data_pfpetherabs _audit_creation_date 2023-02-16 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _shelx_SHELXL_version_number '2016/6' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C25 H8 F14 N2 O2' _chemical_formula_sum 'C25 H8 F14 N2 O2' _chemical_formula_weight 634.33 _chemical_melting_point ? _chemical_oxdiff_formula 'C25 H8 N2 O2 F14' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 61 _space_group_name_H-M_alt 'P b c a' _space_group_name_Hall '-P 2ac 2ab' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 16.4796(2) _cell_length_b 11.46540(10) _cell_length_c 24.7037(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4667.65(9) _cell_formula_units_Z 8 _cell_measurement_reflns_used 55350 _cell_measurement_temperature 100.00(15) _cell_measurement_theta_max 27.3750 _cell_measurement_theta_min 1.6360 _shelx_estimated_absorpt_T_max 0.955 _shelx_estimated_absorpt_T_min 0.931 _exptl_absorpt_coefficient_mu 0.192 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.276 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.805 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description prism _exptl_crystal_F_000 2512 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -4 -5 -1 0.1504 3 3 -5 0.0996 0 0 1 0.0970 -1 -1 5 0.1179 2 3 5 0.1621 1 -5 -4 0.1278 -5 -1 -1 0.1296 5 1 1 0.1831 5 -4 -3 0.1664 4 -5 -4 0.1450 -3 -1 5 0.1227 4 2 -5 0.1134 1 5 -5 0.0874 -2 0 -5 0.1385 3 0 5 0.1709 -5 -1 -3 0.1310 -1 1 0 0.1820 -5 -1 1 0.1290 -4 -1 5 0.1239 2 -5 0 0.1265 -3 -5 -3 0.1505 -4 1 5 0.1579 -5 0 -2 0.1440 0 -1 -5 0.1486 1 -5 4 0.1366 1 -2 5 0.1515 2 0 5 0.1478 5 1 -5 0.1425 _exptl_crystal_size_max 0.379 _exptl_crystal_size_mid 0.298 _exptl_crystal_size_min 0.242 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -4.0000 -5.0000 -1.0000 -0.0012 0.0760 -0.3469 3.0000 3.0000 -5.0000 0.0016 -0.2047 0.1729 0.0000 0.0000 1.0000 -0.0041 0.0272 0.0083 -1.0000 -1.0000 5.0000 -0.0143 0.1588 -0.0298 2.0000 3.0000 5.0000 -0.0026 0.0785 0.2372 1.0000 -5.0000 -4.0000 -0.1733 -0.0627 -0.2771 -5.0000 -1.0000 -1.0000 0.1580 0.0415 -0.1557 5.0000 1.0000 1.0000 -0.1580 -0.0415 0.1557 5.0000 -4.0000 -3.0000 -0.2944 -0.0927 -0.1403 4.0000 -5.0000 -4.0000 -0.2840 -0.0970 -0.2202 -3.0000 -1.0000 5.0000 0.0595 0.1817 -0.0678 4.0000 2.0000 -5.0000 -0.0659 -0.2046 0.1393 1.0000 5.0000 -5.0000 0.1365 -0.2048 0.2400 -2.0000 -0.0000 -5.0000 0.0944 -0.1130 -0.0796 3.0000 0.0000 5.0000 -0.1313 0.1016 0.0986 -5.0000 -1.0000 -3.0000 0.1662 -0.0129 -0.1724 -1.0000 1.0000 0.0000 0.0675 -0.0001 0.0336 -5.0000 -1.0000 1.0000 0.1498 0.0958 -0.1390 -4.0000 -1.0000 5.0000 0.0964 0.1931 -0.0867 2.0000 -5.0000 -0.0000 -0.2266 0.0346 -0.2248 -3.0000 -5.0000 -3.0000 -0.0298 0.0103 -0.3446 -4.0000 1.0000 5.0000 0.1576 0.1701 0.0183 -5.0000 -0.0000 -2.0000 0.1927 0.0028 -0.1115 -0.0000 -1.0000 -5.0000 -0.0100 -0.1244 -0.0942 1.0000 -5.0000 4.0000 -0.2062 0.1547 -0.2104 1.0000 -2.0000 5.0000 -0.1186 0.1474 -0.0444 2.0000 0.0000 5.0000 -0.0944 0.1130 0.0796 5.0000 1.0000 -5.0000 -0.1333 -0.2045 0.1057 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0340 _diffrn_reflns_av_unetI/netI 0.0150 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.969 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 81813 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.969 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.467 _diffrn_reflns_theta_min 1.649 _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(15) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -27.00 30.00 0.50 10.00 -- 8.73 -87.00 -41.00 114 2 \w 12.00 37.00 0.50 10.00 -- 8.73 87.00 75.00 50 3 \w -25.00 46.00 0.50 10.00 -- -9.44 87.00 75.00 142 4 \w -43.00 18.00 0.50 10.00 -- -9.44 -87.00 -41.00 122 5 \w -61.00 -24.00 0.50 10.00 -- 8.73 -19.00-150.00 74 6 \w -20.00 5.00 0.50 10.00 -- 8.73 -19.00 60.00 50 7 \w -21.00 21.00 0.50 10.00 -- 8.73 -99.00 -90.00 84 8 \w 9.00 57.00 0.50 10.00 -- 8.73-125.00 90.00 96 9 \w -23.00 14.00 0.50 10.00 -- 8.73 -99.00 30.00 74 10 \w 11.00 57.00 0.50 10.00 -- 8.73-125.00 60.00 92 11 \w 0.00 79.00 0.50 10.00 -- 8.73 19.00 90.00 158 12 \w 9.00 55.00 0.50 10.00 -- 8.73-125.00-120.00 92 13 \w 4.00 50.00 0.50 10.00 -- 8.73 77.00 -60.00 92 14 \w -57.00 33.00 0.50 10.00 -- 8.73 -77.00 -90.00 180 15 \w -48.00 -22.00 0.50 10.00 -- 8.73 -19.00 60.00 52 16 \w 24.00 51.00 0.50 10.00 -- -9.44 37.00-180.00 54 17 \w -6.00 21.00 0.50 10.00 -- -9.44 -99.00 150.00 54 18 \w -53.00 -14.00 0.50 10.00 -- -9.44 125.00 150.00 78 19 \w -18.00 8.00 0.50 10.00 -- -9.44 37.00-180.00 52 20 \w 17.00 43.00 0.50 10.00 -- -9.44 37.00 -60.00 52 21 \w -56.00 -9.00 0.50 10.00 -- -9.44 125.00 60.00 94 22 \w -19.00 13.00 0.50 10.00 -- -9.44 37.00 -60.00 64 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at offset/far, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0368931000 _diffrn_orient_matrix_UB_12 0.0305716000 _diffrn_orient_matrix_UB_13 -0.0041150000 _diffrn_orient_matrix_UB_21 -0.0114341000 _diffrn_orient_matrix_UB_22 -0.0114951000 _diffrn_orient_matrix_UB_23 0.0271732000 _diffrn_orient_matrix_UB_31 0.0189680000 _diffrn_orient_matrix_UB_32 0.0525403000 _diffrn_orient_matrix_UB_33 0.0083346000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4485 _reflns_number_total 5176 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 0.332 _refine_diff_density_min -0.248 _refine_diff_density_rms 0.042 _refine_ls_extinction_coef 0.00068(17) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 389 _refine_ls_number_reflns 5176 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0365 _refine_ls_R_factor_gt 0.0300 _refine_ls_restrained_S_all 1.063 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0361P)^2^+2.0816P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0765 _refine_ls_wR_factor_ref 0.0800 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C7(H7), C8(H8), C10(H10), C11(H11), C16(H16), C17(H17), C19(H19), C20(H20) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F1 F 1.15729(5) 0.66212(8) 0.55022(4) 0.0367(2) Uani 1 1 d . . . . . F2 F 1.04400(5) 0.82405(7) 0.57350(3) 0.02691(18) Uani 1 1 d . . . . . F3 F 0.85316(5) 0.51614(7) 0.58345(4) 0.0330(2) Uani 1 1 d . . . . . F4 F 0.97659(6) 0.36823(7) 0.56348(4) 0.0348(2) Uani 1 1 d . . . . . F5 F 0.40806(5) 0.49772(7) 0.44400(3) 0.0316(2) Uani 1 1 d . . . . . F6 F 0.42943(4) 0.64999(6) 0.52656(3) 0.02354(17) Uani 1 1 d . . . . . F7 F 0.22173(5) 0.44717(7) 0.61969(3) 0.02799(19) Uani 1 1 d . . . . . F8 F 0.20495(5) 0.31176(7) 0.52998(4) 0.0332(2) Uani 1 1 d . . . . . F9 F 0.69287(5) 0.87106(8) 0.78546(4) 0.0366(2) Uani 1 1 d . . . . . F10 F 0.56655(5) 0.84885(8) 0.80513(3) 0.0337(2) Uani 1 1 d . . . . . F11 F 0.60204(5) 0.93241(7) 0.73036(3) 0.02980(19) Uani 1 1 d . . . . . F12 F 0.64483(5) 0.52632(7) 0.75731(3) 0.02714(18) Uani 1 1 d . . . . . F13 F 0.67971(5) 0.65280(8) 0.81743(3) 0.0329(2) Uani 1 1 d . . . . . F14 F 0.55366(5) 0.61473(8) 0.80395(3) 0.0312(2) Uani 1 1 d . . . . . O1 O 0.88847(6) 0.76007(8) 0.58940(4) 0.0284(2) Uani 1 1 d . . . . . O2 O 0.32829(5) 0.62707(8) 0.61927(4) 0.0222(2) Uani 1 1 d . . . . . N1 N 1.06683(7) 0.51528(10) 0.55769(5) 0.0265(3) Uani 1 1 d . . . . . N2 N 0.30663(7) 0.40581(10) 0.48759(5) 0.0254(2) Uani 1 1 d . . . . . C1 C 1.08124(8) 0.62796(12) 0.56003(5) 0.0240(3) Uani 1 1 d . . . . . C2 C 1.02404(8) 0.71099(11) 0.57179(5) 0.0204(3) Uani 1 1 d . . . . . C3 C 0.94451(8) 0.67639(11) 0.58145(5) 0.0203(3) Uani 1 1 d . . . . . C4 C 0.92871(8) 0.55716(12) 0.57795(5) 0.0228(3) Uani 1 1 d . . . . . C5 C 0.99211(9) 0.48276(11) 0.56700(5) 0.0243(3) Uani 1 1 d . . . . . C6 C 0.82443(8) 0.74270(11) 0.62617(5) 0.0223(3) Uani 1 1 d . . . . . C7 C 0.83543(8) 0.68933(12) 0.67570(6) 0.0257(3) Uani 1 1 d . . . . . H7 H 0.886927 0.658655 0.685510 0.031 Uiso 1 1 calc R U . . . C8 C 0.76992(8) 0.68112(12) 0.71107(5) 0.0233(3) Uani 1 1 d . . . . . H8 H 0.776818 0.644452 0.745250 0.028 Uiso 1 1 calc R U . . . C9 C 0.69441(7) 0.72611(11) 0.69686(5) 0.0190(3) Uani 1 1 d . . . . . C10 C 0.68594(8) 0.78048(11) 0.64658(5) 0.0214(3) Uani 1 1 d . . . . . H10 H 0.634824 0.812119 0.636572 0.026 Uiso 1 1 calc R U . . . C11 C 0.75058(8) 0.78913(11) 0.61108(5) 0.0229(3) Uani 1 1 d . . . . . H11 H 0.744239 0.826314 0.576978 0.028 Uiso 1 1 calc R U . . . C12 C 0.62024(7) 0.72607(11) 0.73484(5) 0.0189(3) Uani 1 1 d . . . . . C13 C 0.62513(8) 0.62974(12) 0.77879(5) 0.0237(3) Uani 1 1 d . . . . . C14 C 0.62038(8) 0.84533(12) 0.76435(6) 0.0256(3) Uani 1 1 d . . . . . C15 C 0.54111(7) 0.70518(11) 0.70314(5) 0.0173(2) Uani 1 1 d . . . . . C16 C 0.47119(8) 0.77261(11) 0.70846(5) 0.0198(3) Uani 1 1 d . . . . . H16 H 0.471057 0.837176 0.732561 0.024 Uiso 1 1 calc R U . . . C17 C 0.40177(7) 0.74671(11) 0.67904(5) 0.0206(3) Uani 1 1 d . . . . . H17 H 0.354754 0.794147 0.682275 0.025 Uiso 1 1 calc R U . . . C18 C 0.40183(7) 0.65109(11) 0.64498(5) 0.0181(2) Uani 1 1 d . . . . . C19 C 0.46988(7) 0.58156(11) 0.63934(5) 0.0186(2) Uani 1 1 d . . . . . H19 H 0.469016 0.515407 0.616196 0.022 Uiso 1 1 calc R U . . . C20 