Shear Bond Strength and Color Stability of Novel Antibacterial Nanofilled Dental Adhesive Resins
Abstract
:1. Introduction
2. Materials and Methods
2.1. Synthesis of Nanoparticles
2.2. Synthesis of Experimental Adhesives
2.3. Fabrication of Specimens
2.3.1. For Shear Bond Strength Test
2.3.2. For Color Stability Test
2.4. Shear Bond Strength Test
2.5. Scanning Electron Microscopy
2.6. Color Stability Test
2.7. Statistical Analysis
3. Results
4. Discussion
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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24 h–3 Months | 3 Months–6 Months | |
---|---|---|
OPTB | −22.1% | −4.6% |
10% N_TiO2 | −15.4% | −16.0% |
20% N_TiO2 | −22.8% | −15.9% |
30% N_TiO2 | −20.7% | −12.5% |
24 h | 3 Months | 6 Months | |
---|---|---|---|
10% N_TiO2 | 0.0% | 3.3% | 5.5% |
20% N_TiO2 | 4.5% | −1.4% | 0.8% |
30% N_TiO2 | −2.4% | −5.5% | 0.4% |
ΔE00 | ||||||||||
---|---|---|---|---|---|---|---|---|---|---|
GROUP | NUMBER OF CYCLES | |||||||||
1000 | 2000 | 3000 | 4000 | 5000 | 6000 | 7000 | 8000 | 9000 | 10,000 | |
OPTB | 1.3 (0.2) | 1.6 (0.4) | 2.0 (0.5) | 1.8 (0.5) | 2.4 (0.7) | 3.0 (0.6) | 3.0 (0.6) | 3.3 (0.6) | 4.1 (0.6) | 4.1 (0.6) |
10% NF_TiO2 | 0.9 (0.3) | 1.6 (0.4) | 2.2 (0.5) | 2.8 (0.6) | 3.5 (0.8) | 3.7 (0.5) | 4.0 (0.7) | 4.0 (0.7) | 4.6 (0.8) | 4.9 (0.8) |
20% NF_TiO2 | 0.7 (0.3) | 2.7 (1.2) | 2.2 (0.5) | 2.9 (0.9) | 2.8 (0.4) | 3.7 (0.3) | 3.6 (0.3) | 4.0 (0.3) | 4.2 (0.5) | 4.3 (0.4) |
30% NF_TiO2 | 0.7 (0.2) | 1.5 (0.4) | 2.0 (0.5) | 2.0 (0.3) | 2.1 (0.5) | 2.6 (0.6) | 2.5 (0.6) | 2.9 (0.5) | 3.3 (0.7) | 3.8 (0.7) |
ΔEab | ||||||||||
---|---|---|---|---|---|---|---|---|---|---|
GROUP | NUMBER OF CYCLES | |||||||||
1000 | 2000 | 3000 | 4000 | 5000 | 6000 | 7000 | 8000 | 9000 | 10,000 | |
OPTB | 1.0 (0.2) | 1.7 (0.6) | 2.3 (0.6) | 1.8 (0.6) | 2.5 (0.7) | 3.2 (0.7) | 3.2 (0.7) | 3.6 (0.8) | 4.5 (0.7) | 4.4 (1.1) |
10% NF_TiO2 | 1.1 (0.4) | 1.7 (0.6) | 2.5 (0.8) | 3.2 (0.9) | 3.9 (0.9) | 4.2 (0.6) | 4.6 (1.1) | 4.8 (1.1) | 5.1 (0.9) | 5.3 (1.0) |
20% NF_TiO2 | 0.9 (0.5) | 3.8 (1.8) | 2.5 (0.7) | 3.5 (1.4) | 2.8 (0.5) | 4.1 (0.7) | 3.9 (0.5) | 4.4 (0.5) | 4.7 (0.7) | 4.6 (0.5) |
30% NF_TiO2 | 0.9 (0.5) | 1.7 (0.5) | 2.2 (1.0) | 2.3 (0.5) | 2.2 (0.6) | 3.0 (0.7) | 2.6 (0.7) | 3.1 (0.7) | 3.5 (0.7) | 4.2 (0.6) |
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Hong, Q.; Pierre-Bez, A.C.; Kury, M.; Curtis, M.E.; Hiers, R.D.; Esteban Florez, F.L.; Mitchell, J.C. Shear Bond Strength and Color Stability of Novel Antibacterial Nanofilled Dental Adhesive Resins. Nanomaterials 2023, 13, 1. https://doi.org/10.3390/nano13010001
Hong Q, Pierre-Bez AC, Kury M, Curtis ME, Hiers RD, Esteban Florez FL, Mitchell JC. Shear Bond Strength and Color Stability of Novel Antibacterial Nanofilled Dental Adhesive Resins. Nanomaterials. 2023; 13(1):1. https://doi.org/10.3390/nano13010001
Chicago/Turabian StyleHong, Qing, Alexandra C. Pierre-Bez, Matheus Kury, Mark E. Curtis, Rochelle D. Hiers, Fernando L. Esteban Florez, and John C. Mitchell. 2023. "Shear Bond Strength and Color Stability of Novel Antibacterial Nanofilled Dental Adhesive Resins" Nanomaterials 13, no. 1: 1. https://doi.org/10.3390/nano13010001