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Exclusive Papers of the Editorial Board Members and Topical Advisory...
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Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry"

A special issue of Catalysts (ISSN 2073-4344). This special issue belongs to the section "Catalysis in Organic and Polymer Chemistry".

Deadline for manuscript submissions: closed (31 December 2023) | Viewed by 9185

Special Issue Editors

Prof. Dr. Kotohiro Nomura

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Department of Chemistry, Graduate School of Science, Tokyo Metropolitan University (TMU), 1-1 Minami Osawa, Hachioji, Tokyo 192-0397, Japan
Interests: homogeneous catalysis; organometallics; catalysis and fine chemicals; precise olefin polymerization
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Prof. Dr. Raffaella Mancuso

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Laboratory of Industrial and Synthetic Organic Chemistry (LISOC), Department of Chemistry and Chemical Technologies, University of Calabria, Via Pietro Bucci 12/C, 87036 Arcavacata di Rende, CS, Italy
Interests: innovative syntheses of high-value molecules through catalytic process; new syntheses of heterocyclic compounds of pharmaceutical interest; carbonylation catalyzed chemistry; application of unconventional solvents in advanced organic synthesis; synthesis of novel materials for advanced applications
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Prof. Dr. Zhengguo Cai

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State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, College of Materials Science and Engineering, Donghua University, Shanghai 201620, China
Interests: polymer chemistry; organometallic catalysis; coordination polymerization
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Prof. Dr. Samuel Dagorne

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Institut de Chimie de Strasbourg, CNRS-Université de Strasbourg, 1 Rue Blaise Pascal, 67000 Strasbourg, France
Interests: organometallic complexes; homogeneous catalysis; polymerization; oxophilic and electrophilic metal species
Prof. Dr. Moris S. Eisen

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Schulich Faculty of Chemistry, Technion-Israel Institute of Technology, Haifa 3200008, Israel
Interests: actinide and lanthanide organometallic chemistry; polymerisation catalysis; organo-f-complexes in catalysis; small molecule activation; transition metal organometallic chemistry; metal-ligand multiple bonding; group 4 organometallics in catalysis
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Dr. Luca Gonsalvi

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Institute of Chemistry of Organometallic Compounds, National Research Council of Italy (ICCOM-CNR), Via Madonna del Piano 10, 50019 Sesto Fiorentino, Florence, Italy
Interests: organometallics and catalysis in water and biphasic systems; CO2 activation and utilization processes; hydrogen activation, production, and storage by organometallics; homogeneous catalysis; catalytic mechanisms
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Prof. Dr. Martin Kotora

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Department of Organic Chemistry, Faculty of Science, Charles University, Hlavova 8, 12843 Prague, Czech Republic
Interests: transition metal complex catalysis; asymmetric synthesis; organometallic chemistry; organocatalysis
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Prof. Dr. Bun Yeoul Lee

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Department of Molecular Science and Technology, Ajou University, Suwon 16499, Republic of Korea
Interests: organic chemistry; polymer synthesis; green chemistry; organometallics; polymerization catalyst chemistry
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Prof. Dr. Shaofeng Liu

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Key Laboratory of Biobased Polymer Materials, College of Polymer Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, China
Interests: organometallic catalysts for olefin polymerization; organocatalysts for ring-opening polymerization; structure-property relationships of catalysts
Prof. Dr. Luísa Margarida Martins

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Centro de Química Estrutural e Departamento de Engenharia Química, Institute of Molecular Sciences, Instituto Superior Técnico, Universidade de Lisboa, Av. Rovisco Pais, 1049-001 Lisboa, Portugal
Interests: green chemistry; innovative product design; sustainable processes; functionalized materials (in particular, involving C-scorpionates); catalysis (homogeneous, supported or nano- catalysis); electrochemistry
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Prof. Dr. Takeshi Ohkuma

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1. Division of Applied Chemistry, Faculty of Engineering, Hokkaido University, Sapporo, Hokkaido 060-8628, Japan
2. Frontier Chemistry Center, Faculty of Engineering, Hokkaido University, Sapporo, Hokkaido 060-8628, Japan
Interests: dual catalysis; allylic alcohol; asymmetric cyanation; combined metal catalyst; unsaturated ketone; unsaturated carbonyl compound; asymmetric isomerization; box ligands; Cu complexes; Pd nanoparticles; photocyclization; kinetic resolution; DPEN; DAIPEN; XylBINAP; BINAP; TolBINAP; DMAPEN; PICA; IPHAN; LiCl; organometallic chemistry; synthetic organic chemistry (4602); organometallic chemistry (4072); asymmetric catalysis (4072); research areas applied chemistry/functional materials chemistry
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Prof. Dr. Armando Pombeiro