C 0.53939(7) 0.61006(11) 0.66806(5) 0.0185(2) Uani 1 1 d . . . . . H20 H 0.586778 0.563811 0.663728 0.022 Uiso 1 1 calc R U . . . C21 C 0.32630(7) 0.55298(11) 0.57635(5) 0.0189(3) Uani 1 1 d . . . . . C22 C 0.26899(7) 0.46384(12) 0.57640(5) 0.0213(3) Uani 1 1 d . . . . . C23 C 0.26134(8) 0.39547(11) 0.53095(6) 0.0238(3) Uani 1 1 d . . . . . C24 C 0.36138(8) 0.48840(12) 0.48804(5) 0.0229(3) Uani 1 1 d . . . . . C25 C 0.37343(7) 0.56571(11) 0.53007(5) 0.0195(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F1 0.0164(4) 0.0346(5) 0.0593(6) 0.0055(4) 0.0073(4) 0.0018(3) F2 0.0231(4) 0.0202(4) 0.0375(4) -0.0010(3) 0.0030(3) -0.0041(3) F3 0.0219(4) 0.0266(4) 0.0505(5) 0.0051(4) 0.0028(4) -0.0068(3) F4 0.0436(5) 0.0184(4) 0.0423(5) -0.0010(3) 0.0066(4) -0.0012(4) F5 0.0388(5) 0.0341(5) 0.0219(4) -0.0025(3) 0.0085(3) 0.0023(4) F6 0.0210(4) 0.0237(4) 0.0260(4) 0.0009(3) 0.0030(3) -0.0036(3) F7 0.0198(4) 0.0372(5) 0.0270(4) 0.0053(3) 0.0028(3) -0.0053(3) F8 0.0265(4) 0.0255(4) 0.0475(5) -0.0029(4) -0.0058(4) -0.0078(3) F9 0.0280(4) 0.0400(5) 0.0417(5) -0.0161(4) -0.0130(4) -0.0016(4) F10 0.0336(5) 0.0413(5) 0.0261(4) -0.0136(4) 0.0012(3) 0.0053(4) F11 0.0288(4) 0.0214(4) 0.0392(5) -0.0053(3) -0.0029(4) -0.0002(3) F12 0.0268(4) 0.0253(4) 0.0293(4) 0.0065(3) -0.0004(3) 0.0034(3) F13 0.0293(4) 0.0484(5) 0.0210(4) 0.0036(4) -0.0086(3) 0.0014(4) F14 0.0243(4) 0.0456(5) 0.0236(4) 0.0077(4) 0.0045(3) 0.0019(4) O1 0.0216(5) 0.0224(5) 0.0412(6) 0.0088(4) 0.0113(4) 0.0045(4) O2 0.0136(4) 0.0312(5) 0.0219(4) -0.0071(4) -0.0005(3) 0.0008(4) N1 0.0252(6) 0.0254(6) 0.0290(6) 0.0013(5) 0.0034(5) 0.0047(5) N2 0.0268(6) 0.0232(6) 0.0262(6) -0.0030(5) -0.0049(5) 0.0032(5) C1 0.0173(6) 0.0276(7) 0.0270(7) 0.0028(5) 0.0012(5) 0.0007(5) C2 0.0202(6) 0.0200(6) 0.0210(6) 0.0010(5) -0.0010(5) -0.0017(5) C3 0.0180(6) 0.0214(6) 0.0216(6) 0.0030(5) 0.0012(5) 0.0025(5) C4 0.0190(6) 0.0236(6) 0.0259(7) 0.0034(5) 0.0006(5) -0.0035(5) C5 0.0309(7) 0.0182(6) 0.0239(6) 0.0006(5) -0.0001(5) -0.0005(5) C6 0.0172(6) 0.0194(6) 0.0305(7) 0.0011(5) 0.0053(5) -0.0007(5) C7 0.0160(6) 0.0278(7) 0.0334(7) 0.0037(6) -0.0020(5) 0.0029(5) C8 0.0193(6) 0.0266(7) 0.0239(6) 0.0027(5) -0.0034(5) 0.0015(5) C9 0.0163(6) 0.0189(6) 0.0219(6) -0.0021(5) -0.0007(5) -0.0010(5) C10 0.0166(6) 0.0211(6) 0.0263(6) 0.0022(5) -0.0018(5) 0.0023(5) C11 0.0216(6) 0.0214(6) 0.0258(6) 0.0054(5) 0.0015(5) 0.0012(5) C12 0.0165(6) 0.0215(6) 0.0185(6) -0.0017(5) -0.0018(5) 0.0015(5) C13 0.0191(6) 0.0323(7) 0.0196(6) 0.0019(5) -0.0012(5) 0.0014(5) C14 0.0214(7) 0.0289(7) 0.0264(7) -0.0074(5) -0.0036(5) 0.0009(5) C15 0.0153(6) 0.0204(6) 0.0162(5) 0.0010(5) -0.0001(4) -0.0007(5) C16 0.0194(6) 0.0208(6) 0.0193(6) -0.0031(5) 0.0008(5) 0.0018(5) C17 0.0155(6) 0.0246(6) 0.0216(6) -0.0009(5) 0.0023(5) 0.0040(5) C18 0.0137(6) 0.0237(6) 0.0168(6) 0.0019(5) 0.0002(4) -0.0016(5) C19 0.0189(6) 0.0189(6) 0.0180(6) -0.0016(5) 0.0009(5) -0.0007(5) C20 0.0161(6) 0.0196(6) 0.0200(6) 0.0008(5) 0.0018(5) 0.0031(5) C21 0.0152(6) 0.0218(6) 0.0197(6) -0.0004(5) -0.0037(5) 0.0037(5) C22 0.0153(6) 0.0254(6) 0.0231(6) 0.0046(5) -0.0010(5) 0.0015(5) C23 0.0194(6) 0.0206(6) 0.0315(7) 0.0014(5) -0.0069(5) -0.0006(5) C24 0.0240(7) 0.0250(7) 0.0196(6) 0.0007(5) 0.0000(5) 0.0052(5) C25 0.0168(6) 0.0190(6) 0.0227(6) 0.0016(5) -0.0015(5) 0.0012(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F1 C1 1.3353(15) . ? F2 C2 1.3380(15) . ? F3 C4 1.3379(15) . ? F4 C5 1.3407(15) . ? F5 C24 1.3368(15) . ? F6 C25 1.3390(14) . ? F7 C22 1.3366(15) . ? F8 C23 1.3361(15) . ? F9 C14 1.3365(16) . ? F10 C14 1.3431(16) . ? F11 C14 1.3390(16) . ? F12 C13 1.3389(16) . ? F13 C13 1.3381(15) . ? F14 C13 1.3429(15) . ? O1 C3 1.3461(15) . ? O1 C6 1.4065(15) . ? O2 C18 1.3957(15) . ? O2 C21 1.3590(15) . ? N1 C1 1.3148(19) . ? N1 C5 1.3070(18) . ? N2 C23 1.3110(18) . ? N2 C24 1.3079(18) . ? C1 C2 1.3709(19) . ? C2 C3 1.3900(18) . ? C3 C4 1.3943(18) . ? C4 C5 1.3756(19) . ? C6 C7 1.3802(19) . ? C6 C11 1.3796(19) . ? C7 H7 0.9500 . ? C7 C8 1.3920(19) . ? C8 H8 0.9500 . ? C8 C9 1.3922(18) . ? C9 C10 1.3966(18) . ? C9 C12 1.5408(17) . ? C10 H10 0.9500 . ? C10 C11 1.3833(18) . ? C11 H11 0.9500 . ? C12 C13 1.5508(18) . ? C12 C14 1.5496(18) . ? C12 C15 1.5399(16) . ? C15 C16 1.3939(17) . ? C15 C20 1.3933(17) . ? C16 H16 0.9500 . ? C16 C17 1.3874(18) . ? C17 H17 0.9500 . ? C17 C18 1.3820(18) . ? C18 C19 1.3830(17) . ? C19 H19 0.9500 . ? C19 C20 1.3863(17) . ? C20 H20 0.9500 . ? C21 C22 1.3915(18) . ? C21 C25 1.3900(18) . ? C22 C23 1.3752(19) . ? C24 C25 1.3795(18) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 O1 C6 120.54(10) . . ? C21 O2 C18 119.96(10) . . ? C5 N1 C1 116.27(12) . . ? C24 N2 C23 116.82(11) . . ? F1 C1 C2 118.70(12) . . ? N1 C1 F1 116.72(12) . . ? N1 C1 C2 124.58(12) . . ? F2 C2 C1 120.69(12) . . ? F2 C2 C3 120.20(11) . . ? C1 C2 C3 119.11(12) . . ? O1 C3 C2 117.94(11) . . ? O1 C3 C4 125.43(12) . . ? C2 C3 C4 116.44(12) . . ? F3 C4 C3 120.81(12) . . ? F3 C4 C5 120.58(12) . . ? C5 C4 C3 118.58(12) . . ? F4 C5 C4 118.37(12) . . ? N1 C5 F4 116.60(12) . . ? N1 C5 C4 124.98(12) . . ? C7 C6 O1 122.46(12) . . ? C11 C6 O1 115.65(11) . . ? C11 C6 C7 121.77(12) . . ? C6 C7 H7 120.5 . . ? C6 C7 C8 118.99(12) . . ? C8 C7 H7 120.5 . . ? C7 C8 H8 119.7 . . ? C9 C8 C7 120.66(12) . . ? C9 C8 H8 119.7 . . ? C8 C9 C10 118.61(12) . . ? C8 C9 C12 123.74(11) . . ? C10 C9 C12 117.55(11) . . ? C9 C10 H10 119.4 . . ? C11 C10 C9 121.26(12) . . ? C11 C10 H10 119.4 . . ? C6 C11 C10 118.71(12) . . ? C6 C11 H11 120.6 . . ? C10 C11 H11 120.6 . . ? C9 C12 C13 112.66(10) . . ? C9 C12 C14 106.56(10) . . ? C14 C12 C13 107.40(11) . . ? C15 C12 C9 111.23(10) . . ? C15 C12 C13 106.81(10) . . ? C15 C12 C14 112.20(10) . . ? F12 C13 F14 106.41(11) . . ? F12 C13 C12 111.46(10) . . ? F13 C13 F12 107.14(10) . . ? F13 C13 F14 106.53(10) . . ? F13 C13 C12 113.19(11) . . ? F14 C13 C12 111.70(10) . . ? F9 C14 F10 106.91(11) . . ? F9 C14 F11 106.38(11) . . ? F9 C14 C12 112.32(11) . . ? F10 C14 C12 112.24(11) . . ? F11 C14 F10 107.39(11) . . ? F11 C14 C12 111.26(11) . . ? C16 C15 C12 124.46(11) . . ? C20 C15 C12 117.09(11) . . ? C20 C15 C16 118.42(11) . . ? C15 C16 H16 119.6 . . ? C17 C16 C15 120.90(12) . . ? C17 C16 H16 119.6 . . ? C16 C17 H17 120.4 . . ? C18 C17 C16 119.22(11) . . ? C18 C17 H17 120.4 . . ? C17 C18 O2 115.66(11) . . ? C17 C18 C19 121.28(11) . . ? C19 C18 O2 122.99(11) . . ? C18 C19 H19 120.6 . . ? C18 C19 C20 118.86(11) . . ? C20 C19 H19 120.6 . . ? C15 C20 H20 119.3 . . ? C19 C20 C15 121.30(11) . . ? C19 C20 H20 119.3 . . ? O2 C21 C22 118.35(11) . . ? O2 C21 C25 124.24(11) . . ? C25 C21 C22 117.20(11) . . ? F7 C22 C21 120.07(12) . . ? F7 C22 C23 121.22(12) . . ? C23 C22 C21 118.69(12) . . ? F8 C23 C22 119.20(12) . . ? N2 C23 F8 116.51(12) . . ? N2 C23 C22 124.29(12) . . ? F5 C24 C25 118.57(12) . . ? N2 C24 F5 116.61(11) . . ? N2 C24 C25 124.81(12) . . ? F6 C25 C21 120.94(11) . . ? F6 C25 C24 120.94(11) . . ? C24 C25 C21 118.11(12) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F1 C1 C2 F2 -0.11(19) . . . . ? F1 C1 C2 C3 179.27(12) . . . . ? F2 C2 C3 O1 3.64(18) . . . . ? F2 C2 C3 C4 178.92(11) . . . . ? F3 C4 C5 F4 -1.80(19) . . . . ? F3 C4 C5 N1 175.60(13) . . . . ? F5 C24 C25 F6 1.40(18) . . . . ? F5 C24 C25 C21 -178.03(11) . . . . ? F7 C22 C23 F8 0.73(19) . . . . ? F7 C22 C23 N2 -178.73(12) . . . . ? O1 C3 C4 F3 -1.2(2) . . . . ? O1 C3 C4 C5 176.78(12) . . . . ? O1 C6 C7 C8 176.50(12) . . . . ? O1 C6 C11 C10 -176.74(11) . . . . ? O2 C18 C19 C20 -177.65(11) . . . . ? O2 C21 C22 F7 -5.02(17) . . . . ? O2 C21 C22 C23 173.85(11) . . . . ? O2 C21 C25 F6 4.80(19) . . . . ? O2 C21 C25 C24 -175.76(11) . . . . ? N1 C1 C2 F2 179.80(12) . . . . ? N1 C1 C2 C3 -0.8(2) . . . . ? N2 C24 C25 F6 -178.04(12) . . . . ? N2 C24 C25 C21 2.5(2) . . . . ? C1 N1 C5 F4 178.55(12) . . . . ? C1 N1 C5 C4 1.1(2) . . . . ? C1 C2 C3 O1 -175.74(12) . . . . ? C1 C2 C3 C4 -0.46(19) . . . . ? C2 C3 C4 F3 -176.07(11) . . . . ? C2 C3 C4 C5 1.90(19) . . . . ? C3 O1 C6 C7 40.87(19) . . . . ? C3 O1 C6 C11 -143.10(13) . . . . ? C3 C4 C5 F4 -179.77(12) . . . . ? C3 C4 C5 N1 -2.4(2) . . . . ? C5 N1 C1 F1 -179.55(12) . . . . ? C5 N1 C1 C2 0.5(2) . . . . ? C6 O1 C3 C2 -144.65(12) . . . . ? C6 O1 C3 C4 40.53(19) . . . . ? C6 C7 C8 C9 -0.1(2) . . . . ? C7 C6 C11 C10 -0.7(2) . . . . ? C7 C8 C9 C10 -0.5(2) . . . . ? C7 C8 C9 C12 -176.75(12) . . . . ? C8 C9 C10 C11 0.55(19) . . . . ? C8 C9 C12 C13 -24.03(17) . . . . ? C8 C9 C12 C14 93.50(14) . . . . ? C8 C9 C12 C15 -143.93(12) . . . . ? C9 C10 C11 C6 0.0(2) . . . . ? C9 C12 C13 F12 -48.03(14) . . . . ? C9 C12 C13 F13 72.83(14) . . . . ? C9 C12 C13 F14 -166.93(10) . . . . ? C9 C12 C14 F9 -49.18(14) . . . . ? C9 C12 C14 F10 -169.68(10) . . . . ? C9 C12 C14 F11 69.94(13) . . . . ? C9 C12 C15 C16 -131.39(13) . . . . ? C9 C12 C15 C20 50.56(15) . . . . ? C10 C9 C12 C13 159.71(11) . . . . ? C10 C9 C12 C14 -82.76(13) . . . . ? C10 C9 C12 C15 39.81(15) . . . . ? C11 C6 C7 C8 0.7(2) . . . . ? C12 C9 C10 C11 177.01(12) . . . . ? C12 C15 C16 C17 -178.85(12) . . . . ? C12 C15 C20 C19 177.50(11) . . . . ? C13 C12 C14 F9 71.78(14) . . . . ? C13 C12 C14 F10 -48.72(13) . . . . ? C13 C12 C14 F11 -169.10(10) . . . . ? C13 C12 C15 C16 105.30(14) . . . . ? C13 C12 C15 C20 -72.75(13) . . . . ? C14 C12 C13 F12 -165.07(10) . . . . ? C14 C12 C13 F13 -44.21(14) . . . . ? C14 C12 C13 F14 76.04(13) . . . . ? C14 C12 C15 C16 -12.13(17) . . . . ? C14 C12 C15 C20 169.82(11) . . . . ? C15 C12 C13 F12 74.38(12) . . . . ? C15 C12 C13 F13 -164.76(10) . . . . ? C15 C12 C13 F14 -44.51(14) . . . . ? C15 C12 C14 F9 -171.14(11) . . . . ? C15 C12 C14 F10 68.36(14) . . . . ? C15 C12 C14 F11 -52.02(14) . . . . ? C15 C16 C17 C18 1.44(19) . . . . ? C16 C15 C20 C19 -0.67(18) . . . . ? C16 C17 C18 O2 176.42(11) . . . . ? C16 C17 C18 C19 -0.58(19) . . . . ? C17 C18 C19 C20 -0.88(18) . . . . ? C18 O2 C21 C22 130.65(12) . . . . ? C18 O2 C21 C25 -54.82(17) . . . . ? C18 C19 C20 C15 1.51(18) . . . . ? C20 C15 C16 C17 -0.83(19) . . . . ? C21 O2 C18 C17 165.09(11) . . . . ? C21 O2 C18 C19 -17.97(17) . . . . ? C21 C22 C23 F8 -178.13(11) . . . . ? C21 C22 C23 N2 2.4(2) . . . . ? C22 C21 C25 F6 179.39(11) . . . . ? C22 C21 C25 C24 -1.18(18) . . . . ? C23 N2 C24 F5 179.23(11) . . . . ? C23 N2 C24 C25 -1.32(19) . . . . ? C24 N2 C23 F8 179.30(11) . . . . ? C24 N2 C23 C22 -1.2(2) . . . . ? C25 C21 C22 F7 -179.93(11) . . . . ? C25 C21 C22 C23 -1.06(18) . . . . ? _shelx_res_file ; TITL pfpetherabs_a.res in Pbca pfpetherabs.res created by SHELXL-2016/6 at 16:28:05 on 16-Feb-2023 REM Old TITL PFPEtherABS in Pbca REM SHELXT solution in Pbca REM R1 0.105, Rweak 0.002, Alpha 0.010, Orientation as input REM Formula found by SHELXT: C25 N2 O3 F13 CELL 0.71073 16.4796 11.4654 24.7037 90 90 90 ZERR 8 0.0002 0.0001 0.0003 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H F N O UNIT 200 64 112 16 16 L.S. 10 PLAN 5 SIZE 0.242 0.298 0.379 TEMP -173 CONF BOND $H list 4 fmap 2 53 ACTA MORE -1 REM REM REM WGHT 0.036100 2.081600 EXTI 0.000678 FVAR 0.28714 F1 3 1.157294 0.662118 0.550222 11.00000 0.01636 0.03457 = 0.05927 0.00553 0.00729 0.00175 F2 3 1.044001 0.824054 0.573498 11.00000 0.02309 0.02016 = 0.03747 -0.00104 0.00296 -0.00411 F3 3 0.853156 0.516137 0.583450 11.00000 0.02190 0.02657 = 0.05051 0.00515 0.00277 -0.00679 F4 3 0.976585 0.368230 0.563476 11.00000 0.04359 0.01841 = 0.04229 -0.00103 0.00658 -0.00115 F5 3 0.408059 0.497722 0.443999 11.00000 0.03879 0.03409 = 0.02190 -0.00253 0.00849 0.00233 F6 3 0.429429 0.649988 0.526557 11.00000 0.02095 0.02365 = 0.02601 0.00087 0.00302 -0.00363 F7 3 0.221734 0.447175 0.619691 11.00000 0.01985 0.03717 = 0.02695 0.00534 0.00280 -0.00526 F8 3 0.204953 0.311764 0.529985 11.00000 0.02647 0.02552 = 0.04750 -0.00294 -0.00584 -0.00779 F9 3 0.692869 0.871063 0.785465 11.00000 0.02800 0.03998 = 0.04168 -0.01612 -0.01302 -0.00164 F10 3 0.566552 0.848852 0.805134 11.00000 0.03365 0.04130 = 0.02613 -0.01357 0.00121 0.00535 F11 3 0.602039 0.932406 0.730360 11.00000 0.02877 0.02141 = 0.03923 -0.00531 -0.00292 -0.00016 F12 3 0.644827 0.526323 0.757312 11.00000 0.02685 0.02529 = 0.02928 0.00649 -0.00038 0.00338 F13 3 0.679709 0.652798 0.817435 11.00000 0.02935 0.04840 = 0.02100 0.00360 -0.00864 0.00136 F14 3 0.553660 0.614728 0.803949 11.00000 0.02434 0.04559 = 0.02364 0.00774 0.00453 0.00189 O1 5 0.888468 0.760065 0.589400 11.00000 0.02161 0.02236 = 0.04118 0.00877 0.01125 0.00446 O2 5 0.328287 0.627068 0.619272 11.00000 0.01362 0.03116 = 0.02192 -0.00714 -0.00048 0.00078 N1 4 1.066834 0.515277 0.557692 11.00000 0.02517 0.02535 = 0.02900 0.00128 0.00342 0.00472 N2 4 0.306629 0.405815 0.487589 11.00000 0.02678 0.02323 = 0.02616 -0.00296 -0.00493 0.00318 C1 1 1.081238 0.627959 0.560035 11.00000 0.01728 0.02759 = 0.02704 0.00275 0.00124 0.00071 C2 1 1.024038 0.710994 0.571792 11.00000 0.02020 0.01999 = 0.02103 0.00101 -0.00101 -0.00166 C3 1 0.944508 0.676388 0.581450 11.00000 0.01796 0.02144 = 0.02156 0.00300 0.00117 0.00251 C4 1 0.928709 0.557159 0.577947 11.00000 0.01904 0.02356 = 0.02588 0.00345 0.00057 -0.00354 C5 1 0.992107 0.482764 0.566996 11.00000 0.03086 0.01819 = 0.02389 0.00063 -0.00008 -0.00047 C6 1 0.824430 0.742701 0.626165 11.00000 0.01717 0.01936 = 0.03046 0.00115 0.00532 -0.00071 C7 1 0.835433 0.689326 0.675702 11.00000 0.01598 0.02781 = 0.03335 0.00375 -0.00200 0.00295 AFIX 43 H7 2 0.886927 0.658655 0.685510 11.00000 -1.20000 AFIX 0 C8 1 0.769924 0.681118 0.711072 11.00000 0.01929 0.02658 = 0.02390 0.00270 -0.00335 0.00153 AFIX 43 H8 2 0.776818 0.644452 0.745250 11.00000 -1.20000 AFIX 0 C9 1 0.694406 0.726109 0.696858 11.00000 0.01634 0.01891 = 0.02189 -0.00215 -0.00073 -0.00097 C10 1 0.685945 0.780476 0.646582 11.00000 0.01660 0.02112 = 0.02635 0.00220 -0.00179 0.00232 AFIX 43 H10 2 0.634824 0.812119 0.636572 11.00000 -1.20000 AFIX 0 C11 1 0.750580 0.789127 0.611082 11.00000 0.02158 0.02141 = 0.02577 0.00541 0.00148 0.00123 AFIX 43 H11 2 0.744239 0.826314 0.576978 11.00000 -1.20000 AFIX 0 C12 1 0.620242 0.726070 0.734838 11.00000 0.01655 0.02150 = 0.01851 -0.00172 -0.00184 0.00154 C13 1 0.625133 0.629742 0.778786 11.00000 0.01909 0.03227 = 0.01961 0.00187 -0.00117 0.00137 C14 1 0.620380 0.845331 0.764347 11.00000 0.02143 0.02894 = 0.02642 -0.00737 -0.00360 0.00089 C15 1 0.541112 0.705175 0.703137 11.00000 0.01529 0.02044 = 0.01620 0.00103 -0.00006 -0.00072 C16 1 0.471186 0.772608 0.708461 11.00000 0.01945 0.02081 = 0.01927 -0.00315 0.00080 0.00176 AFIX 43 H16 2 0.471057 0.837176 0.732561 11.00000 -1.20000 AFIX 0 C17 1 0.401770 0.746711 0.679042 11.00000 0.01552 0.02459 = 0.02158 -0.00087 0.00229 0.00396 AFIX 43 H17 2 0.354754 0.794147 0.682275 11.00000 -1.20000 AFIX 0 C18 1 0.401829 0.651094 0.644980 11.00000 0.01367 0.02373 = 0.01676 0.00192 0.00019 -0.00160 C19 1 0.469884 0.581559 0.639345 11.00000 0.01892 0.01892 = 0.01798 -0.00162 0.00087 -0.00074 AFIX 43 H19 2 0.469016 0.515407 0.616196 11.00000 -1.20000 AFIX 0 C20 1 0.539387 0.610056 0.668057 11.00000 0.01608 0.01956 = 0.01998 0.00075 0.00183 0.00312 AFIX 43 H20 2 0.586778 0.563811 0.663728 11.00000 -1.20000 AFIX 0 C21 1 0.326295 0.552976 0.576354 11.00000 0.01519 0.02180 = 0.01968 -0.00039 -0.00374 0.00367 C22 1 0.268991 0.463835 0.576404 11.00000 0.01532 0.02541 = 0.02308 0.00460 -0.00097 0.00145 C23 1 0.261339 0.395470 0.530952 11.00000 0.01935 0.02059 = 0.03155 0.00143 -0.00694 -0.00062 C24 1 0.361379 0.488397 0.488042 11.00000 0.02402 0.02499 = 0.01965 0.00074 -0.00002 0.00520 C25 1 0.373432 0.565705 0.530068 11.00000 0.01684 0.01898 = 0.02265 0.00159 -0.00146 0.00122 HKLF 4 REM pfpetherabs_a.res in Pbca REM R1 = 0.0300 for 4485 Fo > 4sig(Fo) and 0.0365 for all 5176 data REM 389 parameters refined using 0 restraints END WGHT 0.0361 2.0816 REM Highest difference peak 0.332, deepest hole -0.248, 1-sigma level 0.042 Q1 1 0.5799 0.7193 0.7174 11.00000 0.05 0.33 Q2 1 0.6558 0.7214 0.7181 11.00000 0.05 0.32 Q3 1 0.6188 0.7821 0.7477 11.00000 0.05 0.32 Q4 1 0.6233 0.6826 0.7568 11.00000 0.05 0.31 Q5 1 0.2814 0.4126 0.5599 11.00000 0.05 0.27 ; _shelx_res_checksum 65873 _shelx_hkl_file ; 0 0 2 173.15 6.23 0 0 2 181.87 6.30 0 0 -3 -0.07 0.09 0 0 3 2.10 0.36 0 0 3 0.06 0.16 0 0 -3 -0.05 0.11 0 0 -3 0.13 0.13 0 0 -3 1.75 0.33 0 0 4 1103.79 37.10 0 0 -4 1103.54 37.07 0 0 -4 1209.98 37.13 0 0 4 1139.22 37.25 0 0 -4 1220.29 37.27 0 0 -4 1123.53 36.87 0 0 -4 1113.69 36.99 0 0 -5 0.09 0.26 0 0 -5 0.36 0.29 0 0 -5 0.50 0.31 0 0 5 0.94 0.38 0 0 -5 0.10 0.32 0 0 -5 0.32 0.35 0 0 5 -0.11 0.29 0 0 6 6152.14 208.03 0 0 -6 6573.58 207.86 0 0 -6 6617.07 207.91 0 0 6 6588.02 207.98 0 0 6 6529.25 208.11 0 0 -6 6506.87 207.52 0 0 -6 6730.37 207.77 0 0 6 6419.70 207.81 0 0 -6 6455.21 207.03 0 0 -7 0.56 0.24 0 0 -7 0.13 0.48 0 0 7 0.15 0.47 0 0 -7 0.28 0.45 0 0 -7 0.59 0.42 0 0 -7 -0.25 0.34 0 0 7 0.67 0.46 0 0 7 -0.16 0.39 0 0 8 9453.23 306.68 0 0 8 9032.04 306.57 0 0 -8 9529.02 306.40 0 0 -8 9442.01 306.41 0 0 8 9999.00 306.63 0 0 -8 9462.05 306.28 0 0 -8 9459.87 305.93 0 0 8 9774.97 306.41 0 0 -8 9804.40 305.31 0 0 9 1.79 0.85 0 0 -9 0.52 0.30 0 0 9 1.15 0.70 0 0 -9 0.34 0.61 0 0 9 0.42 0.40 0 0 -9 0.48 0.52 0 0 -9 1.11 0.55 0 0 -9 0.18 0.55 0 0 9 0.34 0.61 0 0 9 0.21 0.68 0 0 10 11.23 1.50 0 0 -10 10.95 0.82 0 0 10 13.53 1.53 0 0 -10 12.14 1.44 0 0 10 11.20 1.06 0 0 -10 12.19 1.36 0 0 -10 11.87 1.45 0 0 -10 10.96 1.16 0 0 10 10.42 1.33 0 0 10 13.83 1.65 0 0 11 -0.24 0.65 0 0 -11 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561.00 21.94 2 0 12 648.69 20.48 -2 0 12 622.38 22.11 2 0 -12 621.77 20.92 -2 0 12 629.45 20.26 -2 0 13 -0.26 0.76 -2 0 13 0.94 0.84 2 0 13 -0.62 0.79 2 0 13 -0.57 0.80 -2 0 13 0.29 0.81 2 0 -13 -1.38 0.77 -2 0 -13 0.10 0.38 2 0 13 -0.28 0.81 2 0 -13 0.48 0.73 2 0 13 0.30 0.69 2 0 13 0.55 0.48 -2 0 13 0.28 0.82 -2 0 -13 0.36 0.54 -2 0 -13 -0.26 0.73 2 0 -13 0.82 0.89 2 0 -13 0.56 0.52 2 0 13 0.42 0.35 -2 0 13 0.53 0.94 -2 0 13 -0.07 0.34 -2 0 -13 -0.12 0.45 -2 0 14 1751.53 59.17 2 0 14 1854.63 59.30 -2 0 14 1768.59 58.95 2 0 14 1790.15 58.94 2 0 -14 1807.18 58.47 2 0 14 1685.92 58.77 2 0 -14 1671.42 