-solid fluidized beds (LSFBs) have several advantages including; high mixture rates (temperature homogeneity and efficient solid mixing), greater surface area, and a high fluid/solid relative velocity [2].”, is

not very clear what “high mixtures rates” is referring to. If is probably related with the velocity of a liquid-solid mixture in a fluidized bed, it must be expressed accordingly. Please rephrase.

As suggested by the reviewer, this note has been corrected (red color)

 

3.

The introduction does not state properly the novelty of the results emphasized in the manuscript.

 As suggested by the reviewer, this note has been corrected (red color)

 

4.

The way equations (5) and (6) are presented is not clear.

Please rearrange.

 

As the reviewer commented, the equations have been corrected

5.

Equation (8) should include a partial derivative on the left side of the equal sign. Please correct.

As the reviewer commented, the equation have been corrected

6.

In order to make the simulation section clearer, please provide the minimum configuration of the system on which

the calculations were carried out as well as the software used

for these calculations.

As suggested by the reviewer, this note has been done                       (red color) and figure 2

 

 

7.

Titles of the figures should start with capital letters.

As suggested by the reviewer, this note has been corrected

8.

Measurement units representation in table with the symbols should be corrected (i.e. Pa.s is not the right unit for fluid dynamic viscosity).

As suggested by the reviewer, this note has been corrected

9

No clear comparison between modeling and experimental results is provided in the results section, based on numerical results.

As suggested by the reviewer, this note has been done (red color) and figures 11, 12 and 13.

 

10

The quality of the figures should be drastically improved.

As suggested by the reviewer, this note has been corrected

11

The structure of the manuscript should be improved (Tables interlapping with text sections, equations without proper numbering, several typing errors).

As suggested by the reviewer, this note has been done and corrected

 

Author Response File: Author Response.docx

Reviewer 3 Report

The paper under review deals with the research on the different hydrodynamic parameters such as pressure drop, minimum fluidization velocity, bed expansion, and individual phase hold-up were investigated using computational fluid dynamics. The results in the study are achieved via simulating study. The idea is of interest and might be within the scope of the journal. The experimental part of the article contains crucial information regarding the research model and method. It also includes the information on the available equipment and presents the research outcomes and their detailed description. The paper is written in good English. The article contains 26 literature items. In my opinion, the paper can be accepted for publication after a major correction.

Short comments:

  1. The scientific side of the article should be clearly indicated. What's new in this article?
  2. Figures 2-6 should be corrected.
  3. The numbers of Equations should be corrected.
  4. The reference’s style should be checked and corrected.
  5. A table in Conclusions???
  6. Reynolds number in Nomenclature – indexes.
  7. mi_f (table in Conclusions) or mi_l (Nomenclature) – fluid viscosity?
  8. Generally, the paper should be corrected and well organized.

Author Response

No.

Comments

Response to the reviewer

1.

The scientific side of the article should be clearly indicated.

What's new in this article?

 

  We appreciate the reviewer’s comments very much. As you commented, The particle size distribution (PSD) is an important property that can influence the hydrodynamics and chemical conversion in fluidized bed system. The objective of this study is to investigate the effect of PSDs of particle on pressure drop (ΔP), minimum fluidization velocity (Umf) and individual phase hold-up. As a research team, we are working on the use of catalyst with diameters ranging from 2 mm to 6 mm, and therefore we need to study these dimensions because there are subsequent studies on the heat and mass transfer coefficient.

2.

Figures 2-6 should be corrected.

As suggested by the reviewer, figures have been corrected according to the journal standard.

3.

The numbers of Equations should be corrected.

 As commented by the reviewer, Equations and numbering have been corrected according to the journal standard.

4.

The reference’s style should be checked and corrected.

As commented by the reviewer, the errors in the format of the references has been corrected, in addition to that, new references have been added.

 

5.

A table in Conclusions???

As commented by the reviewer, this note has been corrected

6.

Reynolds number in Nomenclature – indexes.

As suggested by the reviewer, this note has been corrected

7.

mi_f (table in Conclusions) or mi_l (Nomenclature) – fluid viscosity?

As commented by the reviewer, this note has been corrected

8.

Generally, the paper should be corrected and well organized.