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Centro de Quimica Estrutural, Instituto Superior Tecnico, Lisbon, Portugal
Interests: coordination chemistry; oxidation catalysis; electrocatalysis; alkane functionalization; carboxylation; C-C coupling; non-covalent interactions in synthesis
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Prof. Dr. Fabio Ragaini

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Dipartimento di Chimica, Università degli Studi di Milano, Via C. Golgi 19, 20133 Milan, Italy
Interests: homogeneous catalysis; carbonylation reactions; nitroarene reductive cyclization; nitroarene reductive carbonylation; catalytic synthesis of isocyanates, carbamates, and ureas; oxidative carbonylation of amines; nitrogen-enriched graphitic metal catalysts; synthesis and use of nitrogen ligands
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Prof. Dr. Carl Redshaw

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Department of Chemistry, University of Hull, Hull, UK
Interests: calixarenes; coordination chemistry’ catalysis; polymers; imaging and anti-cancer agents
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Prof. Dr. Marc Visseaux

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UMR 8181—UCCS—Unité de Catalyse et Chimie du Solide, Université de Lille, CNRS, Centrale Lille, Université d'Artois, F-59000 Lille, France
Interests: coordinative polymerization catalysis; rare-earth and iron organometallic chemistry
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Prof. Dr. Zongquan Wu

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State Key Laboratory of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun 130012, China
Interests: catalysts for living polymerization; chiral polymers; functional materials
Prof. Dr. Hiroto Yoshida

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Department of Applied Chemistry, Graduate School of Engineering, Hiroshima University, Higashi-Hiroshima 739-8527, Japan
Interests: copper catalysis; borylation; stannylation; silylation; main group organometallics; cross-coupling; multicomponent coupling; aryne chemistry
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Prof. Dr. Masamichi Ogasawara

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Department of Natural Science, Graduate School of Science and Technology, Tokushima University, Minamijosanjima-cho, Tokushima 770-8506, Japan
Interests: organometallic chemistry; homogeneous catalysis; asymmetric synthesis

Special Issue Information

Dear Colleagues,

We are pleased to announce the launch of a new Special Issue, “Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry"”. This will be a collection of papers edited by the editorial board members of the Section “Catalysis in Organic and Polymer Chemistry.” The issue will covers papers with a wide scope in the field of homogeneous catalysis, organometallic chemistry, and polymer chemistry, including such topics as sustainable polymers (prepared by coordination polymerization, ring opening polymerization), polyolefin synthesis, chemical recycling (conversion to monomers) and upcycling (conversion to upgraded chemicals, polymers), biobased polymers, and related catalysis chemistry. Topics related to the design of molecular catalysis, including mechanistic studies, which are at the core of homogeneous catalysis, will be highly welcome to this Special Issue.

We look forward to receiving many outstanding submissions on the topics above, which will contribute to the creation of an important Special Issue in this journal.

Prof. Dr. Kotohiro Nomura
Prof. Dr. Raffaella Mancuso
Prof. Dr. Zhengguo Cai
Prof. Dr. Samuel Dagorne
Prof. Dr. Moris S. Eisen
Dr. Luca Gonsalvi 
Prof. Dr. Martin Kotora
Prof. Dr. Bun Yeoul Lee
Prof. Dr. Shaofeng Liu
Prof. Dr. Luísa Margarida Martins
Prof. Dr. Takeshi Ohkuma
Prof. Dr. Armando Pombeiro
Prof. Dr. Fabio Ragaini 
Prof. Dr. Carl Redshaw
Prof. Dr. Marc Visseaux
Prof. Dr. Zongquan Wu
Prof. Dr. Hiroto Yoshida
Prof. Dr. Masamichi Ogasawara
Guest Editors

Manuscript Submission Information

Manuscripts should be submitted online at www.mdpi.com by registering and logging in to this website. Once you are registered, click here to go to the submission form. Manuscripts can be submitted until the deadline. All submissions that pass pre-check are peer-reviewed. Accepted papers will be published continuously in the journal (as soon as accepted) and will be listed together on the special issue website. Research articles, review articles as well as short communications are invited. For planned papers, a title and short abstract (about 100 words) can be sent to the Editorial Office for announcement on this website.