58.14 -2 0 -14 1766.98 56.75 -2 0 -14 1798.25 58.62 -2 0 14 1700.24 58.70 -2 0 14 1802.81 58.65 2 0 14 1739.79 59.05 2 0 14 1743.28 57.20 -2 0 -14 1798.80 58.15 -2 0 -14 1630.96 57.60 2 0 -14 1775.21 58.73 -2 0 14 1623.00 58.44 2 0 -14 1835.55 57.32 -2 0 -14 1748.68 56.94 -2 0 15 -0.36 1.48 -2 0 15 -0.58 1.06 2 0 15 -0.36 1.34 -2 0 15 -0.33 1.54 2 0 15 -0.33 1.52 2 0 -15 -0.26 0.86 -2 0 -15 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6.72 -4 -4 5 166.29 6.97 -4 4 -5 152.60 5.98 -4 -4 -5 165.46 6.03 4 4 -5 163.57 7.41 -4 -4 -5 151.52 7.00 -4 -4 5 149.14 7.09 4 4 -5 163.48 7.50 -4 4 -5 150.78 7.10 -4 -4 5 165.67 7.32 4 -4 5 143.25 6.69 -4 -4 -5 165.75 6.89 -4 4 5 153.39 5.89 -4 -4 5 156.33 7.05 -4 -4 5 154.61 6.62 -4 -4 -5 156.37 6.92 4 -4 -5 179.34 7.30 -4 -4 5 157.98 6.46 -4 -4 5 156.42 6.13 -4 4 5 177.10 7.35 -4 4 5 166.20 7.52 4 -4 -5 161.16 7.41 -4 -4 -5 150.17 6.92 4 4 -6 111.44 5.87 -4 4 -6 110.25 5.86 -4 -4 6 126.87 6.14 4 -4 6 120.82 6.02 4 -4 -6 119.66 5.94 -4 4 -6 98.14 5.81 -4 -4 -6 114.27 5.85 4 4 -6 117.61 6.11 4 -4 -6 127.93 5.48 -4 4 6 113.96 4.92 -4 -4 -6 130.05 6.34 -4 -4 6 113.32 5.51 4 4 -6 119.75 4.51 4 4 6 108.42 6.28 -4 4 6 116.42 5.48 4 4 -6 116.18 5.17 4 -4 6 110.64 5.69 -4 -4 6 118.91 5.23 -4 -4 -6 118.27 4.90 -4 -4 -6 116.76 6.15 -4 -4 -6 129.28 5.72 4 4 -6 135.45 6.30 -4 4 -6 113.46 5.72 -4 4 -6 119.26 4.65 -4 -4 -6 123.18 5.91 -4 -4 6 116.77 5.86 -4 -4 -6 128.93 5.61 4 4 -6 119.76 6.24 -4 4 -6 115.20 5.91 -4 -4 6 124.95 6.06 -4 4 6 118.53 4.49 4 -4 6 121.24 5.57 -4 -4 6 120.44 5.38 -4 -4 -6 119.29 5.68 -4 -4 6 109.96 5.25 -4 -4 6 116.62 5.77 4 -4 -6 110.34 5.95 -4 -4 6 115.95 5.11 -4 -4 -6 126.79 5.83 -4 4 6 112.66 5.77 4 -4 -6 99.14 5.53 4 4 6 123.92 4.35 -4 4 6 130.00 6.34 -4 -4 6 129.77 4.81 -4 -4 7 125.26 6.40 4 -4 7 140.85 6.61 4 4 -7 127.86 6.39 -4 4 -7 133.05 6.50 4 4 7 136.89 6.75 4 4 -7 127.15 6.56 -4 4 -7 122.44 6.57 -4 -4 -7 130.71 6.40 4 -4 -7 133.03 6.43 -4 4 7 118.53 6.50 4 -4 -7 133.86 5.88 -4 4 7 131.90 5.29 -4 -4 -7 141.40 6.82 -4 -4 7 136.71 6.14 4 4 -7 130.13 5.04 -4 4 7 124.08 5.95 4 4 7 142.85 7.14 -4 -4 -7 136.53 6.10 4 -4 7 125.53 6.21 -4 -4 -7 125.27 6.62 -4 -4 -7 121.14 5.32 -4 -4 7 123.76 5.67 4 4 -7 126.04 5.44 -4 -4 7 121.55 6.25 4 4 -7 127.22 6.48 -4 4 -7 134.88 4.91 -4 4 -7 125.19 6.21 -4 -4 -7 134.00 6.31 4 -4 7 129.31 5.91 4 4 -7 128.57 6.63 -4 -4 7 122.34 6.34 -4 4 -7 134.19 6.48 -4 -4 -7 134.73 5.95 4 -4 -7 136.32 6.59 -4 -4 7 133.49 6.31 -4 -4 7 126.70 5.65 -4 4 7 129.77 4.64 -4 -4 -7 131.45 6.14 -4 -4 7 134.05 5.95 4 4 7 133.67 4.91 -4 -4 -7 129.50 6.19 -4 -4 7 130.16 5.48 -4 4 7 126.56 6.25 4 -4 -7 128.55 6.19 -4 -4 7 129.34 4.98 -4 4 7 138.07 6.70 -4 -4 8 41.25 3.12 4 -4 8 29.35 2.73 4 4 -8 33.14 2.87 -4 4 -8 36.96 2.98 4 -4 -8 34.47 2.90 4 4 -8 34.06 3.02 -4 -4 -8 37.67 2.99 -4 4 8 39.94 3.26 -4 4 -8 35.45 3.06 4 4 8 31.73 2.94 -4 4 8 38.83 2.16 -4 -4 -8 28.82 2.85 -4 -4 8 39.88 2.83 4 4 -8 41.24 2.14 -4 4 8 37.03 2.75 4 4 -8 34.18 2.84 4 4 8 38.70 3.36 4 4 -8 33.17 2.12 -4 -4 -8 34.52 2.62 -4 4 8 36.60 2.04 -4 -4 -8 36.07 2.31 -4 -4 8 37.34 2.57 -4 -4 -8 31.51 2.97 4 -4 8 35.55 2.83 4 -4 8 36.10 2.18 4 4 -8 42.32 3.20 -4 4 -8 31.70 2.69 -4 -4 -8 42.19 3.01 -4 4 -8 33.30 1.64 -4 -4 8 32.54 2.79 -4 4 -8 36.34 2.98 4 -4 8 34.75 2.56 4 4 -8 29.26 2.92 -4 4 -8 38.14 2.70 -4 -4 -8 39.95 2.62 -4 -4 8 36.54 3.02 -4 -4 -8 31.20 2.61 -4 -4 8 39.62 2.95 -4 -4 8 40.20 2.47 4 -4 -8 35.82 2.99 4 4 8 32.91 1.88 -4 -4 8 39.77 2.76 -4 4 8 41.74 3.01 -4 -4 -8 35.99 2.76 4 -4 -8 36.04 2.79 -4 -4 8 36.82 2.17 -4 4 8 41.29 3.21 -4 4 8 38.25 2.85 -4 -4 8 38.86 1.82 4 -4 -9 146.48 6.91 4 4 -9 128.76 6.71 -4 4 -9 131.70 6.77 -4 -4 -9 139.81 6.77 4 -4 -9 140.34 6.61 -4 4 -9 133.61 7.01 -4 4 9 140.85 7.14 4 4 9 134.74 7.04 4 4 -9 150.47 7.29 -4 -4 -9 129.11 6.89 4 4 -9 136.76 6.66 -4 -4 9 126.13 6.31 4 4 -9 137.14 5.53 -4 4 9 142.05 6.55 4 4 9 130.35 7.24 -4 4 9 136.93 5.46 4 4 -9 134.83 5.51 -4 4 -9 129.27 6.41 -4 -4 9 137.33 6.24 -4 -4 -9 124.28 6.88 -4 -4 -9 132.53 6.22 -4 4 9 134.24 5.50 -4 -4 -9 128.84 5.77 -4 -4 9 140.54 6.71 4 -4 9 136.94 5.48 4 4 -9 137.99 6.84 -4 4 -9 130.86 6.55 -4 -4 -9 138.25 6.53 4 4 -9 140.75 7.14 -4 4 -9 127.64 6.69 4 -4 9 130.00 6.17 -4 -4 9 141.83 6.88 -4 4 -9 133.28 6.23 -4 -4 9 139.36 6.38 4 -4 -9 136.54 6.82 -4 -4 9 125.07 5.65 4 4 9 135.89 5.37 -4 -4 9 120.63 6.41 -4 -4 -9 124.17 6.20 4 -4 -9 133.46 6.42 -4 -4 -9 128.79 6.36 -4 4 9 139.21 6.94 -4 -4 9 134.91 5.46 -4 4 9 132.84 6.40 4 -4 -10 27.57 2.71 4 -4 -10 26.85 2.51 4 4 -10 25.57 2.63 -4 4 -10 30.09 2.81 -4 -4 -10 26.88 2.67 4 4 -10 23.56 2.64 -4 4 -10 33.48 3.06 4 -4 -10 30.79 2.88 -4 -4 -10 25.06 2.67 -4 4 10 34.03 3.12 4 4 10 25.73 2.78 4 4 -10 27.96 1.94 -4 4 10 30.08 2.63 -4 -4 -10 28.76 2.88 4 4 10 27.37 3.01 -4 4 10 25.61 1.79 4 4 -10 28.53 2.63 -4 4 -10 25.51 2.43 -4 -4 10 28.30 2.44 -4 -4 -10 26.17 2.77 -4 4 10 28.67 1.98 4 4 -10 27.22 1.82 -4 -4 -10 25.55 2.29 -4 -4 -10 22.74 2.04 -4 -4 10 29.86 2.70 4 4 10 26.02 2.23 4 4 -10 27.66 2.68 4 -4 10 32.42 1.90 -4 4 -10 29.26 2.67 -4 -4 -10 26.65 2.49 4 -4 10 22.08 2.13 4 4 -10 25.63 2.77 -4 4 -10 26.19 2.59 -4 4 -10 27.15 2.30 -4 -4 10 24.15 2.56 4 -4 -10 26.68 2.66 4 4 10 30.05 1.92 -4 -4 -10 21.99 2.18 -4 -4 10 32.84 2.76 -4 -4 10 30.36 2.04 -4 -4 10 27.02 2.41 -4 4 10 32.09 2.58 -4 4 10 26.92 2.72 -4 -4 -10 25.61 2.38 4 4 10 28.53 2.58 -4 -4 10 28.04 1.75 4 -4 -10 29.46 2.55 4 -4 -11 8.57 1.48 -4 4 -11 8.13 1.59 4 4 -11 10.01 1.80 4 4 11 7.34 1.63 -4 -4 -11 8.90 1.65 4 -4 -11 6.17 1.55 4 -4 -11 9.75 1.74 4 4 -11 10.24 1.90 -4 -4 -11 8.82 1.66 -4 4 -11 10.68 1.86 -4 4 11 7.50 1.66 4 -4 -11 5.42 1.01 4 4 -11 8.60 1.54 -4 4 11 8.51 1.55 4 4 11 11.10 2.02 -4 4 11 8.95 1.06 4 4 -11 10.07 1.23 -4 -4 -11 9.79 1.47 4 4 -11 10.77 1.06 -4 4 11 8.73 1.17 4 4 11 5.85 1.43 -4 4 -11 10.17 1.59 4 -4 11 9.31 1.02 4 4 11 10.05 1.47 -4 -4 11 10.33 1.73 -4 4 -11 10.23 1.65 -4 -4 -11 10.42 1.69 4 4 11 11.18 1.71 4 4 -11 6.66 1.41 -4 -4 11 6.49 1.30 -4 -4 -11 12.50 1.48 -4 -4 11 9.10 1.62 4 4 -11 8.30 1.66 -4 4 -11 7.40 1.61 4 -4 11 9.68 1.41 -4 4 -11 10.16 1.41 4 4 11 6.85 1.01 -4 -4 11 9.88 1.16 -4 -4 11 11.33 1.67 -4 -4 -11 10.23 1.45 -4 -4 11 5.52 1.36 4 -4 -11 6.60 1.47 -4 -4 -11 9.83 1.57 4 -4 -11 9.21 1.48 -4 -4 11 7.76 0.87 -4 4 11 10.70 1.54 -4 4 11 8.07 1.55 -4 4 -12 788.75 28.90 4 -4 -12 773.49 28.34 4 4 -12 776.48 28.86 4 -4 -12 756.12 28.67 -4 -4 -12 810.24 28.79 4 4 -12 826.13 29.49 4 -4 -12 759.61 28.98 -4 -4 -12 812.81 29.12 -4 4 12 791.56 29.39 4 4 12 799.97 29.39 4 4 -12 829.50 27.43 -4 4 12 791.29 27.01 -4 4 12 802.88 28.67 4 4 12 803.12 29.80 4 4 -12 860.33 29.00 4 -4 -12 823.42 27.42 4 4 -12 779.04 26.64 -4 4 -12 808.84 28.46 -4 -4 12 797.56 28.36 4 4 12 798.05 28.94 -4 4 12 815.64 27.51 -4 -4 -12 806.78 27.98 -4 -4 -12 799.51 27.71 -4 -4 12 840.11 28.93 4 4 12 808.63 28.21 4 4 -12 781.92 28.75 -4 -4 -12 806.15 28.33 -4 4 -12 840.19 28.75 4 4 -12 761.45 29.06 -4 4 -12 755.98 28.63 4 -4 12 771.81 27.69 -4 -4 12 834.44 28.95 -4 4 -12 823.98 28.01 -4 -4 12 831.88 28.51 4 -4 -12 786.34 28.77 4 4 12 789.37 27.24 -4 -4 -12 801.12 28.06 -4 -4 12 797.89 28.59 -4 -4 -12 813.66 28.22 4 4 12 813.07 28.64 -4 4 12 824.05 28.16 4 -4 -12 821.73 28.27 -4 4 12 818.19 28.96 -4 4 -13 14.24 2.13 4 -4 -13 8.35 1.74 -4 -4 -13 10.56 1.85 4 4 -13 13.79 2.11 4 -4 -13 10.66 1.70 4 -4 -13 17.12 2.41 -4 -4 -13 10.50 1.90 -4 4 13 15.49 2.37 4 4 13 13.11 2.27 4 4 -13 11.23 1.86 -4 4 13 15.93 2.17 4 4 13 11.35 2.19 4 -4 -13 14.73 1.62 4 4 -13 16.75 1.73 -4 -4 -13 14.33 1.80 4 4 13 13.14 2.12 -4 4 -13 12.02 1.84 -4 4 -13 17.52 2.20 -4 -4 -13 14.14 1.90 4 4 13 15.22 1.88 4 4 13 12.50 1.86 -4 -4 13 11.46 1.98 4 4 -13 12.81 2.00 -4 4 -13 10.52 1.84 -4 -4 13 11.88 2.01 4 4 -13 12.14 2.13 -4 -4 -13 16.01 1.77 -4 -4 13 15.79 2.03 4 -4 13 9.89 1.50 -4 4 -13 13.20 1.71 -4 -4 13 13.75 1.96 -4 -4 -13 12.78 1.71 -4 -4 13 13.68 2.03 4 -4 -13 15.00 2.08 4 -4 -13 11.56 1.78 -4 4 13 12.10 2.03 -4 -4 -13 11.84 1.75 -4 4 13 14.64 1.82 4 4 -14 26.23 2.94 -4 4 -14 24.54 2.88 4 -4 -14 28.82 2.97 -4 -4 -14 28.83 2.97 4 4 14 36.76 3.58 4 -4 -14 30.62 3.18 -4 -4 -14 30.18 3.16 -4 4 14 25.61 3.14 4 -4 14 30.91 3.08 -4 4 14 21.03 2.64 4 4 14 23.38 3.04 4 -4 -14 31.68 2.41 4 4 -14 28.24 2.93 4 4 -14 24.83 2.28 -4 4 -14 29.79 2.86 -4 -4 -14 28.32 2.52 -4 -4 -14 29.41 2.55 -4 -4 14 27.63 2.81 4 4 14 31.45 3.17 -4 4 14 31.79 3.02 -4 -4 14 31.44 3.11 4 4 14 31.01 2.86 4 4 -14 29.22 2.92 4 -4 -14 27.67 2.76 -4 -4 -14 27.99 2.64 -4 -4 14 30.93 2.90 -4 4 -14 36.53 3.28 4 4 -14 28.14 3.14 -4 -4 14 23.94 2.80 4 -4 14 29.22 2.47 -4 4 -14 30.74 2.62 -4 -4 -14 27.41 2.49 4 -4 -14 32.33 3.07 -4 4 14 32.20 3.18 -4 -4 14 28.79 2.87 -4 -4 -14 26.82 2.56 -4 4 14 30.17 2.62 4 -4 -14 26.46 2.63 4 4 14 28.65 2.81 4 4 -15 25.01 2.89 4 -4 -15 23.37 2.72 -4 -4 -15 17.78 2.50 -4 4 -15 17.04 2.53 4 -4 -15 14.00 2.10 4 -4 -15 16.20 2.53 -4 -4 -15 16.39 2.49 -4 4 15 14.42 2.55 4 4 15 18.23 2.71 4 4 -15 18.35 2.52 -4 4 15 20.50 2.64 4 -4 15 18.26 2.42 4 4 15 17.49 2.84 -4 -4 -15 17.36 