Mechanical Properties and Liquid Absorption of Calcium Phosphate Composite Cements
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Mechanical Properties Testing
2.2.1. Compressive Strength (According to ISO 4049/2000) [27]
2.2.2. Tensile Strength (According to ADA, Sp.27) [28]
2.2.3. Flexural Strength (According to ISO 4049/2000) [27]
2.3. Liquid Absorption and Solubility Testing
2.4. Statistical Analysis
2.5. X-ray Diffraction (XRD)
2.6. Scanning Electron Microscopy (SEM) Investigation
3. Results and Discussion
3.1. Mechanical Properties
3.2. Liquid Absorption and Solubility
3.3. Crystalline Matter Assesment
3.4. Microstructural Aspects
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Cement | Organic Phase (%) | Inorganic Phase (%) | Initiation System (%) | ||||||
---|---|---|---|---|---|---|---|---|---|
UDMA | HEMA | PEG 400 | PCL | TCP | Chitosan | HA | POB | DHEPT | |
S0 | 3 | 25 | 22 | 0 | 0 | 0 | 0 | 2 | 0.75 |
S1 | 3 | 25 | 22 | 0 | 50 | 0 | 0 | 2 | 0.75 |
S2 | 3 | 25 | 22 | 0 | 37.5 | 12.5 | 0 | 2 | 0.75 |
S3 | 5 | 25 | 20 | 15 | 0 | 17.5 | 17.5 | 2 | 0.75 |
Samples | Identified Elements, Wt.%. | |||
---|---|---|---|---|
C | O | P | Ca | |
S0 | 63.54 | 36.46 | - | - |
S1 | 35.6 | 22.5 | 16.76 | 25.14 |
S2 | 44.12 | 26.37 | 10.75 | 18.76 |
S3 | 39.18 | 24.56 | 13.79 | 22.47 |
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Lacan, I.; Moldovan, M.; Sarosi, C.; Cuc, S.; Pastrav, M.; Petean, I.; Ene, R. Mechanical Properties and Liquid Absorption of Calcium Phosphate Composite Cements. Materials 2023, 16, 5653. https://doi.org/10.3390/ma16165653
Lacan I, Moldovan M, Sarosi C, Cuc S, Pastrav M, Petean I, Ene R. Mechanical Properties and Liquid Absorption of Calcium Phosphate Composite Cements. Materials. 2023; 16(16):5653. https://doi.org/10.3390/ma16165653
Chicago/Turabian StyleLacan, Ioana, Marioara Moldovan, Codruta Sarosi, Stanca Cuc, Mihaela Pastrav, Ioan Petean, and Razvan Ene. 2023. "Mechanical Properties and Liquid Absorption of Calcium Phosphate Composite Cements" Materials 16, no. 16: 5653. https://doi.org/10.3390/ma16165653