Submitted manuscripts should not have been published previously, nor be under consideration for publication elsewhere (except conference proceedings papers). All manuscripts are thoroughly refereed through a single-blind peer-review process. A guide for authors and other relevant information for submission of manuscripts is available on the Instructions for Authors page. Catalysts is an international peer-reviewed open access monthly journal published by MDPI.

Please visit the Instructions for Authors page before submitting a manuscript. The Article Processing Charge (APC) for publication in this open access journal is 2700 CHF (Swiss Francs). Submitted papers should be well formatted and use good English. Authors may use MDPI's English editing service prior to publication or during author revisions.

Keywords

  • molecular catalyst
  • green sustainable catalysts
  • sustainable polymers
  • chemical recycling
  • upcycling
  • organometallics
  • polymerization
  • catalyzed fine chemicals synthesis
  • designed catalysts
  • green reaction pathways

Published Papers (7 papers)

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Research

Jump to: Review

12 pages, 1886 KiB  
Article
Molybdenum-Catalyzed Enantioselective Ring-Closing Metathesis/Kinetic Resolution of Racemic Planar-Chiral 1,1′-Diallylferrocenes
by Haruna Imazu, Kakeru Masaoka, Saki Uike and Masamichi Ogasawara
Catalysts 2024, 14(2), 123; https://doi.org/10.3390/catal14020123 - 04 Feb 2024
Viewed by 1041
Abstract
The molybdenum-catalyzed enantioselective ring-closing metathesis/kinetic resolution of a series of racemic planar-chiral 1,1′-diallylferrocene derivatives was reinvestigated utilizing the method of generating catalytically active chiral molybdenum-alkylidene species in situ, which allowed us to examine a variety of chiral molybdenum-alkylidene metathesis precatalysts in the present [...] Read more.
The molybdenum-catalyzed enantioselective ring-closing metathesis/kinetic resolution of a series of racemic planar-chiral 1,1′-diallylferrocene derivatives was reinvestigated utilizing the method of generating catalytically active chiral molybdenum-alkylidene species in situ, which allowed us to examine a variety of chiral molybdenum-alkylidene metathesis precatalysts in the present asymmetric reaction. With the catalyst screening experiments conducted in this study, the more practical reaction conditions, including a choice of a proper chiral molybdenum precatalyst, giving planar-chiral ferrocenes of higher enantiomeric purity and better chemoselectivity could be optimized. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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21 pages, 3983 KiB  
Article
Exploring Long Range para-Phenyl Effects in Unsymmetrically Fused bis(imino)pyridine-Cobalt Ethylene Polymerization Catalysts
by Yizhou Wang, Zheng Wang, Qiuyue Zhang, Song Zou, Yanping Ma, Gregory A. Solan, Wenjuan Zhang and Wen-Hua Sun
Catalysts 2023, 13(10), 1387; https://doi.org/10.3390/catal13101387 - 23 Oct 2023
Cited by 1 | Viewed by 943
Abstract
Unsymmetrical 11-phenyl-1,2,3,7,8,9,10-heptahydrocyclohepta[b]quinoline-4,6-dione, incorporating a para-phenyl substituted pyridine unit fused by both 6- and 7-membered carbocyclic rings, has been prepared on the gram-scale via a multi-step procedure involving cyclization, hydrogenation and oxidation. Templating this diketone, in the presence of cobalt(II) chloride [...] Read more.
Unsymmetrical 11-phenyl-1,2,3,7,8,9,10-heptahydrocyclohepta[b]quinoline-4,6-dione, incorporating a para-phenyl substituted pyridine unit fused by both 6- and 7-membered carbocyclic rings, has been prepared on the gram-scale via a multi-step procedure involving cyclization, hydrogenation and oxidation. Templating this diketone, in the presence of cobalt(II) chloride hexahydrate, with the corresponding aniline afforded in good yield five examples of doubly fused bis(arylimino)pyridine-cobalt(II) chlorides, Co1 (aryl = 2,6-dimethylphenyl), Co2 (2,6-diethylphenyl), Co3 (2,6-diisopropylphenyl), Co4 (2,4,6-trimethylphenyl) and Co5 (2,6-diethyl-4-methylphenyl). Structural characterization of Co1, Co2 and Co3 highlights the flexible nature of the inequivalent fused rings on the NNN’-ligand and the skewed disposition of the para-phenyl group. On activation with MAO, Co1–Co5 exhibited high activity for