2.04 -4 4 -15 19.30 2.37 -4 -4 15 17.02 2.33 4 4 15 16.95 2.47 -4 4 -15 19.67 2.43 -4 -4 -15 20.50 2.31 -4 4 15 22.87 2.58 4 4 15 22.54 2.56 4 4 15 12.25 2.03 4 4 -15 20.42 2.50 -4 -4 15 22.55 2.70 -4 4 -15 22.59 2.64 4 4 -15 18.20 2.62 -4 -4 -15 16.17 2.05 -4 -4 15 20.44 2.55 -4 4 -15 21.73 2.25 -4 -4 15 17.99 2.34 -4 -4 15 15.61 2.29 4 -4 -15 18.15 2.48 -4 -4 -15 22.44 2.23 -4 4 15 14.50 1.98 4 -4 -15 15.21 2.07 -4 -4 -15 18.85 2.20 -4 4 15 19.62 2.60 4 4 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-3 155.78 6.98 7 4 -3 160.05 7.13 -7 4 -3 155.33 7.08 -7 -4 3 159.66 7.02 7 -4 3 154.09 6.97 7 -4 -3 145.30 6.84 -7 -4 -3 158.28 7.00 -7 -4 -3 153.14 6.97 7 -4 -3 159.22 7.02 7 -4 -3 155.54 5.93 -7 -4 -3 156.17 7.57 -7 -4 -3 142.99 6.77 7 4 -3 144.73 7.34 7 4 3 165.48 7.46 -7 -4 -3 158.99 7.19 7 4 -3 154.22 7.10 7 4 -3 157.50 7.76 7 4 3 160.81 6.19 -7 -4 -3 166.46 7.36 -7 -4 3 168.45 7.60 -7 -4 3 161.17 7.39 7 4 -3 161.95 7.65 -7 -4 -3 169.05 7.01 7 4 3 158.71 7.05 7 4 3 144.11 7.28 -7 -4 3 161.07 6.40 -7 -4 -3 161.18 7.50 7 4 -3 160.16 7.27 -7 -4 3 149.15 7.15 -7 4 3 151.97 7.45 7 -4 -3 142.02 7.71 7 4 -4 1918.99 61.99 -7 4 -4 1825.24 61.94 -7 -4 4 1828.42 62.05 -7 -4 4 1902.52 62.17 7 -4 4 1954.20 62.13 7 4 -4 1942.18 62.22 -7 4 -4 1848.54 62.11 7 -4 -4 1817.38 61.87 -7 -4 -4 1846.21 61.93 7 -4 -4 1929.01 61.99 -7 -4 -4 1884.53 61.89 7 -4 -4 1826.25 60.58 -7 -4 -4 1903.19 62.83 7 4 -4 1808.45 62.53 -7 -4 -4 1814.40 61.70 7 -4 4 1885.70 62.93 -7 -4 -4 1915.02 61.43 -7 -4 -4 1844.59 63.19 7 4 4 1860.35 62.41 -7 -4 -4 1892.37 62.14 7 4 -4 1860.13 61.98 7 4 -4 1848.84 62.98 -7 -4 -4 1886.14 62.20 7 4 4 1898.84 60.68 -7 -4 4 1823.79 62.50 7 4 -4 1855.64 62.80 -7 -4 -4 1863.82 61.64 7 4 4 1862.17 61.87 -7 -4 4 1809.71 62.33 -7 -4 4 1913.19 61.30 7 4 4 1912.26 62.57 7 4 -4 1930.73 62.25 -7 -4 -4 1893.69 62.53 -7 -4 4 1918.22 62.26 -7 4 4 1916.90 62.66 7 -4 -4 1868.94 63.29 7 4 -5 537.57 19.57 -7 4 -5 551.28 19.65 -7 -4 5 527.84 19.71 -7 -4 5 557.90 19.71 7 -4 5 541.25 19.61 7 4 -5 551.81 19.79 -7 4 -5 531.57 19.77 7 -4 -5 564.64 19.63 -7 -4 -5 548.22 19.61 7 -4 -5 527.01 19.48 -7 -4 -5 531.24 19.50 -7 -4 -5 545.58 20.34 7 4 5 553.03 19.17 -7 -4 5 539.14 19.64 7 4 -5 531.30 20.13 -7 -4 -5 518.10 19.24 -7 4 5 572.84 19.58 7 4 5 533.92 20.58 7 4 5 529.32 19.92 7 -4 5 527.32 20.31 -7 -4 -5 535.28 19.08 -7 -4 -5 516.69 19.63 -7 -4 -5 518.76 20.65 7 4 -5 533.47 19.45 -7 -4 5 536.92 20.12 -7 -4 -5 539.36 19.67 7 4 -5 530.72 20.45 7 4 5 549.71 18.14 -7 -4 -5 557.95 19.18 7 4 -5 525.76 20.33 -7 -4 5 534.78 20.02 7 -4 5 543.35 19.30 7 4 5 552.06 20.12 7 4 -5 524.20 19.56 -7 -4 -5 554.45 20.10 -7 -4 5 551.03 19.73 -7 -4 5 524.64 19.00 -7 4 5 541.02 20.03 -7 -4 -5 551.91 20.02 7 -4 -5 572.29 20.81 -7 4 5 554.09 20.73 -7 -4 6 76.13 4.24 7 -4 6 63.92 3.97 7 4 -6 63.95 3.95 -7 4 -6 62.98 3.97 -7 -4 6 73.44 4.31 7 4 -6 62.58 4.06 7 -4 -6 65.16 3.98 -7 -4 -6 60.36 3.84 -7 4 -6 62.58 4.04 -7 -4 -6 65.80 4.43 -7 -4 6 61.49 3.90 -7 4 6 67.70 3.82 7 4 6 61.06 4.50 7 4 6 68.81 3.77 7 4 -6 68.22 4.37 7 4 6 73.28 4.30 7 -4 6 65.80 4.46 -7 -4 -6 63.64 3.65 -7 -4 -6 52.19 4.27 -7 -4 -6 70.61 4.12 7 4 -6 62.96 3.77 -7 -4 6 67.86 4.34 7 4 6 63.36 2.74 -7 -4 -6 64.82 3.94 -7 -4 -6 66.30 3.63 7 4 -6 70.73 4.59 7 -4 6 54.69 3.47 -7 -4 -6 56.98 3.43 7 4 -6 68.26 4.55 -7 -4 6 62.62 4.24 7 4 6 61.56 4.13 7 4 -6 69.68 3.96 7 -4 -6 64.26 4.55 -7 -4 -6 53.79 3.91 -7 -4 6 59.33 3.55 -7 -4 6 66.25 3.94 -7 4 6 61.03 4.10 -7 -4 -6 63.50 4.12 -7 4 6 71.26 4.77 7 4 -7 41.72 3.00 -7 4 -7 28.89 2.66 -7 -4 7 28.51 2.74 7 -4 -7 30.73 2.70 -7 -4 -7 34.23 2.75 7 4 -7 31.87 2.84 -7 4 -7 31.13 2.84 -7 -4 -7 33.58 3.14 -7 -4 7 38.31 2.92 7 4 -7 37.94 3.17 7 4 7 37.77 3.49 -7 4 7 36.77 2.62 -7 4 7 31.52 2.15 7 4 7 27.54 2.41 7 4 7 38.00 3.01 7 -4 7 36.05 3.17 -7 -4 -7 37.66 2.71 -7 -4 -7 33.02 3.21 -7 -4 -7 33.57 2.77 7 4 -7 36.20 2.64 -7 -4 -7 24.40 2.41 7 4 7 39.72 1.72 7 4 -7 36.37 3.24 -7 -4 -7 35.84 2.56 -7 -4 -7 32.65 2.38 7 4 -7 34.78 3.19 7 -4 7 27.18 2.31 -7 -4 7 32.93 3.00 7 4 -7 29.16 2.50 -7 -4 -7 35.21 2.98 -7 -4 7 26.22 2.40 7 4 7 31.72 2.87 7 -4 -7 31.45 3.14 -7 -4 -7 33.83 2.90 -7 4 7 35.94 2.96 -7 4 7 34.80 3.31 7 4 -8 4.37 1.21 -7 4 -8 5.80 1.38 -7 -4 8 3.61 1.24 -7 4 8 4.71 1.29 7 4 -8 4.87 1.41 -7 4 -8 7.66 1.51 7 -4 -8 6.59 1.27 -7 -4 -8 7.50 1.38 -7 -4 8 8.28 1.45 -7 -4 -8 6.16 1.59 7 4 -8 5.67 1.40 -7 4 8 5.24 1.13 7 4 8 6.78 1.66 -7 4 8 7.89 1.14 -7 -4 -8 4.83 1.40 7 -4 8 6.93 1.50 7 4 8 10.87 1.76 -7 -4 -8 6.78 1.39 7 4 8 8.03 1.36 -7 -4 -8 6.08 1.22 7 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8.42 -7 -4 -11 180.74 8.44 -7 4 11 170.73 8.61 7 4 11 173.48 8.58 7 4 -11 169.42 8.56 7 4 -11 178.92 8.80 -7 -4 11 189.32 8.34 -7 4 11 167.56 7.64 7 4 11 170.78 9.20 7 4 11 176.01 8.16 7 4 11 164.64 8.12 -7 -4 -11 163.40 7.86 -7 -4 -11 168.22 7.97 -7 -4 -11 170.39 9.16 7 4 -11 162.26 7.24 -7 4 -11 164.03 8.36 7 4 -11 176.02 8.87 -7 -4 -11 165.14 8.08 -7 -4 -11 173.03 7.71 -7 -4 11 181.10 8.73 7 4 -11 173.54 9.06 7 4 -11 190.54 7.50 7 -4 -11 167.22 8.68 -7 -4 11 188.93 8.28 -7 -4 -11 172.00 8.23 -7 -4 11 179.12 8.33 7 4 11 178.10 8.25 -7 -4 -11 154.73 7.85 -7 4 11 175.35 8.17 -7 4 11 181.80 9.04 7 -4 -12 415.58 16.14 -7 -4 -12 390.69 15.97 -7 -4 12 409.73 16.59 -7 4 -12 450.50 16.60 7 4 -12 401.46 16.23 7 -4 -12 394.39 16.60 7 4 -12 396.46 16.58 7 -4 -12 425.84 16.55 -7 -4 -12 389.38 16.27 -7 4 -12 390.62 16.58 -7 4 12 397.24 16.69 7 4 12 418.93 16.74 7 4 -12 413.76 16.77 -7 -4 12 401.44 16.02 -7 4 12 389.53 15.58 7 4 12 444.91 17.78 7 4 12 433.29 16.26 -7 -4 -12 394.10 15.70 -7 -4 -12 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82.42 5.52 7 -4 -14 629.99 22.42 -7 -4 -14 584.00 22.11 7 -4 -14 561.44 22.60 7 4 -14 589.79 22.52 -7 4 -14 588.21 22.55 -7 -4 14 612.05 22.92 7 -4 -14 599.13 22.69 -7 -4 -14 588.27 22.59 -7 4 14 582.66 23.07 7 4 -14 601.95 23.06 7 4 14 583.81 22.94 -7 4 -14 583.36 22.99 -7 -4 14 638.62 22.42 7 4 14 594.08 22.41 7 4 14 541.57 23.43 7 4 -14 591.22 22.84 -7 4 -14 583.27 22.50 7 4 14 585.91 23.00 -7 -4 14 563.88 22.16 -7 -4 -14 603.75 21.78 7 4 -14 622.96 23.23 -7 4 -14 596.66 22.64 -7 -4 -14 571.53 22.04 -7 4 -14 566.94 22.65 -7 -4 14 624.87 23.03 7 4 -14 565.93 23.16 -7 -4 -14 600.67 22.04 7 4 14 606.19 22.04 -7 -4 14 633.22 22.50 -7 -4 14 578.05 22.21 7 -4 -14 587.89 22.96 -7 -4 -14 595.77 21.96 -7 4 14 644.51 23.45 -7 4 14 567.65 21.71 -7 -4 15 414.11 17.02 7 4 -15 431.43 16.91 -7 4 -15 395.66 16.68 7 -4 -15 414.73 16.46 -7 -4 -15 405.21 16.31 7 -4 -15 420.08 16.95 -7 -4 -15 435.03 17.01 -7 4 15 409.57 17.35 7 4 15 394.46 17.20 -7 -4 15 433.84 16.58 7 4 15 415.49 18.02 7 4 15 416.41 16.73 7 4 -15 394.43 17.00 -7 4 -15 428.71 16.87 7 4 15 452.32 17.51 -7 -4 15 402.99 16.47 -7 -4 -15 392.13 15.80 7 4 -15 391.07 17.02 7 -4 -15 422.37 17.03 -7 -4 -15 412.94 16.24 -7 4 -15 413.73 16.85 -7 4 -15 411.00 16.93 7 4 -15 416.02 17.52 -7 -4 15 401.77 16.97 -7 -4 -15 413.57 16.13 -7 -4 15 422.11 16.61 7 -4 -15 359.78 16.70 -7 -4 15 395.40 16.37 7 4 15 421.59 16.18 -7 -4 -15 392.64 15.98 -7 4 15 382.18 15.76 -7 4 15 411.39 17.28 7 -4 -16 58.25 4.54 7 4 -16 70.40 5.13 -7 -4 -16 71.53 4.87 -7 4 -16 65.32 4.97 7 -4 -16 63.59 4.97 -7 -4 -16 68.83 5.10 -7 4 16 60.54 5.17 7 4 16 59.63 5.13 7 4 16 66.34 5.75 7 4 -16 71.42 5.27 7 4 16 72.16 5.08 -7 4 -16 64.48 4.89 -7 -4 16 73.23 5.05 -7 -4 -16 67.10 4.36 7 -4 -16 77.12 5.35 7 4 -16 68.21 5.27 -7 -4 -16 65.61 4.53 7 4 -16 68.30 5.39 7 -4 -16 75.30 5.44 -7 -4 16 74.01 5.06 -7 -4 16 63.98 4.74 -7 -4 -16 57.22 4.30 -7 4 16 59.21 4.16 7 -4 -17 301.78 12.59 -7 -4 -17 294.17 12.47 7 4 -17 285.60 12.74 -7 4 -17 272.23 12.61 7 -4 -17 299.20 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9.22 1.95 -10 -3 4 11.40 1.59 10 3 -5 -0.33 1.13 10 3 5 0.22 0.61 10 3 5 0.34 0.91 -10 -3 -5 -0.30 0.95 -10 -3 5 1.20 1.06 -10 3 5 0.92 0.97 10 -3 5 0.40 1.13 10 -3 5 -0.48 0.96 10 3 -5 -0.30 0.88 10 3 5 -0.98 1.16 -10 -3 -5 -0.24 0.74 10 3 -5 -0.38 1.11 10 3 -5 -0.34 0.84 -10 -3 5 0.93 1.04 10 3 -5 1.39 0.73 10 3 5 1.08 1.13 10 3 -5 2.90 1.17 -10 3 5 1.60 1.21 10 -3 -5 0.81 0.98 -10 -3 5 -0.25 0.72 -10 -3 -6 177.46 8.48 -10 -3 6 169.40 8.32 -10 3 6 174.67 8.41 10 3 6 184.41 8.90 10 3 -6 181.90 9.19 10 -3 6 191.28 9.31 10 -3 6 186.31 8.25 -10 -3 -6 189.87 9.45 10 3 -6 186.48 8.49 10 3 6 171.74 8.58 10 3 -6 185.87 9.10 10 3 -6 185.83 8.83 -10 -3 -6 178.27 7.93 -10 -3 6 186.14 8.71 10 3 -6 167.27 8.69 10 3 -6 178.42 8.01 10 3 6 178.72 8.84 10 3 -6 193.87 8.74 -10 -3 6 182.24 8.19 10 -3 -6 181.57 9.22 -10 3 6 195.40 8.73 -10 3 6 175.37 9.21 -10 -3 -7 74.47 4.75 -10 3 7 71.41 4.56 10 3 7 67.24 4.85 10 3 -7 75.98 5.25 10 -3 7 70.76 5.14 10 -3 7 74.61 4.54 -10 -3 -7 53.44 4.73 10 3 -7 67.99 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12.42 3.00 10 3 -25 13.41 3.07 -10 -3 25 11.89 2.75 -10 3 25 6.70 2.39 10 -3 -25 13.35 3.17 10 3 -25 6.14 2.55 10 -3 -25 6.76 2.41 10 3 25 10.25 2.95 10 3 -25 5.75 2.45 -10 -3 26 2.45 2.12 -10 3 26 3.74 2.10 10 -3 -26 2.71 1.99 10 3 -26 7.66 2.72 10 3 -26 5.55 2.51 10 -3 26 6.35 2.42 10 3 26 8.11 2.80 10 3 -26 9.11 2.85 -10 -4 0 84.52 5.24 -10 -4 0 91.99 5.23 10 4 0 89.14 4.65 10 4 0 99.08 5.60 -10 -4 0 94.09 5.43 10 4 0 97.02 5.77 10 4 0 89.15 4.90 10 4 0 99.87 5.40 -10 -4 0 80.95 4.81 10 4 0 86.75 5.47 10 -4 0 91.09 6.18 -10 -4 -1 342.38 13.88 -10 -4 1 333.42 13.71 -10 -4 1 340.01 13.57 -10 -4 -1 315.86 13.37 10 4 -1 343.31 12.84 10 4 1 343.55 12.98 10 4 -1 348.80 13.96 10 4 1 341.95 13.93 -10 -4 1 342.14 13.88 10 4 1 358.49 14.27 10 4 -1 341.55 14.27 10 4 1 331.30 13.06 10 4 -1 340.21 13.32 -10 -4 -1 334.41 13.71 -10 -4 1 334.59 13.39 10 4 -1 334.69 13.75 -10 -4 -1 349.36 13.24 10 4 1 354.82 13.61 10 4 1 336.42 14.13 10 4 -1 327.61 13.99 10 -4 -1 328.99 14.85 10 -4 1 342.64 14.96 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121.66 6.46 10 4 -4 132.74 6.93 10 4 4 125.31 5.97 10 4 -4 131.08 5.70 10 4 4 128.25 6.90 10 4 -4 121.38 6.60 10 -4 -4 107.29 6.92 -10 4 4 114.98 6.62 -10 -4 -5 7.56 1.64 -10 -4 -5 6.92 1.57 -10 4 5 8.00 1.65 10 4 5 6.61 1.61 10 -4 5 8.87 1.95 -10 -4 -5 5.84 1.64 10 4 -5 5.60 1.37 -10 -4 -5 6.38 1.42 10 4 -5 5.12 1.36 10 4 -5 7.72 1.76 10 4 -5 3.75 1.31 -10 -4 5 7.45 1.59 10 4 5 5.93 1.52 10 4 -5 3.94 1.24 -10 4 5 6.33 1.55 10 -4 -5 6.13 1.82 -10 -4 6 96.97 5.84 -10 -4 -6 94.23 5.82 10 4 6 96.16 6.16 -10 4 6 110.59 5.86 10 4 -6 99.53 6.28 -10 -4 -6 95.13 5.51 10 -4 6 96.26 6.32 -10 -4 -6 101.07 6.57 10 4 -6 113.77 5.93 10 4 6 100.88 5.96 10 4 -6 103.49 6.40 -10 -4 -6 108.55 5.61 -10 -4 6 106.15 6.02 10 4 -6 92.86 6.04 10 4 6 97.38 6.02 10 4 -6 108.24 5.92 10 -4 -6 98.09 6.39 -10 4 6 95.22 5.84 -10 -4 7 475.00 18.69 -10 -4 -7 467.12 18.72 -10 4 7 486.63 18.28 10 4 -7 465.81 19.26 10 4 7 475.61 19.26 10 4 7 477.95 18.76 10 4 -7 491.70 18.35 10 -4 7 497.49 19.51 -10 -4 -7 473.37 19.68 10 4 -7 466.75 19.24 -10 -4 -7 473.98 17.94 -10 -4 7 476.50 18.72 10 4 -7 501.02 19.38 10 4 7 487.43 18.98 10 4 -7 480.19 18.38 10 -4 -7 459.99 19.38 -10 4 7 509.63 18.83 -10 4 7 480.07 19.53 -10 -4 8 661.54 25.58 -10 -4 -8 716.21 25.87 10 4 8 717.00 25.14 -10 -4 8 679.45 25.24 -10 4 8 753.18 25.27 10 4 -8 703.50 26.37 10 4 8 683.72 26.28 10 4 8 672.74 25.54 -10 -4 -8 687.62 24.96 10 -4 8 666.73 26.25 -10 -4 -8 681.47 26.72 10 4 -8 709.83 25.12 10 4 -8 658.26 26.18 -10 -4 8 679.66 25.63 10 4 -8 711.74 26.36 10 4 8 675.11 25.70 10 -4 -8 695.86 26.39 10 4 -8 699.80 25.18 -10 -4 -8 688.28 25.47 -10 4 8 679.61 26.44 -10 4 8 707.83 25.58 -10 -4 9 75.63 5.22 10 -4 -9 82.28 5.81 -10 -4 -9 72.50 5.12 -10 -4 9 82.87 5.06 10 4 9 74.21 4.78 -10 4 9 85.87 4.87 10 4 9 76.67 5.56 10 4 -9 77.56 5.56 10 4 9 72.25 5.02 -10 -4 -9 67.97 4.61 10 -4 9 74.41 5.44 -10 -4 -9 79.74 5.89 10 4 -9 84.99 4.87 10 4 -9 73.54 5.44 -10 -4 9 80.64 5.36 10 4 -9 70.50 5.34 10 4 9 75.24 5.18 10 4 -9 71.90 4.61 10 -4 -9 72.62 5.45 -10 -4 -9 71.66 4.91 -10 4 9 61.47 4.60 -10 4 9 68.06 5.43 -10 -4 10 1.18 1.28 10 -4 -10 1.88 1.38 -10 -4 10 3.01 1.22 10 4 10 0.95 1.28 10 4 -10 3.63 1.57 10 -4 10 1.38 1.29 10 4 10 4.43 1.70 -10 -4 -10 0.31 1.11 10 4 10 3.60 1.48 10 4 -10 3.52 1.22 -10 -4 -10 3.59 1.51 -10 -4 -10 0.69 1.19 10 4 -10 2.78 1.51 10 4 -10 3.22 1.63 -10 -4 10 3.18 1.48 10 -4 -10 0.92 1.24 10 4 10 2.30 1.36 10 4 -10 2.65 1.27 -10 4 10 4.45 1.50 -10 4 10 2.35 1.66 10 -4 -11 141.20 8.15 -10 -4 11 138.72 7.73 -10 -4 11 142.16 7.36 10 4 11 151.10 8.49 10 4 -11 128.73 7.83 10 4 11 150.05 7.51 10 4 11 144.98 7.57 -10 -4 -11 132.48 7.08 10 -4 11 122.89 7.75 -10 -4 -11 128.54 8.21 10 4 -11 135.67 6.83 -10 4 -11 128.98 7.58 10 4 -11 137.67 8.11 10 4 -11 128.36 7.92 -10 -4 11 143.30 7.87 10 4 11 127.74 7.35 10 4 -11 143.26 6.94 10 -4 -11 124.04 7.81 -10 4 11 133.67 7.14 -10 -4 -11 148.27 7.51 10 -4 -12 77.17 5.81 -10 -4 12 85.96 5.82 10 4 12 91.20 5.63 10 4 12 80.38 6.13 10 4 -12 86.82 6.08 10 4 12 81.27 5.45 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23.74 2.98 -10 -5 -4 21.95 3.05 -10 -5 4 25.28 2.89 10 5 -4 18.64 2.67 -10 -5 -4 20.87 2.42 10 5 -4 16.98 2.47 -10 -5 4 22.33 2.54 10 5 4 19.91 2.21 10 5 4 24.95 2.80 10 5 -4 19.36 2.48 -10 -5 -4 21.12 2.66 -10 5 4 22.99 2.77 10 -5 -4 18.90 2.88 -10 -5 5 0.32 1.10 -10 5 5 1.23 1.12 10 5 -5 1.67 1.36 -10 -5 -5 0.77 0.98 -10 -5 -5 2.72 1.08 10 5 -5 1.62 1.05 10 5 5 2.60 1.51 10 -5 5 2.22 1.25 -10 -5 -5 3.40 1.48 10 5 -5 3.09 1.34 -10 -5 -5 2.49 1.16 10 5 -5 3.28 1.29 -10 -5 5 1.73 1.23 10 5 5 1.94 1.22 10 5 -5 1.36 1.07 -10 -5 -5 0.37 1.10 -10 5 5 1.94 1.26 10 -5 -5 0.95 1.22 -10 -5 6 8.00 1.77 -10 -5 -6 6.24 1.72 -10 -5 6 6.89 1.60 -10 5 6 9.03 1.73 10 5 -6 7.24 1.84 10 5 -6 5.42 1.46 10 5 6 3.76 1.45 -10 -5 -6 8.91 2.14 10 -5 6 9.82 2.25 10 5 -6 9.48 2.12 -10 -5 -6 4.67 1.50 -10 -5 -6 6.46 1.64 10 5 -6 9.37 1.97 -10 -5 6 6.09 1.63 10 5 6 8.60 1.84 10 5 -6 7.67 1.66 -10 -5 -6 6.78 1.66 10 -5 -6 5.21 1.69 -10 5 6 6.17 1.67 -10 -5 7 69.92 4.74 -10 -5 -7 67.58 4.90 -10 -5 7 61.17 4.40 10 5 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10 -5 -9 141.49 8.12 -10 -5 -9 127.11 7.30 -10 5 9 154.47 7.77 -10 -5 -9 124.71 7.20 -10 -5 10 41.67 3.83 10 -5 -10 40.34 4.06 10 5 10 28.65 3.73 -10 -5 -10 41.36 3.88 10 5 10 32.68 3.12 -10 -5 10 35.44 3.36 10 5 -10 31.70 3.68 10 5 10 39.82 3.71 10 -5 10 40.94 4.07 10 5 -10 40.91 3.33 -10 -5 -10 33.03 3.96 10 5 -10 41.71 4.17 -10 -5 -10 30.74 3.30 -10 -5 10 36.03 3.66 10 5 -10 34.83 3.83 10 5 10 29.78 3.36 10 5 -10 42.05 3.36 10 -5 -10 39.05 4.09 -10 5 10 32.95 3.45 -10 -5 11 6.53 1.94 10 -5 -11 0.49 1.26 10 5 -11 4.79 1.91 10 5 11 4.78 2.07 10 -5 11 2.42 1.76 10 5 11 3.23 1.47 10 5 11 3.29 1.20 -10 -5 -11 1.67 1.50 10 5 -11 5.02 1.87 -10 -5 -11 4.85 1.61 10 5 -11 1.52 1.75 10 5 11 2.84 1.51 -10 -5 11 2.79 1.59 10 -5 -11 2.47 1.61 -10 5 11 5.35 1.62 10 -5 -12 138.03 8.22 10 5 12 137.90 7.32 10 5 12 132.90 8.49 10 5 -12 149.80 8.50 10 5 12 139.70 7.77 10 -5 12 125.54 7.97 -10 -5 -12 134.51 8.58 10 5 -12 138.88 8.37 10 5 -12 149.39 8.65 10 -5 -12 132.79 8.20 -10 -5 12 133.32 7.60 10 5 12 143.89 7.78 -10 5 12 134.68 7.50 10 -5 -13 81.56 5.97 10 5 13 70.88 6.06 10 5 -13 75.10 5.85 10 5 13 80.33 5.31 10 5 13 74.58 5.39 10 5 -13 88.10 6.39 -10 5 13 85.14 5.48 10 -5 -13 75.20 5.88 -10 -5 13 67.34 5.16 10 5 13 83.25 5.58 10 5 -13 73.27 5.98 10 5 14 35.40 4.29 10 5 -14 31.05 3.75 10 5 14 33.07 3.42 10 5 -14 30.97 3.91 10 5 -14 27.31 3.73 -10 -5 14 43.91 3.99 10 -5 -14 37.69 4.15 10 5 14 34.56 3.64 10 -5 -14 34.68 3.96 10 5 15 38.85 3.70 10 5 15 32.34 4.33 10 5 -15 29.77 3.78 -10 -5 15 32.49 3.44 10 5 -15 29.44 3.90 10 5 -15 31.57 4.01 -10 -5 15 33.32 3.56 10 -5 -15 38.89 4.23 10 5 15 30.91 3.39 10 -5 -15 30.00 3.75 10 5 16 179.92 9.24 10 5 16 155.98 10.17 10 5 -16 181.39 10.12 -10 -5 16 174.27 9.09 10 5 -16 191.29 10.39 10 5 -16 158.81 9.93 10 -5 -16 176.27 9.93 -10 -5 16 182.77 9.39 10 5 16 176.36 9.16 10 -5 -16 176.81 9.89 10 5 17 114.23 8.26 10 5 17 134.79 7.56 10 5 -17 129.93 8.17 -10 -5 17 122.72 7.19 10 5 -17 104.27 7.57 10 5 -17 117.23 8.08 10 -5 -17 103.29 7.53 -10 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8.07 1.95 10 -6 -8 14.80 2.74 -10 -6 9 155.45 8.39 -10 -6 -9 158.45 8.83 10 6 -9 164.62 9.00 10 6 9 170.31 8.90 10 -6 9 157.62 9.03 -10 -6 -9 160.26 9.60 10 6 -9 172.59 8.11 10 6 -9 163.82 9.50 10 6 -9 154.21 9.09 10 -6 -9 157.54 9.21 10 6 9 162.22 8.67 10 6 -9 160.67 8.00 -10 6 9 177.33 8.95 -10 -6 10 84.66 5.79 10 -6 -10 62.56 5.64 10 6 -10 89.19 6.29 10 6 10 92.04 6.73 10 6 10 91.92 6.07 10 -6 10 83.03 6.16 -10 -6 -10 83.15 6.53 10 6 -10 92.32 6.56 10 6 -10 87.16 6.33 -10 -6 10 98.61 6.24 10 -6 -10 89.89 6.45 10 6 10 87.45 5.92 10 6 -10 91.20 5.39 -10 6 10 89.94 6.05 10 -6 -11 49.08 4.87 10 6 -11 61.07 5.13 10 6 11 59.18 5.49 10 -6 11 57.80 5.12 -10 -6 -11 55.56 5.38 10 6 -11 63.03 5.39 10 6 -11 56.78 5.17 10 -6 -11 62.55 5.26 -10 -6 11 70.98 5.17 10 6 11 59.72 4.77 -10 6 11 62.42 4.89 10 -6 -12 285.12 13.67 10 6 -12 296.65 13.83 10 6 12 278.40 14.18 10 -6 12 295.04 13.80 -10 -6 -12 283.26 14.22 10 6 -12 291.24 14.00 10 6 -12 281.80 14.00 10 -6 -12 306.41 14.10 -10 -6 12 278.64 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20.63 3.52 10 6 -19 24.03 4.01 10 6 -19 23.15 3.67 -10 -6 19 21.94 3.27 10 -6 -19 21.56 3.61 10 -6 -19 23.77 3.61 10 6 -20 15.43 3.22 10 -6 -20 19.56 3.45 10 -6 20 18.40 3.21 10 6 20 14.97 3.48 10 6 -20 19.87 3.53 10 6 -20 11.60 3.13 -10 6 21 2.29 1.80 10 6 -21 3.13 2.16 10 6 -21 1.39 2.12 10 -6 -21 2.41 2.08 10 -6 21 -0.58 1.96 10 6 21 1.54 2.17 10 6 -21 4.44 2.31 10 -6 22 21.95 3.62 -10 6 22 22.59 3.60 10 6 -22 24.04 3.81 10 6 -22 26.99 4.19 10 -6 -22 23.19 3.75 10 6 22 22.12 4.18 10 6 -22 21.45 3.62 10 -6 23 12.06 2.88 -10 6 23 12.90 2.80 10 6 -23 17.25 3.38 10 6 -23 11.56 3.28 10 -6 -23 7.43 2.54 10 6 23 5.67 2.48 10 6 -23 8.63 2.87 -10 6 24 19.20 3.31 -10 6 24 19.61 3.41 10 6 -24 18.71 3.50 10 -6 -24 25.72 4.00 10 -6 24 22.06 3.75 -10 6 25 0.59 1.93 -10 -7 0 0.43 1.27 10 7 0 1.18 1.28 -10 -7 0 1.41 1.18 10 7 0 -0.42 1.32 10 7 0 0.41 1.20 -10 -7 0 -0.35 1.01 -10 7 0 0.94 1.52 10 -7 0 -0.57 1.46 -10 -7 -1 162.22 8.61 -10 -7 1 142.12 8.18 10 7 -1 164.16 