As suggested by the reviewer, this note has been corrected

Author Response File: Author Response.docx

Reviewer 4 Report

The authors have investigated the variation of parameters such as bed expansion, phase hold up, and minimum fluidization velocity with particle size by a combination of experimental and simulation methods. However, I do not consider this paper to be particularly innovative and, given the current research content of the paper, I do not believe that it can be revised to meet the publication requirements of the journal. Therefore, my opinion is: Reject.

(1) The authors should carefully and thoroughly revise the format of the manuscript to meet the publication requirements before submission.

(2) "because of its applications in various process industries, such as fluid catalytic cracking (FCC) and fluidized bed combustion (FBC) in the petroleum industry," like FCC and FBC should belong to gas-solid fluidized bed, right?

(3) I could not find the author's description of the simulation mesh in the manuscript.

(4) The third part is not part of the Results, and should be put in the second part.

(5) In some figures, I can't find the scale. Please ask the author to revise it carefully

(6) For the description of the picture, the author should first describe the content of the picture and then discuss the content of the picture presentation.

(7) Figure 13 is too blurry.

(8) The language of the manuscript needs to be greatly improved.

(9) The references cited by the authors are too old. In addition, there are many errors in the format of the references, so please revise them carefully.

Author Response

No.

Comments

Response to the reviewer

1.

The authors should carefully and thoroughly revise the format of the manuscript to meet the publication requirements before submission.

 We appreciate the reviewer’s comments very much, As commented by the reviewer, this note has been corrected

2.

because of its applications in various process industries, such as fluid catalytic cracking (FCC) and fluidized bed combustion (FBC) in the petroleum industry," like FCC and FBC should belong to gas-solid fluidized bed, right?

Correct, you are right. This note has been corrected as suggested

3.

I could not find the author's description of the simulation mesh in the manuscript.

Right, you can find it now in section (3.1 Simulation Details) and figure 2.

4.

The third part is not part of the Results, and should be put in the second part.

As commented by the reviewer, this note has been corrected

5.

In some figures, I can't find the scale. Please ask the author to revise it carefully

As suggested by the reviewer,  this note has been corrected

6.

For the description of the picture, the author should first describe the content of the picture and then discuss the content of the picture presentation.

As commented by the reviewer, this note has been corrected

7.

Figure 13 is too blurry.

As suggested by the reviewer,  this note has been corrected

8.

The language of the manuscript needs to be greatly improved.

As commented by the reviewer, this note has been corrected

9.

The references cited by the authors are too old. In addition, there are many errors in the format of the references, so please

revise them carefully.

As commented by the reviewer , the errors in the format of the references has been corrected, in addition to that, new references have been added.

Author Response File: Author Response.docx

Round 2

Reviewer 3 Report

In my opinion, it would be better to remove the frames around the Figures. The article can be accepted.

Author Response

No.

Comments

Response to the reviewer

1.

English language and style are fine/minor spell check required.

 

We appreciate the reviewer’s comments very much. As you commented, This comment has been addressed.

2.

In my opinion, it would be better to remove the frames around the Figures.

As commented by the reviewer, this comment has been modified through the whole manuscript.

Author Response File: Author Response.docx

Reviewer 4 Report

Based on the previous review, the authors have improved the quality of the manuscript, but the following problems remain. Therefore, my suggestion is major revision.

(1) "Correspondence: *Correspondence: lssf25@umsystem.edu", please check,

(2) I couldn't find any keywords?

(3) “Abstract: In this study, different hydrodynamic parameters … were investigated using computational fluid dynamics (CFD)” suggested to be changed to ......and individual phase hold-up were investigated using computational fluid dynamics (CFD) and experiment.

(4) Currently, the innovative of the article is not reflected in the manuscript. The authors should highlight the innovative of the article in the abstract and introduction. What new methods were used and what new conclusions were obtained?

(5) The authors discuss some of the results of previous research in the introduction, but do not summaries the work cited., For example, key issues that have been under-researched or have received little attention, highlighting the research difficulties and innovation of this article.

(6) I could not understand what the author was trying to convey in section 1.1 and what it does for the whole article.

(7) I could not find Figure 12

(8) In Figures 11 and 13, why did the author separate A and B. What is the difference in the meaning that the two figures are trying to convey.

(9) Figure 17 is too low quality, please change it.

 

Author Response

No.

