Ascorbic Acid Sensor Based on CdS QDs@PDA Fluorescence Resonance Energy Transfer
Abstract
:1. Introduction
2. Results and Discussion
2.1. Characterization
2.1.1. TEM Characterization
2.1.2. X-ray Photoelectron Spectroscopy (XPS) Characterization of CdS QDs and CdS QDs@PDA
2.1.3. FTIR Characterization of DA and CdS QDs@PDA
2.1.4. UV-Vis and Fluorescence Lifetime Characterization
2.2. Optimum Proposal
2.2.1. Study on Fluorescence Quenching and Recovery of CdS QDs
2.2.2. Effect of DA Concentration and Reaction Time on Fluorescence Quenching of CdS QDs
2.3. Analysis Characteristics of Sensors
2.3.1. Linear Range and Detection Limits
2.3.2. Selectivity
2.3.3. Actual Sample Analysis and Recovery
3. Experiment
3.1. Material and Reagents
3.2. Apparatus
3.3. Synthesis of CdS QDs
3.4. Optimization of Fluorescence Quenching Conditions
3.5. Determination of Ascorbic Acid
3.6. Actual Sample Handling
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
Sample Availability
References
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Sample | Labeled (g/Piece) |
Detected/μmol·L−1 | Added /μmol/L |
Found/μmol/L |
Recovery/% |
---|---|---|---|---|---|
Vc tables | 0.1 | 7.28 ± 0.61 | 7.50 | 14.63 ± 0.11 | 98.01 ± 1.47 |
20.23 ± 0.80 | 20.00 | 40.19 ± 0.81 | 100.7 ± 1.55 | ||
40.88 ± 1.68 | 40.00 | 80.46 ± 1.05 | 99.01 ± 2.60 |
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Li, P.; Chen, X.; Wu, G.; Wang, Z.; Huang, C. Ascorbic Acid Sensor Based on CdS QDs@PDA Fluorescence Resonance Energy Transfer. Molecules 2022, 27, 2097. https://doi.org/10.3390/molecules27072097
Li P, Chen X, Wu G, Wang Z, Huang C. Ascorbic Acid Sensor Based on CdS QDs@PDA Fluorescence Resonance Energy Transfer. Molecules. 2022; 27(7):2097. https://doi.org/10.3390/molecules27072097
Chicago/Turabian StyleLi, Pu, Xiaoxiao Chen, Gaojun Wu, Zhe Wang, and Chaobiao Huang. 2022. "Ascorbic Acid Sensor Based on CdS QDs@PDA Fluorescence Resonance Energy Transfer" Molecules 27, no. 7: 2097. https://doi.org/10.3390/molecules27072097