data_naka413 _audit_creation_method 'SHELXL-2018/1' _shelx_SHELXL_version_number '2018/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C36 H34 N, B F4, H2 O' _chemical_formula_sum 'C36 H36 B F4 N O' _chemical_formula_weight 585.47 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'B' 'B' 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 10.5927(15) _cell_length_b 16.799(2) _cell_length_c 17.106(2) _cell_angle_alpha 90 _cell_angle_beta 100.067(2) _cell_angle_gamma 90 _cell_volume 2997.2(7) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 5355 _cell_measurement_theta_min 2.30 _cell_measurement_theta_max 26.87 _exptl_crystal_description 'prism' _exptl_crystal_colour 'yellow' _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.297 _exptl_crystal_F_000 1232 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.170 _exptl_crystal_size_mid 0.160 _exptl_crystal_size_min 0.120 _exptl_absorpt_coefficient_mu 0.094 _shelx_estimated_absorpt_T_min 0.984 _shelx_estimated_absorpt_T_max 0.989 _exptl_absorpt_correction_type 'numerical' _exptl_absorpt_correction_T_min 0.9843 _exptl_absorpt_correction_T_max 0.9889 _exptl_absorpt_process_details 'SADABS (Sheldrick, 1997)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'Bruker TXS fine-focus rotating anode' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method 'phi and omega scans' _diffrn_detector_area_resol_mean 8.333 _diffrn_reflns_number 14609 _diffrn_reflns_av_unetI/netI 0.0992 _diffrn_reflns_av_R_equivalents 0.1328 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_theta_min 1.712 _diffrn_reflns_theta_max 25.500 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measured_fraction_theta_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_point_group_measured_fraction_full 0.995 _reflns_number_total 5540 _reflns_number_gt 4138 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_molecular_graphics 'Yadokari-XG 2009 (Wakita Nemoto et al., 2009)' _computing_publication_material 'Yadokari-XG 2009 (Wakita Nemoto et al., 2009)' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0514P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5540 _refine_ls_number_parameters 400 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0658 _refine_ls_R_factor_gt 0.0497 _refine_ls_wR_factor_ref 0.1342 _refine_ls_wR_factor_gt 0.1252 _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_restrained_S_all 1.043 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group F3 F 0.94491(11) 0.40248(9) 0.67473(7) 0.0469(4) Uani 1 1 d . . . . . F1 F 1.15583(12) 0.39843(9) 0.67094(9) 0.0577(4) Uani 1 1 d . . . . . C5 C 1.00953(16) 0.03758(11) 0.83460(9) 0.0190(4) Uani 1 1 d . . . . . N1 N 0.76187(13) 0.17765(9) 0.76069(8) 0.0206(3) Uani 1 1 d . . . . . F2 F 1.02965(14) 0.29666(8) 0.62218(9) 0.0591(4) Uani 1 1 d . . . . . C3 C 0.79864(16) 0.11495(11) 0.80405(9) 0.0199(4) Uani 1 1 d . . . . . H3 H 0.745442 0.086580 0.833734 0.024 Uiso 1 1 calc R U . . . C11 C 1.17922(17) 0.13680(11) 0.84132(9) 0.0220(4) Uani 1 1 d . . . . . C4 C 0.92690(16) 0.09466(11) 0.80133(9) 0.0183(4) Uani 1 1 d . . . . . C35 C 0.84299(18) -0.12744(11) 0.92523(10) 0.0253(4) Uani 1 1 d . . . . . H33 H 0.759731 -0.149893 0.920806 0.030 Uiso 1 1 calc R U . . . C6 C 1.09295(17) 0.19460(11) 0.80717(9) 0.0217(4) Uani 1 1 d . . . . . C1 C 0.97974(16) 0.15829(11) 0.75013(9) 0.0195(4) Uani 1 1 d . . . . . C10 C 1.28562(17) 0.15649(14) 0.89684(10) 0.0290(5) Uani 1 1 d . . . . . H7 H 1.344987 0.116865 0.919367 0.035 Uiso 1 1 calc R U . . . C17 C 1.12401(16) 0.05319(11) 0.72354(9) 0.0196(4) Uani 1 1 d . . . . . C19 C 0.63062(16) 0.20563(12) 0.74110(10) 0.0228(4) Uani 1 1 d . . . . . C24 C 0.59513(17) 0.27366(12) 0.77974(10) 0.0268(4) Uani 1 1 d . . . . . C34 C 0.94359(19) -0.15834(12) 0.97940(10) 0.0279(4) Uani 1 1 d . . . . . H32 H 0.929495 -0.201874 1.012263 0.034 Uiso 1 1 calc R U . . . C16 C 1.18440(17) 0.00335(12) 0.67782(10) 0.0246(4) Uani 1 1 d . . . . . H11 H 1.241976 -0.036566 0.701810 0.029 Uiso 1 1 calc R U . . . C15 C 1.15921(19) 0.01273(12) 0.59549(11) 0.0283(4) Uani 1 1 d . . . . . H10 H 1.200284 -0.020995 0.563051 0.034 Uiso 1 1 calc R U . . . C36 C 0.86364(17) -0.06392(11) 0.87756(9) 0.0219(4) Uani 1 1 d . . . . . H34 H 0.794353 -0.043164 0.840334 0.026 Uiso 1 1 calc R U . . . C12 C 1.03775(16) 0.11084(11) 0.68855(10) 0.0197(4) Uani 1 1 d . . . . . C13 C 1.01331(18) 0.12011(11) 0.60696(10) 0.0238(4) Uani 1 1 d . . . . . H8 H 0.955186 0.159707 0.582889 0.029 Uiso 1 1 calc R U . . . C2 C 0.86358(16) 0.21000(12) 0.72002(10) 0.0233(4) Uani 1 1 d . . . . . H1 H 0.881257 0.266520 0.734266 0.028 Uiso 1 1 calc R U . . . H2 H 0.838561 0.205641 0.661650 0.028 Uiso 1 1 calc R U . . . F4 F 1.01216(17) 0.41357(10) 0.55826(8) 0.0748(5) Uani 1 1 d . . . . . C31 C 0.98578(16) -0.02988(11) 0.88365(9) 0.0195(4) Uani 1 1 d . . . . . C32 C 1.08648(18) -0.06201(12) 0.93824(10) 0.0237(4) Uani 1 1 d . . . . . H30 H 1.170149 -0.040103 0.942909 0.028 Uiso 1 1 calc R U . . . C33 C 1.06475(19) -0.12550(12) 0.98543(10) 0.0268(4) Uani 1 1 d . . . . . H31 H 1.133753 -0.146880 1.022457 0.032 Uiso 1 1 calc R U . . . C21 C 0.42275(19) 0.19224(13) 0.66398(11) 0.0332(5) Uani 1 1 d . . . . . H13 H 0.362904 0.165046 0.625255 0.040 Uiso 1 1 calc R U . . . C18 C 1.14320(16) 0.05217(11) 0.81378(9) 0.0202(4) Uani 1 1 d . . . . . H12 H 1.207841 0.011842 0.837956 