ethylene polymerization at 30 °C (up to 5.66 × 106 g (PE) mol−1 (Co) h−1) with the relative order being as follows: Co4 > Co1 > Co5 > Co3 > Co2. All polyethylenes were strictly linear, while their molecular weights and dispersities showed some notable variations. For Co1, Co2, Co4 and Co5, all polymerizations were well controlled as evidenced by the narrow dispersities of their polymers (Mw/Mn range: 1.8–2.7), while their molecular weights (Mw range: 2.9–10.9 kg mol−1) steadily increased in line with the greater steric properties of the N-aryl ortho-substituents. By contrast, the most hindered 2,6-diisopropyl counterpart Co3 displayed a broad distribution with bimodal characteristics (Mw/Mn = 10.3) and gave noticeably higher molecular weight polymer (Mw = 75.5 kg mol−1). By comparison, the MMAO-activated catalysts were generally less active, but showed similar trends in molecular weight and polymer dispersity. End group analysis of selected polymers via 13C and 1H NMR spectroscopy revealed the presence of both saturated and unsaturated polyethylenes in accordance with competing chain transfer pathways. Notably, when comparing Co3/MAO with its non-phenyl substituted analogue (E2,6-iPr2Ph)CoCl2/MAO, the former, though less controlled, displayed higher activity and molecular weight, a finding that points towards a role played by the remote para-phenyl group. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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10 pages, 1796 KiB  
Article
Expression of Reaction Selectivity and the Substituent Effect in Ullmann, Suzuki, Hiyama, and Allylic Arylation Reactions Caused by Reducing Catalyst Loading
by Misa Kawase, Tomohiro Shibata, Shouhei Masuu, Masaki Yamaguchi, Yoshimasa Matsumura, Osamu Shimomura and Atsushi Ohtaka
Catalysts 2023, 13(7), 1115; https://doi.org/10.3390/catal13071115 - 17 Jul 2023
Cited by 1 | Viewed by 877
Abstract
The control of stereo-, regio-, and chemo-selectivity in transition-metal-catalyzed coupling reactions is a key topic in organic synthesis. Several methods for controlling selectivity have been reported thus far. On the other hand, the reduction of catalyst loading during reactions is one of the [...] Read more.
The control of stereo-, regio-, and chemo-selectivity in transition-metal-catalyzed coupling reactions is a key topic in organic synthesis. Several methods for controlling selectivity have been reported thus far. On the other hand, the reduction of catalyst loading during reactions is one of the most important issues in organic synthesis from the standpoint of green sustainable chemistry. As another advantage of reducing catalyst loading, the expression of reaction selectivity and the substituent effect caused by the reduction of catalyst loading to the parts-per-million (ppm) level in various catalytic reactions is presented herein. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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12 pages, 2554 KiB  
Article
Synthesis of Cationic [4], [5], and [6]Azahelicenes with Extended π-Conjugated Systems
by Samuel Hrubý, Jan Ulč, Ivana Císařová and Martin Kotora
Catalysts 2023, 13(5), 912; https://doi.org/10.3390/catal13050912 - 22 May 2023
Viewed by 1289
Abstract
The scope of Rh-catalyzed C–C bond cleavage/annulation of biphenylene with various aromatic nitriles was studied. The subsequent Rh- and Ir-catalyzed C–H bond activation/annulation sequence of the formed 9-arylphenanthridines with alkynes gave rise to cationic [4], [5], [6] helical quinolizinium salts. The scope of [...] Read more.
The scope of Rh-catalyzed C–C bond cleavage/annulation of biphenylene with various aromatic nitriles was studied. The subsequent Rh- and Ir-catalyzed C–H bond activation/annulation sequence of the formed 9-arylphenanthridines with alkynes gave rise to cationic [4], [5], [6] helical quinolizinium salts. The scope of the reaction with respect to the structural features of the starting 9-arylphenanthridines and alkynes was studied. Their helical arrangement was confirmed through single-crystal X-ray analyses of selected compounds. Most of the prepared quinolizinium salts exhibited fluorescence emission maxima in the region of 525–623 nm with absolute quantum yields up to 25%. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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Review

