10-Methacryloyloxydecyl Dihydrogen Phosphate (10-MDP)-Containing Cleaner Improves Bond Strength to Contaminated Monolithic Zirconia: An In-Vitro Study
Abstract
:1. Introduction
2. Materials and Methods
2.1. Zirconia Specimen Preparation
2.2. Contamination and Decontamination
2.3. Shear Bond Strength (SBS) Test
2.4. Failure Mode Evaluation
2.5. Statistical Analysis
3. Results
3.1. SBS
3.2. Failure Modes
4. Discussion
5. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Material (Manufacturer) | Composition |
---|---|
inCoris TZI C medi S (Sirona Dental Systems GmbH, Bensheim, Germany) LOT: 3314000419 | ZrO2, HfO2, Y2O3, Al2O3, other oxides |
Etch-Rite (Pulpdent Corp., Watertown, MA, USA) LOT: 200114 | 38% phosphoric acid gel |
Isopropanol Alcohol Ez CLEAN (Avalon Pharma; Riyadh, Saudi Arabia. LOT: 2040027 | Isopropanol alcohol (C3H8O, 70%), water (30%) |
Ivoclean (Ivoclar Vivadent, Schaan, Lichtenstein) LOT: Y36272 | ZrO2, water, polyethylene glycol, sodium hydroxide, pigments and additives |
Katana Cleaner (Kuraray Noritake, Tokyo, Japan) LOT: 3C0006 | Water, 10-MDP, triethanolamine, polyethylene glycol, stabilizer, dyes |
Z-Prime Plus (Bisco Inc., Schaumburg, IL, USA) LOT: 2000006418 | 10-MDP, BPDM, HEMA, ethanol |
Multilink N (Ivoclar Vivadent, Schaan, Liechtenstein) LOT: Z00RKM | Dimethacrylate, HEMA, barium glass, ytterbium trifluoride, spheroid mixed oxide |
Group Code | Contamination | Decontamination Protocol |
---|---|---|
Un-No | Uncontaminated | No decontamination |
Sa-No | Saliva |
|
Sa-Etch | Saliva |
|
Sa-Alc | Saliva |
|
Sa-Ivoc | Saliva |
|
Sa-Kat | Saliva |
|
Bl-No | Blood |
|
Bl-Etch | Blood |
|
Bl-Alc | Blood |
|
Bl-Ivoc | Blood |
|
Bl-Kat | Blood |
|
SBS (24 h) | SBS (10 k TC) | |||
---|---|---|---|---|
Mean ± 1 SD (2 MPa) | 3 ptf/4 n | Mean ± SD (MPa) | ptf/n | |
Un-No | 19.33 ± 5.136 a | 0/10 | 7.479 ± 3.64 A,* | 0/10 |
Sa-No | 5.751 ± 1.874 b | 0/10 | 0.3036 ± 0.96 B,* | 9/10 |
Sa-Etch | 7.93 ± 2.527 b | 0/10 | 1.508 ± 1.713 B,* | 5/10 |
Sa-Alc | 7.469 ± 2.711 b | 0/10 | 0.8409 ± 1.435 B,* | 7/10 |
Sa-Ivoc | 18.18 ± 3.969 c | 0/10 | 6.297 ± 3.083 C,* | 0/10 |
Sa-Kat | 15.51 ± 4.44 c | 0/10 | 5.206 ± 2.212 C,* | 0/10 |
Bl-No | 8.117 ± 2.321 b | 0/10 | 0.8493 ± 1.439 B,* | 7/10 |
Bl-Etch | 8.482 ± 3.999 b | 0/10 | 0.7488 ± 1.041 B,* | 6/10 |
Bl-Alc | 9.312 ± 3.761 b | 0/10 | 1.061 ± 2.294 B,* | 7/10 |
Bl-Ivoc | 16.17 ± 5.43 c | 0/10 | 7.08 ± 3.309 C,* | 0/10 |
Bl-Kat | 14.62 ± 3.439 c | 0/10 | 6.026 ± 2.805 C,* | 0/10 |
1 Df | 2 Sum Sq | 3 Mean Sq | F Value | p-Value | Significance | |
---|---|---|---|---|---|---|
Contamination | 2 | 734.6 | 367.3 | 372,831 | <0.001 | * |
Cleaner | 4 | 2274.4 | 568.6 | 577,185 | <0.001 | * |
Aging | 1 | 3971.5 | 3971.5 | 4,031,383 | <0.001 | * |
Contamination × Cleaner | 4 | 29.8 | 7.4 | 0.7550 | 0.556 | |
Contamination × Aging | 2 | 61.8 | 30.9 | 31,381 | 0.045 | * |
Cleaner × Aging | 4 | 120.2 | 30.1 | 30,509 | 0.018 | * |
Contamination × Cleaner × Aging | 4 | 46.1 | 11.5 | 11,687 | 0.326 | |
Residuals | 198 | 1950.6 | 9.9 |
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Awad, M.M.; Alhalabi, F.; Alzahrani, K.M.; Almutiri, M.; Alqanawi, F.; Albdiri, L.; Alshehri, A.; Alrahlah, A.; Ahmed, M.H. 10-Methacryloyloxydecyl Dihydrogen Phosphate (10-MDP)-Containing Cleaner Improves Bond Strength to Contaminated Monolithic Zirconia: An In-Vitro Study. Materials 2022, 15, 1023. https://doi.org/10.3390/ma15031023
Awad MM, Alhalabi F, Alzahrani KM, Almutiri M, Alqanawi F, Albdiri L, Alshehri A, Alrahlah A, Ahmed MH. 10-Methacryloyloxydecyl Dihydrogen Phosphate (10-MDP)-Containing Cleaner Improves Bond Strength to Contaminated Monolithic Zirconia: An In-Vitro Study. Materials. 2022; 15(3):1023. https://doi.org/10.3390/ma15031023
Chicago/Turabian StyleAwad, Mohamed M., Feras Alhalabi, Khaled Mosfer Alzahrani, Majed Almutiri, Fawaz Alqanawi, Lafi Albdiri, Abdullah Alshehri, Ali Alrahlah, and Mohammed H. Ahmed. 2022. "10-Methacryloyloxydecyl Dihydrogen Phosphate (10-MDP)-Containing Cleaner Improves Bond Strength to Contaminated Monolithic Zirconia: An In-Vitro Study" Materials 15, no. 3: 1023. https://doi.org/10.3390/ma15031023