Performance Evaluation of CNT Reinforcement on Electroless Plating on Solid Free-Form-Fabricated PETG Specimens for Prosthetic Limb Application
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Methods
2.2.1. Fabrication of 3D-Printed Specimens
2.2.2. Electroless Copper Metallization of 3D-Printed PETG-MWCNT Samples
2.2.3. Tensile Test
2.2.4. Dynamic Mechanical Analysis
2.2.5. Heat Distortion Temperature
2.2.6. Wear Test
2.2.7. Water Contact Angle Measurements (Wettability Test)
2.2.8. Scratch Test
2.2.9. Microhardness
3. Results and Discussion
3.1. Tensile Strength
3.2. Dynamic Mechanical Analysis
3.3. Heat Distortion Test
3.4. Wear
3.5. Contact Angle
3.6. Scratch Test
- P = applied load;
- w = width of the scratch measured from the microscope;
- = constant value.
3.7. Microhardness
4. Conclusions
- With the addition of MWCNTs to the PETG, there was an improvement in the base material properties. Furthermore, the electroless metal layer coating enhanced the strength of the PETG material.
- The heat distortion temperature value increased due to the coating on the PETG-MWCNT compared to the uncoated PETG sample, showing that the material can resist high temperatures; hence, the blended PETG+MWCNT polymer with the coating can be extensively used for various applications.
- The wear characterization specified that the initial wear rate was considerably decreased due to the thickness of the electroless metal layer coating on the PETG-MWCNT specimen, and through the contact angle measurement, it was evident that, with a greater coating thickness on the PETG-MWCNT specimen, the wettability was maximum.
- From the scratch test, it was noted that the PETG-MWCNT substrates coated with Ni had the lowest penetration depth and lowest friction coefficient. The microhardness test indicated the high indentation hardness and, hence, proved that it is superior in terms of abrasion resistance.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Scratch No. | Load (N) | Stroke Length (mm) | Scratch Velocity (mm/s) | Scratch Offset (mm) |
---|---|---|---|---|
1 | 10.0 | 10 | 1.0 | 0.50 |
2 | 20.0 | 10 | 1.0 | 0.50 |
3 | 30.0 | 10 | 1.0 | 0.50 |
Material | UTS | Young’s Modulus (MPa) |
---|---|---|
PETG | 29.41 | 490.03 |
Coated PETG | 32.37 | 491.04 |
PETG+MWCNT | 34.86 | 516.87 |
Coated PETG+MWCNT | 37.72 | 571.5 |
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Siddikali, P.; Sreekanth, P.S.R. Performance Evaluation of CNT Reinforcement on Electroless Plating on Solid Free-Form-Fabricated PETG Specimens for Prosthetic Limb Application. Polymers 2022, 14, 3366. https://doi.org/10.3390/polym14163366
Siddikali P, Sreekanth PSR. Performance Evaluation of CNT Reinforcement on Electroless Plating on Solid Free-Form-Fabricated PETG Specimens for Prosthetic Limb Application. Polymers. 2022; 14(16):3366. https://doi.org/10.3390/polym14163366
Chicago/Turabian StyleSiddikali, Palaiam, and P. S. Rama Sreekanth. 2022. "Performance Evaluation of CNT Reinforcement on Electroless Plating on Solid Free-Form-Fabricated PETG Specimens for Prosthetic Limb Application" Polymers 14, no. 16: 3366. https://doi.org/10.3390/polym14163366