0.024 Uiso 1 1 calc R U . . . C22 C 0.38357(19) 0.25823(14) 0.70093(12) 0.0357(5) Uani 1 1 d . . . . . H14 H 0.297369 0.275996 0.687410 0.043 Uiso 1 1 calc R U . . . C25 C 0.59004(19) 0.09235(12) 0.63946(10) 0.0297(5) Uani 1 1 d . . . . . H16 H 0.684285 0.085283 0.657862 0.036 Uiso 1 1 calc R U . . . C20 C 0.54837(17) 0.16449(12) 0.68218(10) 0.0268(4) Uani 1 1 d . . . . . C8 C 1.2184(2) 0.29331(13) 0.88482(11) 0.0354(5) Uani 1 1 d . . . . . H5 H 1.232495 0.347369 0.900203 0.042 Uiso 1 1 calc R U . . . C28 C 0.6864(2) 0.31325(12) 0.84686(11) 0.0327(5) Uani 1 1 d . . . . . H23 H 0.775886 0.301585 0.839040 0.039 Uiso 1 1 calc R U . . . C14 C 1.07528(19) 0.07048(12) 0.56086(10) 0.0275(4) Uani 1 1 d . . . . . H9 H 1.059608 0.076425 0.504765 0.033 Uiso 1 1 calc R U . . . C7 C 1.11225(19) 0.27342(12) 0.82832(10) 0.0281(4) Uani 1 1 d . . . . . H4 H 1.054206 0.313290 0.804764 0.034 Uiso 1 1 calc R U . . . C9 C 1.30347(19) 0.23605(14) 0.91888(11) 0.0350(5) Uani 1 1 d . . . . . H6 H 1.374995 0.250908 0.957757 0.042 Uiso 1 1 calc R U . . . C27 C 0.5244(2) 0.01745(14) 0.66074(14) 0.0461(6) Uani 1 1 d . . . . . H20 H 0.544952 0.008859 0.718230 0.069 Uiso 1 1 calc R U . . . H21 H 0.554347 -0.028119 0.633220 0.069 Uiso 1 1 calc R U . . . H22 H 0.431430 0.023078 0.644569 0.069 Uiso 1 1 calc R U . . . C23 C 0.46840(19) 0.29886(13) 0.75748(11) 0.0331(5) Uani 1 1 d . . . . . H15 H 0.439990 0.344841 0.781696 0.040 Uiso 1 1 calc R U . . . C30 C 0.6686(2) 0.27666(13) 0.92595(11) 0.0381(5) Uani 1 1 d . . . . . H27 H 0.584120 0.291270 0.937335 0.057 Uiso 1 1 calc R U . . . H28 H 0.735418 0.296654 0.968369 0.057 Uiso 1 1 calc R U . . . H29 H 0.674963 0.218584 0.922898 0.057 Uiso 1 1 calc R U . . . C29 C 0.6708(2) 0.40355(13) 0.84880(12) 0.0428(6) Uani 1 1 d . . . . . H24 H 0.684506 0.426192 0.798147 0.064 Uiso 1 1 calc R U . . . H25 H 0.733841 0.425782 0.892073 0.064 Uiso 1 1 calc R U . . . H26 H 0.584139 0.416619 0.857420 0.064 Uiso 1 1 calc R U . . . B1 B 1.0376(2) 0.37777(14) 0.63151(12) 0.0293(5) Uani 1 1 d . . . . . C26 C 0.5681(3) 0.10505(16) 0.54958(12) 0.0584(7) Uani 1 1 d . . . . . H17 H 0.475924 0.109511 0.529319 0.088 Uiso 1 1 calc R U . . . H18 H 0.603078 0.059758 0.524252 0.088 Uiso 1 1 calc R U . . . H19 H 0.611168 0.154038 0.537580 0.088 Uiso 1 1 calc R U . . . O1 O 0.62576(16) 0.06164(11) 0.92267(10) 0.0452(4) Uani 1 1 d . . . . . H36 H 0.584(4) 0.007(3) 0.901(2) 0.126(14) Uiso 1 1 d . . . . . H35 H 0.592(2) 0.0768(18) 0.9675(17) 0.068(8) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F3 0.0356(7) 0.0613(9) 0.0450(7) -0.0088(6) 0.0101(5) 0.0084(7) F1 0.0325(7) 0.0617(10) 0.0763(10) -0.0152(7) 0.0019(6) -0.0110(7) C5 