8.19 10 7 1 163.44 8.36 -10 -7 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13 97.83 7.52 -10 -7 -13 90.80 7.24 10 7 -13 88.36 6.85 10 7 -13 87.23 6.95 10 -7 -13 103.83 7.23 -10 -7 13 94.41 6.57 -10 7 13 103.66 6.67 -10 7 13 94.67 6.43 10 -7 -14 167.85 9.51 10 7 -14 168.42 9.71 10 7 14 147.55 9.88 -10 -7 -14 171.46 10.32 10 7 -14 172.09 10.16 -10 7 14 159.74 8.97 10 -7 -14 168.43 9.75 -10 -7 14 153.16 9.00 10 7 -14 156.31 9.71 10 -7 -15 59.74 5.33 10 7 -15 69.99 6.10 10 7 -15 65.92 5.76 10 7 15 54.41 5.77 10 7 -15 67.52 6.06 -10 -7 15 63.93 5.36 10 -7 -15 61.98 5.62 -10 7 15 62.87 5.08 10 -7 -16 14.87 2.80 10 7 16 15.37 3.34 10 7 -16 15.01 3.14 10 7 -16 17.60 3.38 10 7 -16 12.84 2.97 10 -7 -16 11.51 2.80 -10 -7 16 15.80 2.96 -10 7 16 10.85 2.50 -10 7 17 14.52 2.95 10 7 -17 13.01 2.93 10 -7 -17 12.23 2.84 -10 -7 17 17.67 2.97 10 7 -17 18.37 3.37 10 7 17 14.39 3.19 10 7 -17 20.66 3.67 -10 7 18 133.01 8.47 10 7 -18 118.01 8.45 -10 -7 18 134.53 8.36 10 -7 -18 121.06 8.31 10 7 -18 138.58 8.86 10 7 18 137.64 9.66 10 7 -18 131.64 9.10 -10 7 19 35.82 4.39 10 7 -19 50.16 5.17 10 -7 -19 31.11 4.21 -10 -7 19 42.04 4.55 10 7 -19 46.04 5.07 10 7 19 45.55 5.53 10 7 -19 41.07 5.07 -10 7 20 4.11 2.24 10 7 -20 2.57 2.27 -10 -7 20 1.10 1.90 10 -7 -20 2.43 2.10 10 -7 20 1.73 1.76 10 7 -20 3.82 2.31 10 7 20 2.34 2.37 10 7 -20 1.42 2.00 -10 7 21 0.60 2.00 10 7 -21 4.54 2.30 10 7 -21 5.78 2.69 10 -7 -21 1.85 2.18 10 -7 21 4.69 2.52 10 7 -21 6.51 2.54 10 7 21 5.60 2.76 10 -7 22 0.59 2.16 -10 7 22 3.63 2.25 10 7 -22 0.65 2.19 10 7 -22 2.20 2.15 10 -7 -22 0.62 1.89 10 7 -22 0.66 2.09 10 7 22 0.82 2.20 10 7 -23 0.66 1.93 10 -7 -23 2.52 2.17 10 -7 23 3.61 2.35 -10 8 0 54.89 4.95 10 -8 0 54.18 5.34 10 8 0 61.37 4.95 -10 8 -1 3.03 1.85 -10 8 1 5.03 1.84 10 -8 -1 8.43 2.40 10 -8 1 4.31 2.30 10 8 1 6.39 1.94 -10 -8 1 7.49 1.91 10 8 -1 8.10 2.17 10 8 -1 6.68 1.87 -10 8 -2 1.01 1.43 -10 8 2 2.01 1.64 10 -8 -2 1.19 1.61 10 -8 2 3.12 1.90 10 8 2 3.13 1.58 10 8 -2 5.38 1.87 10 8 -2 2.05 1.37 -10 8 3 22.67 3.25 10 -8 -3 30.09 4.00 10 -8 3 26.58 3.92 10 8 -3 28.11 3.53 10 8 -3 27.75 3.23 10 8 -4 115.88 7.52 10 -8 4 96.29 6.94 10 8 -4 108.50 6.63 10 8 -4 107.80 6.87 10 -8 4 134.13 8.71 -10 8 -4 109.60 7.26 -10 8 4 113.55 7.40 10 -8 -4 128.59 8.15 10 8 -5 382.21 16.97 10 -8 5 377.15 16.68 10 8 -5 364.53 15.67 -10 -8 -5 385.90 17.64 10 8 -5 388.51 16.42 -10 8 5 399.09 16.97 -10 8 -5 379.39 16.82 10 -8 -5 383.63 17.40 10 8 -6 74.99 6.02 10 -8 6 76.75 5.89 10 8 -6 70.64 5.08 -10 -8 -6 76.41 6.42 10 8 -6 77.52 5.69 -10 8 6 80.25 6.01 10 -8 -6 72.81 6.15 -10 8 -6 84.41 6.13 10 8 -7 8.42 2.17 10 8 -7 9.42 2.44 10 8 -7 7.02 1.94 -10 -8 -7 10.59 2.88 10 -8 7 6.52 2.14 -10 -8 7 10.34 2.34 10 -8 -7 7.49 2.49 -10 8 -7 9.84 2.40 -10 8 7 13.17 2.65 10 8 -8 242.14 11.90 10 8 -8 251.51 12.64 10 -8 8 241.37 12.08 -10 -8 -8 236.63 12.82 10 -8 -8 242.42 12.61 -10 -8 8 240.73 11.87 -10 8 8 239.82 12.06 -10 8 -8 244.96 12.27 10 8 -9 33.52 3.79 10 8 -9 31.42 4.09 10 -8 9 29.75 3.77 -10 -8 -9 22.93 3.71 -10 -8 9 28.43 3.58 -10 8 9 31.41 3.80 10 -8 -9 33.39 4.16 -10 8 -9 25.83 3.65 10 8 -10 2.03 1.80 10 -8 10 5.70 2.02 -10 -8 -10 3.87 2.16 10 8 -10 1.20 1.75 -10 -8 10 -0.49 1.69 -10 8 10 4.84 2.05 -10 8 10 3.05 1.89 10 -8 -10 1.73 2.04 10 8 -11 14.56 2.86 10 -8 11 21.94 3.28 -10 -8 -11 17.00 3.41 -10 8 11 18.50 3.15 10 8 -11 14.08 3.08 10 -8 -11 17.36 3.31 -10 -8 11 18.89 2.97 -10 8 11 18.92 2.98 -10 8 11 17.82 3.12 10 -8 -12 12.95 2.72 10 8 -12 7.47 2.39 10 -8 12 8.95 2.40 -10 -8 -12 11.91 3.01 -10 8 12 14.21 2.76 10 8 -12 7.96 2.60 10 8 -12 11.90 2.89 10 -8 -12 8.72 2.56 -10 -8 12 9.13 2.35 -10 8 12 5.35 1.96 -10 8 12 9.70 2.54 10 -8 -13 45.30 4.61 10 8 -13 52.63 5.04 -10 -8 -13 47.65 5.38 -10 8 13 53.78 4.99 10 8 -13 47.02 5.10 10 8 -13 43.53 4.94 10 -8 -13 48.50 5.00 -10 -8 13 46.57 4.65 -10 8 13 39.42 4.22 10 8 -14 109.77 7.55 -10 -8 -14 102.82 7.94 -10 8 14 108.26 7.51 10 8 -14 115.84 8.10 10 8 -14 98.88 7.66 10 -8 -14 113.47 7.80 -10 -8 14 91.77 6.89 -10 8 14 111.06 7.15 10 8 15 15.69 3.53 10 8 -15 17.35 3.11 -10 -8 -15 20.75 3.65 10 8 -15 23.43 3.78 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1 103.12 7.86 -10 9 -1 110.76 7.48 10 9 1 110.32 7.25 10 9 -1 88.54 6.86 10 9 -2 34.71 4.16 -10 9 2 37.65 3.80 -10 9 2 38.54 4.22 -10 9 -2 36.76 4.25 10 -9 -2 41.22 4.79 10 -9 2 42.58 4.93 10 9 -3 198.33 10.94 -10 9 3 188.58 9.97 10 -9 3 213.65 10.94 -10 9 -3 205.13 10.92 -10 9 3 198.44 10.89 10 -9 -3 204.52 11.50 10 -9 3 205.71 11.84 10 9 -4 11.12 2.58 -10 9 4 15.52 2.55 10 -9 4 14.82 2.84 10 -9 4 8.90 2.75 -10 9 -4 11.38 2.63 10 -9 -4 11.80 3.01 -10 9 4 8.16 2.60 -10 -9 -5 6.51 2.60 10 -9 5 7.16 2.40 -10 9 5 10.53 2.27 10 9 -5 7.40 2.37 -10 -9 5 3.42 1.87 -10 9 -5 4.35 2.08 10 -9 -5 6.77 2.30 -10 9 5 6.53 2.26 -10 -9 -6 3.30 2.21 10 -9 6 2.56 1.95 -10 9 6 0.47 1.33 10 9 -6 -0.58 2.01 -10 -9 6 1.48 1.66 -10 9 -6 2.18 1.82 10 -9 -6 3.06 1.99 -10 9 6 4.35 2.08 -10 -9 -7 15.30 3.22 10 -9 7 14.91 2.86 -10 9 7 9.71 2.40 10 9 -7 15.46 3.12 -10 -9 7 14.00 2.87 -10 9 7 14.87 2.88 -10 9 -7 10.37 2.58 -10 9 7 10.92 2.62 10 -9 -7 9.77 2.92 10 9 -8 333.71 14.83 10 -9 8 296.97 14.63 -10 -9 -8 315.99 15.92 -10 9 8 318.07 14.73 10 9 -8 328.92 15.70 10 -9 -8 301.15 15.30 -10 -9 8 336.53 15.01 -10 9 8 327.38 15.19 -10 9 -8 312.95 14.96 -10 9 8 339.60 15.09 10 9 -9 23.72 3.37 10 -9 9 23.01 3.53 -10 -9 -9 25.74 4.08 -10 9 9 27.68 3.61 10 9 -9 17.37 3.47 -10 -9 9 23.66 3.35 -10 9 9 29.93 3.71 -10 9 -9 22.49 3.51 -10 9 9 26.30 3.64 10 -9 -9 20.05 3.54 10 9 -10 42.51 4.57 10 -9 10 57.46 5.13 -10 -9 -10 46.51 5.19 -10 9 10 58.86 5.13 10 9 -10 37.35 4.79 -10 -9 10 49.23 4.77 -10 9 10 52.74 5.08 -10 9 -10 45.21 4.77 10 -9 -10 42.50 4.74 -10 9 10 46.59 4.62 10 9 -11 3.20 1.79 10 -9 11 0.53 1.67 -10 -9 -11 0.69 1.86 -10 9 11 1.62 1.70 10 9 -11 1.29 2.10 10 -9 -11 -0.61 1.91 -10 -9 11 0.53 1.62 -10 9 11 2.59 1.69 -10 9 11 -0.55 1.61 -10 9 -11 -0.55 1.74 10 9 -12 18.05 3.22 -10 -9 -12 24.40 4.05 -10 9 12 19.86 3.25 10 9 -12 23.77 3.80 10 -9 -12 16.44 3.26 -10 -9 12 15.77 2.98 -10 9 -12 14.40 3.11 -10 9 12 15.62 2.93 10 9 -13 -0.56 1.82 -10 -9 -13 0.70 1.90 -10 9 13 1.13 1.59 10 9 -13 -1.35 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155.82 9.19 -10 10 2 192.71 10.37 -10 10 -2 169.65 9.91 10 -10 -2 173.92 10.54 10 -10 2 174.17 10.74 -10 10 2 142.91 9.08 10 10 -2 160.26 9.74 -10 -10 3 7.10 2.15 -10 10 3 4.81 2.13 -10 10 -3 8.63 2.48 10 -10 -3 7.31 2.54 -10 10 3 4.64 2.27 10 -10 3 7.14 2.85 10 10 -3 3.54 1.87 -10 10 4 63.85 5.20 10 10 -4 58.73 5.63 -10 -10 4 63.56 5.34 -10 10 4 74.29 6.09 10 -10 -4 51.84 5.49 -10 10 -4 57.52 5.53 -10 10 4 55.35 5.17 10 -10 4 63.11 6.26 -10 -10 -5 -0.69 2.25 -10 10 5 0.48 1.70 10 10 -5 1.83 1.92 -10 -10 5 1.04 1.74 10 -10 5 0.73 2.23 -10 10 5 1.08 1.81 -10 10 -5 -1.15 1.98 -10 10 5 0.58 1.89 10 -10 -5 -1.30 1.98 -10 -10 -6 7.71 2.85 -10 10 6 4.96 1.94 10 10 -6 3.10 2.08 -10 -10 6 3.67 1.81 -10 10 6 2.71 1.88 -10 10 6 3.50 2.07 10 -10 -6 6.47 2.52 -10 10 -6 5.17 2.14 -10 -10 -7 12.02 3.12 -10 10 7 9.68 2.48 10 10 -7 15.24 3.29 -10 -10 7 10.64 2.48 -10 10 7 10.90 2.53 -10 10 7 13.45 2.95 10 -10 -7 10.92 2.93 -10 10 -7 16.68 3.19 -10 -10 -8 -2.14 2.17 -10 10 8 3.14 1.90 10 10 -8 -0.65 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14 2.23 1.92 10 10 -15 15.64 3.20 -10 -10 -15 15.01 3.42 10 10 -15 8.04 2.94 -10 10 15 20.20 3.44 10 -10 -15 11.49 2.83 -10 -10 15 17.75 3.29 -10 10 15 10.58 2.60 10 10 -16 2.46 2.18 10 10 -16 2.96 2.41 -10 -10 16 0.62 1.89 10 -10 -16 0.64 1.87 -10 10 16 3.90 1.98 -10 10 16 0.62 2.03 10 10 -17 35.99 4.63 10 -10 -17 48.74 5.32 10 -10 -18 3.22 2.16 -10 -11 0 58.14 5.25 -10 11 0 60.74 5.80 10 -11 0 60.72 6.23 -10 11 0 51.95 5.09 -10 -11 1 186.21 10.18 -10 -11 -1 176.57 9.90 -10 11 1 172.94 10.41 -10 11 -1 170.75 10.41 10 -11 -1 168.49 11.00 10 -11 1 172.21 11.22 -10 11 1 189.38 10.45 -10 11 -1 190.15 10.36 -10 -11 2 2.65 1.93 -10 -11 -2 5.61 2.35 -10 11 2 6.73 2.37 -10 11 -2 5.43 2.17 -10 11 -2 2.44 2.11 -10 11 2 4.92 2.40 10 -11 -2 4.94 2.57 10 -11 2 2.97 2.26 10 11 -2 2.52 2.17 -10 -11 3 9.10 2.40 -10 11 3 7.91 2.36 -10 11 -3 8.61 2.46 -10 11 -3 10.37 2.78 -10 11 3 11.70 2.89 10 -11 -3 13.26 3.27 10 -11 3 15.03 3.42 10 11 -3 11.45 2.99 -10 -11 4 1.08 1.92 -10 11 -4 1.07 1.79 -10 11 -4 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4 -10 6.71 2.06 -11 -4 10 5.79 1.78 11 4 10 3.30 1.61 11 4 -10 3.25 1.33 11 -4 -10 3.89 1.73 -11 4 10 1.80 1.41 11 -4 -11 327.74 14.82 -11 -4 11 333.77 14.35 11 4 11 333.05 14.86 11 4 -11 266.87 14.07 11 4 11 329.43 13.72 11 4 11 320.32 13.88 11 -4 11 317.96 14.68 -11 -4 -11 325.47 15.23 11 4 -11 341.01 13.42 11 4 -11 323.09 14.69 11 4 -11 327.07 14.79 11 4 11 297.44 13.78 11 -4 -11 320.27 14.59 -11 -4 -11 320.48 13.72 -11 4 11 330.17 13.63 11 -4 -12 384.05 17.08 11 4 12 404.35 17.38 11 4 -12 389.48 17.11 11 4 12 391.18 16.12 11 4 12 380.95 16.17 11 -4 12 372.46 16.98 11 4 -12 416.20 17.38 11 4 -12 405.02 17.26 11 4 12 365.83 16.16 11 -4 -12 408.41 17.28 -11 -4 -12 398.66 16.05 