Comments

Response to the reviewer

1.

Moderate English changes required.

We appreciate the reviewer’s comments very much. As you commented, This comment has been addressed through the whole manuscript.

2.

 

Does the introduction provide sufficient background and include all relevant references?

 

As the reviewer suggested, this comment has been addressed in the introduction section.

3.

Are the results clearly presented?

As the reviewer commented, this comment has been addressed in results section

4.

Are the conclusions supported by the results?

As the reviewer suggested, this comment has been addressed.

5.

"Correspondence:*Correspondence:

lssf25@umsystem.edu", please check.

As the reviewer commented, this comment has been modified.

6.

I couldn't find any keywords?

As the reviewer commented, this comment has been modified on page 1 after the abstract section.

7.

“Abstract: In this study, different hydrodynamic parameters … were investigated using computational fluid dynamics (CFD)” suggested to be changed to ......and individual phase hold-up were investigated using computational fluid dynamics (CFD) and experiment.

 

As the reviewer suggested, this comment has been addressed and modified in the abstract section on page 1

8.

Currently, the innovative of the article is not reflected in the manuscript. The authors should highlight the innovative of the article in the abstract and introduction. What new methods were used and what new conclusions were obtained?

 

As the reviewer commented, this comment has been modified on page 1 in the abstract section and in the introduction section.

9.

The authors discuss some of the results of previous research in the introduction, but do not summaries the work cited., For example, key issues that have been under-researched or have received little attention, highlighting the research difficulties and innovation of this article.

As the reviewer suggested, this comment has been addressed and modified in the introduction section as a table that summarize the recent studies in fluidized bed on page 6.

10.

I could not understand what the author was trying to convey in section 1.1 and what it does for the whole article.

 

As the reviewer commented, in this section and By using equations (5-6), we predict the fluidization performance, since the Gibilaro et al. equation is equal to 0.183 in the present study, and according to this value, we used CFD simulation for a particulate.

11.

I could not find Figure 12

 

This figure domenstrate comparisons between CFD simulation results and experimental data of solid holdup for particles diameter of 4 mm: (A) solid holdup for different superficial liquid velocities: (B) solid holdup for different superficial liquid velocities with percent error on page 19.

12.

In Figures 11 and 13, why did the author separate A and B. What is the difference in the meaning that the two figures are trying to convey.

Figures (11A-13A) demonstrate the comparisons between CFD simulation results and experimental data of solid holdup for 3,4 and 6 mm particle size, whereas Figures (11B-13B)  maintained comparisons between CFD simulation results and experimental data of solid holdup with percent error.

13.

Figure 17 is too low quality, please change it.

As the reviewer commented, this comment has been modified.

Author Response File: Author Response.docx

Round 3

Reviewer 4 Report

As per the reviewer's comments, the authors have revised the content of the manuscript, but there are still some issues that need to be revised before publication, hence my suggestion is Minor Revision.

1) In the author's response, I was not able to find the page19 mentioned by the author.

2) I still haven't found Figure 12, so I would ask the author to double check that the title note of figure 11-13 is not clearly labelled.

3) The layout of figures 16-17 is too disorganised. I suggest that the author re-arrange the layout and add some necessary notes as appropriate.

4) I believe that figures 11-13 in the manuscript, figures A and B, convey similar meanings, and that figure B alone illustrates the meaning the author intended to convey, so I would ask the author to check.

Author Response

No.

Comments

Response to the reviewer

1.

In the author'sresponse, I was not able to find the page19 mentioned by the author.

 

Because of the use of the magazine's format in organizing the search, there is a new pagination, and thus the number of the specified page has become (13), which contains figure (12).

2.

I still haven't found Figure 12, so I would ask the author to double check that the title note of figure 11-13 is not clearly labelled.

 

As the reviewer commented, this comment has been modified and it is now on page 13.

3.

The layout of figures 16-17 is too disorganised. I suggest that the author re-arrange the layout and add some necessary notes as appropriate.

 

As the reviewer commented, this comment has been modified.

4.

I believe that figures 11-13 in the manuscript, figures A and B, convey similar meanings, and that figure B alone illustrates the meaning the author intended to convey, so I would ask the

author to check.

As the reviewer suggested, this comment has been modified and it is now on page 13.

Author Response File: Author Response.docx

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