0.0192(9) 0.0244(9) 0.0134(8) -0.0033(7) 0.0023(6) -0.0023(8) N1 0.0184(8) 0.0262(8) 0.0177(7) 0.0014(6) 0.0045(6) 0.0025(7) F2 0.0718(10) 0.0362(8) 0.0743(10) -0.0136(7) 0.0264(8) -0.0129(8) C3 0.0198(9) 0.0259(10) 0.0139(8) -0.0014(7) 0.0030(6) -0.0002(8) C11 0.0195(9) 0.0309(10) 0.0172(8) -0.0011(7) 0.0080(7) -0.0047(8) C4 0.0171(8) 0.0223(9) 0.0157(8) -0.0001(7) 0.0034(6) -0.0026(8) C35 0.0293(10) 0.0254(10) 0.0225(9) -0.0039(7) 0.0080(7) -0.0073(9) C6 0.0227(9) 0.0271(10) 0.0173(8) 0.0003(7) 0.0095(7) -0.0046(9) C1 0.0199(9) 0.0223(9) 0.0172(8) 0.0017(7) 0.0055(7) 0.0004(8) C10 0.0215(10) 0.0461(13) 0.0200(9) -0.0008(8) 0.0049(7) -0.0081(10) C17 0.0165(9) 0.0223(9) 0.0212(9) 0.0006(7) 0.0068(7) -0.0033(8) C19 0.0188(9) 0.0298(10) 0.0209(9) 0.0060(7) 0.0066(7) 0.0047(8) C24 0.0233(10) 0.0323(11) 0.0265(9) 0.0025(8) 0.0092(8) 0.0027(9) C34 0.0400(12) 0.0251(10) 0.0203(9) 0.0031(8) 0.0097(8) -0.0004(10) C16 0.0229(10) 0.0255(10) 0.0270(9) 0.0021(8) 0.0089(7) -0.0009(9) C15 0.0335(11) 0.0277(10) 0.0273(9) -0.0050(8) 0.0150(8) -0.0008(10) C36 0.0237(9) 0.0256(10) 0.0164(8) -0.0020(7) 0.0031(7) -0.0015(8) C12 0.0180(9) 0.0225(9) 0.0198(8) -0.0014(7) 0.0061(7) -0.0047(8) C13 0.0251(10) 0.0255(10) 0.0206(9) 0.0015(7) 0.0033(7) -0.0011(9) C2 0.0227(10) 0.0272(10) 0.0218(9) 0.0039(7) 0.0091(7) 0.0025(9) F4 0.1030(13) 0.0843(12) 0.0415(8) 0.0272(8) 0.0243(8) 0.0385(11) C31 0.0236(9) 0.0220(9) 0.0136(8) -0.0024(7) 0.0049(7) 0.0006(8) C32 0.0225(9) 0.0304(11) 0.0185(8) -0.0013(7) 0.0043(7) 0.0009(9) C33 0.0332(11) 0.0285(10) 0.0182(9) 0.0027(7) 0.0033(7) 0.0054(9) C21 0.0264(11) 0.0458(13) 0.0262(10) 0.0040(9) 0.0009(8) 0.0044(10) C18 0.0161(9) 0.0249(10) 0.0199(9) 0.0015(7) 0.0043(6) -0.0001(8) C22 0.0218(10) 0.0493(14) 0.0361(11) 0.0093(10) 0.0048(8) 0.0117(10) C25 0.0258(10) 0.0378(12) 0.0246(9) -0.0017(8) 0.0022(8) 0.0000(10) C20 0.0251(10) 0.0378(12) 0.0180(8) 0.0045(8) 0.0047(7) 0.0025(9) C8 0.0475(13) 0.0358(12) 0.0261(10) -0.0072(9) 0.0156(9) -0.0202(11) C28 0.0287(11) 0.0365(12) 0.0351(11) -0.0077(9) 0.0116(8) 0.0039(10) C14 0.0348(11) 0.0308(10) 0.0182(9) -0.0008(8) 0.0086(7) -0.0047(9) C7 0.0372(11) 0.0271(10) 0.0231(9) -0.0010(8) 0.0138(8) -0.0068(10) C9 0.0314(11) 0.0523(14) 0.0216(9) -0.0058(9) 0.0056(8) -0.0204(11) C27 0.0450(14) 0.0410(14) 0.0562(14) 0.0028(11) 0.0195(11) 0.0015(12) C23 0.0302(11) 0.0371(12) 0.0344(11) 0.0039(9) 0.0121(9) 0.0114(10) C30 0.0453(13) 0.0337(12) 0.0316(11) -0.0013(9) -0.0040(9) 0.0059(11) C29 0.0600(15) 0.0379(12) 0.0333(11) 0.0000(10) 0.0158(10) -0.0083(12) B1 0.0289(12) 0.0316(13) 0.0268(11) 0.0022(9) 0.0026(9) -0.0005(11) C26 0.100(2) 0.0470(15) 0.0303(12) -0.0036(11) 0.0179(13) 