11 4 13 28.82 3.76 11 4 -13 29.26 3.64 11 4 13 23.20 2.97 11 4 13 27.07 3.11 -11 -4 -13 32.41 3.26 11 4 -13 27.27 3.53 11 4 -13 34.50 3.94 11 4 13 28.68 3.33 11 -4 -13 35.14 3.95 -11 -4 13 31.78 3.35 11 -4 -13 23.82 3.44 11 4 14 190.73 9.47 11 4 14 185.25 10.41 11 4 -14 195.05 10.42 11 4 14 179.37 9.24 11 4 -14 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5.42 2.54 11 5 -21 10.33 3.03 11 5 -21 10.72 2.73 11 -5 -21 15.83 3.22 11 -5 -21 8.66 2.50 11 -5 -22 15.72 3.05 11 5 -22 21.10 3.61 11 -5 -22 13.79 3.27 11 5 -22 17.56 3.52 11 -5 -22 14.23 3.07 11 5 22 30.06 4.51 11 -5 22 19.03 3.47 11 5 -22 18.41 3.38 11 -5 23 26.78 3.85 11 5 -23 23.93 3.93 11 -5 -23 22.00 3.65 11 5 23 20.58 4.13 11 5 -23 28.14 4.21 11 -5 -23 18.19 3.71 11 5 -23 19.33 3.70 -11 5 24 21.78 3.70 11 5 -24 18.30 3.61 11 5 24 17.89 3.96 11 5 -25 5.27 2.57 -11 -6 0 0.40 1.22 -11 -6 0 -0.59 0.99 11 6 0 -0.39 1.24 -11 -6 0 -0.38 1.24 11 6 0 -0.77 1.09 11 6 0 -0.41 1.11 -11 6 0 -0.46 1.24 11 -6 0 -0.55 1.49 -11 -6 -1 42.23 3.96 -11 -6 1 44.27 3.46 -11 -6 1 35.66 3.64 11 6 -1 42.66 3.77 11 6 1 39.06 3.70 -11 -6 -1 38.59 3.67 -11 -6 1 38.60 3.69 11 6 1 36.94 3.52 11 6 -1 44.40 3.89 11 6 1 36.15 3.65 11 6 -1 41.76 3.82 -11 6 -1 42.01 4.10 -11 6 1 44.19 4.20 11 -6 -1 46.10 4.52 11 -6 1 56.03 5.07 -11 -6 -2 5.35 1.78 -11 -6 2 7.41 1.83 11 6 -2 5.74 1.68 11 6 2 5.65 1.71 -11 -6 -2 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29.38 4.01 13 5 -12 21.33 3.40 13 5 12 34.40 3.81 13 -5 -12 25.84 3.60 13 -5 -12 16.48 3.19 13 5 13 1.19 1.74 13 5 -13 1.21 1.96 13 5 13 1.91 1.82 13 5 -13 -0.60 1.95 13 5 -13 1.78 1.93 13 5 13 1.94 1.89 13 -5 -13 4.06 2.36 13 -5 -13 0.59 1.80 13 5 14 206.92 11.58 13 5 -14 196.92 11.35 13 5 14 214.11 10.72 13 5 -14 181.70 11.01 13 5 -14 214.90 11.58 13 5 14 208.50 10.61 -13 -5 14 199.84 10.38 13 -5 -14 194.17 11.02 13 -5 -14 198.46 11.24 13 5 15 1.91 1.87 13 5 -15 2.51 1.91 13 5 15 3.40 1.89 13 5 -15 3.10 2.08 13 5 -15 1.88 1.84 13 5 15 3.88 1.81 13 -5 -15 2.38 1.87 -13 -5 15 2.78 1.77 13 -5 -15 1.20 2.01 13 5 16 79.60 6.83 13 5 -16 75.91 6.61 13 5 16 70.31 5.73 13 5 -16 77.91 6.60 13 5 -16 78.95 6.61 13 -5 -16 79.58 6.54 13 5 16 74.73 5.75 13 -5 -16 86.93 6.76 13 5 17 3.40 2.14 13 5 -17 -0.65 2.05 13 5 -17 0.66 1.78 13 5 -17 0.64 2.02 13 -5 -17 -0.61 1.65 13 -5 -17 0.61 1.65 13 5 -18 47.04 5.13 13 5 18 26.60 4.11 13 -5 -18 42.16 5.00 13 5 -18 35.13 4.58 13 5 -18 42.37 4.97 13 -5 -18 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9.11 15 5 -3 140.14 8.81 15 5 4 28.08 3.59 15 -5 4 24.50 3.67 -15 -5 -4 24.45 3.81 15 5 -4 26.49 3.42 15 5 4 35.03 3.96 15 5 -4 20.48 3.16 15 -5 -4 27.60 3.90 -15 5 4 29.22 3.67 15 -5 4 24.34 3.88 15 5 -4 28.41 3.81 15 -5 5 31.21 4.21 -15 -5 -5 38.49 4.58 15 5 5 40.72 4.20 15 5 -5 32.74 3.72 15 5 -5 47.63 4.37 15 5 5 37.37 4.15 -15 5 5 33.31 3.94 15 -5 -5 32.31 4.23 15 -5 5 35.64 4.56 15 5 -5 38.44 4.28 -15 -5 -6 61.83 5.79 15 -5 6 44.11 4.87 15 5 -6 54.79 4.66 15 5 6 57.96 4.99 15 5 6 49.65 4.75 15 5 -6 47.91 4.51 15 -5 -6 51.55 5.23 -15 5 6 45.69 4.51 15 -5 6 44.55 5.10 15 5 -6 42.60 4.70 15 5 7 67.30 5.57 15 -5 7 68.12 6.07 -15 -5 -7 74.34 6.39 15 5 -7 69.68 5.32 15 5 -7 69.47 6.02 15 5 7 80.25 6.09 15 5 -7 76.99 5.67 15 -5 -7 60.64 5.82 -15 5 7 70.45 5.60 15 -5 7 73.59 6.59 15 -5 8 31.60 4.27 15 5 8 27.80 3.53 -15 -5 -8 19.52 3.56 15 -5 8 31.46 4.12 15 5 -8 22.83 3.07 15 5 -8 29.50 3.92 15 5 -8 27.91 3.69 15 -5 -8 26.51 3.85 15 5 8 27.75 3.69 15 5 -8 22.01 3.04 15 -5 -8 21.82 3.78 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1.97 2.07 15 5 -16 30.95 4.41 15 5 16 31.52 3.97 15 5 -16 28.44 4.29 15 -5 -16 21.35 3.79 15 5 -16 37.07 4.86 15 5 16 29.73 3.84 15 -5 -16 25.07 3.84 15 -5 -16 27.03 4.18 15 5 -17 0.71 2.17 15 5 17 -0.53 1.77 15 5 -17 0.69 1.93 15 -5 -17 -0.65 1.83 15 -5 -17 -0.66 1.71 15 -5 -17 1.36 2.14 15 5 -17 -1.38 2.24 15 5 -18 5.57 2.66 15 -5 -18 5.54 2.53 15 5 -18 7.05 2.69 15 -5 -18 9.20 2.78 15 -5 -18 5.35 2.38 15 -5 -19 -2.69 2.12 15 6 0 -2.48 1.89 -15 6 0 -0.56 1.71 15 -6 0 -1.31 2.13 15 6 0 -0.52 1.52 -15 -6 -1 188.28 10.81 15 6 -1 183.67 9.87 15 6 1 170.83 9.75 15 -6 -1 170.94 10.65 15 -6 1 167.66 10.59 -15 6 1 181.12 10.21 15 6 1 183.47 10.05 15 6 -1 183.46 10.01 15 -6 2 165.57 10.08 -15 -6 -2 180.61 10.46 15 6 -2 161.76 9.14 15 6 2 168.67 9.40 15 6 2 162.73 9.41 15 6 -2 143.33 8.93 15 -6 -2 153.37 9.94 15 -6 2 184.87 10.74 -15 6 2 157.82 9.48 15 6 -3 24.56 3.38 15 6 3 26.39 3.48 15 -6 3 30.21 4.14 -15 -6 -3 25.59 3.93 15 6 3 27.67 3.64 15 6 -3 27.12 3.52 -15 6 3 21.55 3.47 15 -6 -3 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-8 2.94 2.31 19 5 -8 4.36 2.26 19 -6 0 2.17 2.35 -19 6 0 -1.29 2.22 19 -6 -1 8.63 2.99 19 -6 1 8.02 2.85 -19 6 1 10.11 3.01 -19 -6 -2 3.56 2.17 -19 6 2 1.25 2.32 19 -6 -2 5.72 3.02 19 -6 2 2.93 2.46 19 6 -2 3.61 2.13 -19 -6 -3 51.18 5.74 19 -6 3 57.02 6.18 19 6 -3 59.46 5.60 19 -6 -3 54.82 5.97 -19 -6 -4 5.11 2.52 19 -6 4 2.99 2.65 19 6 -4 3.53 2.09 19 -6 5 3.78 2.61 19 6 -5 2.90 2.06 19 -6 6 -0.76 2.23 19 6 -6 2.01 2.24 20 0 0 41.11 4.89 20 0 1 -0.66 1.99 20 0 -1 -1.30 2.30 20 0 2 9.85 2.93 20 0 -2 5.18 2.24 20 0 3 -1.16 1.89 20 0 3 -0.66 2.00 20 0 -3 1.93 2.09 20 0 4 11.57 2.82 20 0 -4 13.94 3.29 20 0 4 18.45 3.50 20 0 -4 20.40 3.77 20 0 5 -0.58 1.88 20 0 -5 -1.28 2.08 20 0 5 0.66 1.93 20 0 -5 -0.63 1.92 20 0 6 16.89 3.35 20 0 6 24.73 3.67 20 0 -6 17.48 3.43 20 0 6 19.11 3.61 20 0 -6 21.92 3.72 20 0 7 -0.63 1.85 20 0 7 -1.15 1.92 20 0 -7 -0.66 2.06 20 0 7 -1.32 2.14 20 0 -7 -1.24 1.67 20 0 8 17.75 3.34 20 0 8 17.09 3.08 20 0 -8 17.88 3.40 20 0 8 18.41 3.46 20 0 -8 14.72 3.04 20 0 -9 2.02 1.97 20 0 -11 -1.94 2.47 20 -1 0 191.15 10.91 20 1 0 166.41 10.17 20 1 0 170.28 10.60 20 -1 0 179.10 10.88 20 -1 -1 11.27 2.93 20 1 -1 7.01 2.33 20 -1 1 3.77 2.17 20 1 1 5.26 2.28 20 -1 -1 5.17 2.52 20 1 1 5.19 2.48 20 1 -1 5.77 2.61 20 -1 1 7.30 2.54 20 -1 -1 3.29 2.27 20 -1 -2 22.52 3.69 20 1 2 19.26 3.42 20 -1 2 18.31 3.50 20 -1 -2 24.08 3.87 20 1 2 24.03 3.94 20 1 -2 20.37 3.53 20 -1 2 19.97 3.65 20 -1 -2 20.94 3.67 20 -1 -3 13.17 3.08 20 1 3 15.74 3.17 20 -1 3 13.96 3.08 20 -1 -3 5.90 2.41 20 1 3 14.33 3.20 20 1 -3 16.42 3.31 20 -1 3 10.01 2.85 20 -1 -3 16.90 3.24 20 1 4 16.30 3.12 20 -1 4 20.52 3.66 20 -1 -4 21.80 3.80 20 1 4 18.91 3.48 20 1 -4 18.85 3.47 20 -1 4 17.35 3.56 20 -1 -4 14.86 3.37 20 -1 5 0.65 1.90 20 1 5 0.58 1.83 20 -1 -5 -0.67 2.10 20 1 5 -0.65 1.91 20 1 -5 0.62 1.89 20 -1 5 2.67 1.96 20 -1 -5 2.56 2.27 20 -1 6 11.75 3.02 20 1 6 3.47 1.85 20 -1 -6 12.10 3.15 20 1 6 15.01 3.20 20 1 -6 14.75 3.10 20 -1 6 14.66 3.22 20 -1 -6 15.25 3.16 20 -1 7 2.63 2.14 20 -1 7 6.82 2.49 20 1 7 6.34 2.35 20 -1 -7 6.11 2.65 20 1 7 1.96 1.99 20 1 -7 0.61 1.98 20 -1 7 3.99 2.48 20 -1 -7 7.55 2.66 20 -1 8 15.21 3.33 20 -1 8 20.92 3.46 20 1 -8 20.00 3.57 20 -1 -8 25.30 4.02 20 1 -8 19.81 3.47 20 -1 8 19.25 3.59 20 -1 -8 17.44 3.34 20 1 -9 1.96 2.19 20 -1 -9 0.69 2.24 20 -1 9 0.56 1.83 20 1 -10 16.56 3.36 20 -2 0 3.27 2.19 20 2 0 3.52 2.28 20 -2 0 1.35 2.06 20 2 0 1.91 2.01 20 -2 -1 17.00 3.56 20 -2 1 11.11 2.85 20 2 -1 13.46 2.90 20 2 1 14.65 3.16 20 -2 -1 20.36 3.81 20 2 1 19.83 3.63 20 2 -1 16.47 3.25 20 -2 -2 64.80 6.14 20 -2 2 85.21 6.95 20 2 -2 77.14 6.41 20 2 2 60.35 5.83 20 -2 -2 69.51 6.51 20 2 2 80.99 6.71 20 2 -2 72.28 6.48 20 -2 -3 15.13 3.25 20 2 -3 16.33 3.19 20 -2 3 20.43 3.75 20 2 3 19.34 3.48 20 -2 -3 13.02 3.29 20 2 3 16.77 3.48 20 2 -3 17.46 3.25 20 -2 4 63.60 6.20 20 2 -4 84.32 6.61 20 2 4 72.57 6.17 20 -2 -4 70.84 6.71 20 2 4 78.79 6.80 20 2 -4 84.66 6.75 20 -2 5 50.19 5.42 20 2 -5 42.90 4.74 20 -2 -5 47.08 5.42 20 2 5 35.61 4.64 20 2 -5 42.81 4.91 20 -2 6 14.86 3.24 20 2 -6 13.28 3.09 20 -2 -6 17.40 3.39 20 2 6 18.78 3.53 20 2 -6 18.76 3.27 20 -2 6 18.83 3.58 20 -2 7 2.04 2.21 20 2 -7 1.72 1.87 20 -2 -7 0.70 2.35 20 2 -7 0.60 1.88 20 -2 9 6.14 2.36 20 2 -10 9.84 2.98 20 3 0 0.63 1.85 20 -3 0 0.68 1.83 20 3 1 8.27 2.54 20 3 -1 10.68 2.90 20 -3 -1 7.11 2.66 20 -3 -1 6.12 2.60 20 -3 1 3.40 2.22 20 3 2 3.84 2.15 20 3 -2 8.11 2.44 20 -3 -2 2.85 2.46 20 -3 -2 7.50 2.72 20 -3 2 5.44 2.48 20 3 3 1.28 1.88 20 3 -3 -0.62 1.81 20 -3 -3 2.14 2.32 20 -3 3 0.68 2.15 20 3 -4 20.20 3.51 20 -3 -4 19.33 3.82 20 -3 4 21.92 3.79 20 -3 -5 39.49 5.18 20 3 -5 41.79 4.74 20 3 -6 1.80 1.95 20 3 -7 0.59 1.86 20 4 -2 -0.62 1.88 20 4 -3 5.52 2.40 20 4 -4 2.43 1.78 20 4 -5 0.60 1.82 20 4 -6 3.55 2.21 20 -5 -3 50.20 5.62 21 -1 1 38.88 4.81 21 -1 2 20.83 3.65 21 -1 3 11.14 3.13 21 -1 -4 69.19 6.54 21 -2 -1 2.79 2.66 21 -2 -2 26.59 4.26 0 0 0 0.00 0.00 TITL PFPEtherABS in Pbca REM Pbca (#61, found as Pcab in ba-c setting) CELL 0.71073 16.479622 11.465421 24.703694 90.0000 90.0000 90.0000 ZERR 6.00 0.000229 0.000143 0.000309 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O F UNIT 150.00 48.00 12.00 12.00 84.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 SIZE 0.24 0.30 0.38 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 32785 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.170 _oxdiff_exptl_absorpt_empirical_full_min 0.853