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19 pages, 10744 KiB  
Review
Air-Stable and Highly Active Transition Metal Phosphide Catalysts for Reductive Molecular Transformations
by Takato Mitsudome
Catalysts 2024, 14(3), 193; https://doi.org/10.3390/catal14030193 - 12 Mar 2024
Viewed by 1093
Abstract
This review introduces transition metal phosphide nanoparticle catalysts as highly efficient and reusable heterogeneous catalysts for various reductive molecular transformations. These transformations include the hydrogenation of nitriles to primary amines, reductive amination of carbonyl compounds, and biomass conversion, specifically, the aqueous hydrogenation reaction [...] Read more.
This review introduces transition metal phosphide nanoparticle catalysts as highly efficient and reusable heterogeneous catalysts for various reductive molecular transformations. These transformations include the hydrogenation of nitriles to primary amines, reductive amination of carbonyl compounds, and biomass conversion, specifically, the aqueous hydrogenation reaction of mono- and disaccharides to sugar alcohols. Unlike traditional air-unstable non-precious metal catalysts, these are stable in air, eliminating the need for strict anaerobic conditions or pre-reduction. Moreover, when combined with supports, metal phosphides exhibit significantly enhanced activity, demonstrating high activity, selectivity, and durability in these hydrogenation reactions. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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17 pages, 4191 KiB  
Review
Acyclic Diene Metathesis (ADMET) Polymerization for the Synthesis of Chemically Recyclable Bio-Based Aliphatic Polyesters
by Kotohiro Nomura and Xiuxiu Wang
Catalysts 2024, 14(2), 97; https://doi.org/10.3390/catal14020097 - 24 Jan 2024
Viewed by 1097
Abstract
The recent developments of the synthesis of bio-based long-chain aliphatic polyesters by the acyclic diene metathesis (ADMET) polymerization of α,ω-dienes, derived from plant oils and bio-based chemicals, like bis(10-undecenoate) with isosorbide, using ruthenium-carbene catalysts are reviewed. The development of subsequent (one-pot) tandem hydrogenation [...] Read more.
The recent developments of the synthesis of bio-based long-chain aliphatic polyesters by the acyclic diene metathesis (ADMET) polymerization of α,ω-dienes, derived from plant oils and bio-based chemicals, like bis(10-undecenoate) with isosorbide, using ruthenium-carbene catalysts are reviewed. The development of subsequent (one-pot) tandem hydrogenation produced saturated polyesters under mild conditions. The polymerizations under bulk (without solvent, 80–90 °C) or in ionic liquids (50 °C) under vacuum conditions enabled the synthesis of high molar mass polymers (Mn > 30,000 g/mol). The polymerization performed by the molybdenum-alkylidene catalyst afforded the highest-molecular-weight polyesters (44,000–49,400 g/mol, in toluene at 25 °C) exhibiting promising tensile properties (strength and elongation at break) compared to polyethylene and polypropylene. Depolymerizations of these polyesters, including closed-loop chemical recycling, were also demonstrated. Catalyst developments (more active, under mild conditions) play a key role in the efficient synthesis of these materials. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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54 pages, 20385 KiB  
Review
Comprehensive Overview of Homogeneous Gold-Catalyzed Transformations of π-Systems for Application Scientists
by Ioannis Stylianakis and Antonios Kolocouris
Catalysts 2023, 13(6), 921; https://doi.org/10.3390/catal13060921 - 23 May 2023
Cited by 1 | Viewed by 2144
Abstract
We present an overview of fundamental catalytic reactions of nucleophiles with π-systems in relation to gold chemistry. We present examples of reactions with gold-activated π-systems, alkynyl or allenyl moieties, and the regulation of their reactivity due to the presence of an electron-donating or [...] Read more.
We present an overview of fundamental catalytic reactions of nucleophiles with π-systems in relation to gold chemistry. We present examples of reactions with gold-activated π-systems, alkynyl or allenyl moieties, and the regulation of their reactivity due to the presence of an electron-donating or -withdrawing group. The reactions describe furnished hard-to-reach heterocyclic building blocks for medicinal chemistry purposes. Important gold(I) or gold(III) complexes that are used as catalysts are presented. We examine the activation of such π-systems using gold(I) or gold(III) catalysts and the corresponding divergent catalytic transformations. We provide examples of divergent catalysis using gold(I) catalyst and other metal catalysts (Pt, Ag, Pd, Rh, Sc, Cu) or by changing the ligands in gold(I) catalyst complexes. We also discuss the role of the solvent, counterions and additives in gold(I)-catalyzed reactions. We mention, in a few cases, characteristic experimental or computational studies of these gold-catalyzed reactions of nucleophiles with π-systems. Full article
(This article belongs to the Special Issue Exclusive Papers of the Editorial Board Members and Topical Advisory Panel Members of Catalysts in Section "Catalysis in Organic and Polymer Chemistry")
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