0.0098(16) O1 0.0462(10) 0.0430(10) 0.0529(10) -0.0049(8) 0.0262(8) -0.0102(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag F3 B1 1.392(3) . ? F1 B1 1.359(3) . ? C5 C4 1.355(2) . ? C5 C31 1.458(2) . ? C5 C18 1.539(2) . ? N1 C3 1.308(2) . ? N1 C19 1.450(2) . ? N1 C2 1.484(2) . ? F2 B1 1.373(3) . ? C3 C4 1.409(2) . ? C11 C10 1.381(2) . ? C11 C6 1.390(3) . ? C11 C18 1.525(3) . ? C4 C1 1.547(2) . ? C35 C36 1.383(3) . ? C35 C34 1.385(3) . ? C6 C7 1.378(3) . ? C6 C1 1.534(2) . ? C1 C2 1.521(2) . ? C1 C12 1.533(2) . ? C10 C9 1.392(3) . ? C17 C16 1.377(2) . ? C17 C12 1.393(2) . ? C17 C18 1.521(2) . ? C19 C20 1.395(3) . ? C19 C24 1.404(3) . ? C24 C23 1.396(3) . ? C24 C28 1.519(3) . ? C34 C33 1.384(3) . ? C16 C15 1.396(2) . ? C15 C14 1.378(3) . ? C36 C31 1.402(2) . ? C12 C13 1.383(2) . ? C13 C14 1.389(3) . ? F4 B1 1.374(3) . ? C31 C32 1.398(2) . ? C32 C33 1.381(3) . ? C21 C22 1.376(3) . ? C21 C20 1.393(3) . ? C22 C23 1.380(3) . ? C25 C27 1.512(3) . ? C25 C20 1.520(3) . ? C25 C26 1.529(3) . ? C8 C9 1.376(3) . ? C8 C7 1.389(3) . ? C28 C29 1.527(3) . ? C28 C30 1.527(3) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 C5 C31 128.92(16) . . ? C4 C5 C18 110.06(15) . . ? C31 C5 C18 121.02(15) . . ? C3 N1 C19 124.79(15) . . ? C3 N1 C2 113.09(14) . . ? C19 N1 C2 121.21(14) . . ? N1 C3 C4 111.67(16) . . ? C10 C11 C6 121.27(18) . . ? C10 C11 C18 124.46(18) . . ? C6 C11 C18 114.25(15) . . ? C5 C4 C3 135.49(16) . . ? C5 C4 C1 117.11(15) . . ? C3 C4 C1 107.33(15) . . ? C36 C35 C34 120.07(18) . . ? C7 C6 C11 120.28(17) . . ? C7 C6 C1 127.77(17) . . ? C11 C6 C1 111.90(15) . . ? C2 C1 C12 117.53(14) . . ? C2 C1 C6 118.99(15) . . ? C12 C1 C6 106.33(13) . . ? C2 C1 C4 103.59(13) . . ? C12 C1 C4 104.94(14) . . ? C6 C1 C4 103.57(13) . . ? C11 C10 C9 118.2(2) . . ? C16 C17 C12 120.91(15) . . ? C16 C17 C18 125.20(16) . . ? C12 C17 C18 113.90(14) . . ? C20 C19 C24 123.97(17) . . ? C20 C19 N1 117.31(16) . . ? C24 C19 N1 118.67(16) . . ? C23 C24 C19 116.26(17) . . ? C23 C24 C28 121.87(18) . . ? C19 C24 C28 121.67(16) . . ? C33 C34 C35 119.70(17) . . ? C17 C16 C15 118.59(18) . . ? C14 C15 C16 120.56(17) . . ? C35 C36 C31 120.66(17) . . ? C13 C12 C17 120.33(16) . . ? C13 C12 C1 127.46(16) . . ? C17 C12 C1 112.22(14) . . ? C12 C13 C14 118.80(18) . . ? N1 C2 C1 104.05(13) . . ? C32 C31 C36 118.62(16) . . ? C32 C31 C5 119.76(16) . . ? C36 C31 C5 121.62(15) . . ? C33 C32 C31 120.21(17) . . ? C32 C33 C34 120.76(17) . . ? C22 C21 C20 121.34(19) . . ? C17 C18 C11 106.54(14) . . ? C17 C18 C5 105.75(13) . . ? C11 C18 C5 105.52(14) . . ? C21 C22 C23 120.58(19) . . ? C27 C25 C20 111.30(16) . . ? C27 C25 C26 111.26(18) . . ? C20 C25 C26 111.48(17) . . ? C21 C20 C19 116.57(18) . . ? C21 C20 C25 120.38(17) . . ? C19 C20 C25 123.05(16) . . ? C9 C8 C7 121.12(19) . . ? C24 C28 C29 113.25(18) . . ? C24 C28 C30 109.45(17) . . ? C29 C28 C30 110.50(16) . . ? C15 C14 C13 120.80(17) . . ? C6 C7 C8 118.6(2) . . ? C8 C9 C10 120.56(18) . . ? C22 C23 C24 121.24(19) . . ? F1 B1 F2 110.10(19) . . ? F1 B1 F4 110.96(19) . . ? F2 B1 F4 109.28(18) . . ? F1 B1 F3 109.55(17) . . ? F2 B1 F3 108.85(18) . . ? F4 B1 F3 108.04(18) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C19 N1 C3 C4 169.65(15) . . . . ? C2 N1 C3 C4 0.5(2) . . . . ? C31 C5 C4 C3 5.2(3) . . . . ? C18 C5 C4 C3 -174.76(19) . . . . ? C31 C5 C4 C1 -178.59(16) . . . . ? C18 C5 C4 C1 1.5(2) . . . . ? N1 C3 C4 C5 179.33(18) . . . . ? N1 C3 C4 C1 2.87(19) . . . . ? C10 C11 C6 C7 0.0(2) . . . . ? C18 C11 C6 C7 178.38(15) . . . . ? C10 C11 C6 C1 -177.52(14) . . . . ? C18 C11 C6 C1 0.86(19) . . . . ? C7 C6 C1 C2 -9.2(2) . . . . ? C11 C6 C1 C2 168.10(14) . . . . ? C7 C6 C1 C12 126.29(18) . . . . ? C11 C6 C1 C12 -56.42(18) . . . . ? C7 C6 C1 C4 -123.40(18) . . . . ? C11 C6 C1 C4 53.89(17) . . . . ? C5 C4 C1 C2 177.94(14) . . . . ? C3 C4 C1 C2 -4.84(17) . . . . ? C5 C4 C1 C12 54.11(19) . . . . ? C3 C4 C1 C12 -128.67(14) . . . . ? C5 C4 C1 C6 -57.22(19) . . . . ? C3 C4 C1 C6 120.00(15) . . . . ? C6 C11 C10 C9 1.0(2) . . . . ? C18 C11 C10 C9 -177.21(16) . . . . ? C3 N1 C19 C20 -77.0(2) . . . . ? C2 N1 C19 C20 91.4(2) . . . . ? C3 N1 C19 C24 105.5(2) . . . . ? C2 N1 C19 C24 -86.2(2) . . . . ? C20 C19 C24 C23 1.4(3) . . . . ? N1 C19 C24 C23 178.77(15) . . . . ? C20 C19 C24 C28 176.37(17) . . . . ? N1 C19 C24 C28 -6.3(3) . . . . ? C36 C35 C34 C33 -0.2(3) . . . . ? C12 C17 C16 C15 1.2(3) . . . . ? C18 C17 C16 C15 -178.49(17) . . . . ? C17 C16 C15 C14 -0.2(3) . . . . ? C34 C35 C36 C31 -0.3(3) . . . . ? C16 C17 C12 C13 -1.4(3) . . . . ? C18 C17 C12 C13 178.31(16) . . . . ? C16 C17 C12 C1 178.75(16) . . . . ? C18 C17 C12 C1 -1.5(2) . . . . ? C2 C1 C12 C13 13.3(3) . . . . ? C6 C1 C12 C13 -122.89(18) . . . . ? C4 C1 C12 C13 127.77(18) . . . . ? C2 C1 C12 C17 -166.80(15) . . . . ? C6 C1 C12 C17 56.96(18) . . . . ? C4 C1 C12 C17 -52.38(18) . . . . ? C17 C12 C13 C14 0.6(3) . . . . ? C1 C12 C13 C14 -179.53(17) . . . . ? C3 N1 C2 C1 -3.63(19) . . . . ? C19 N1 C2 C1 -173.22(14) . . . . ? C12 C1 C2 N1 120.04(16) . . . . ? C6 C1 C2 N1 -109.32(16) . . . . ? C4 C1 C2 N1 4.88(17) . . . . ? C35 C36 C31 C32 0.7(3) . . . . ? C35 C36 C31 C5 -179.38(16) . . . . ? C4 C5 C31 C32 -153.38(17) . . . . ? C18 C5 C31 C32 26.6(2) . . . . ? C4 C5 C31 C36 26.7(3) . . . . ? C18 C5 C31 C36 -153.36(16) . . . . ? C36 C31 C32 C33 -0.6(3) . . . . ? C5 C31 C32 C33 179.47(16) . . . . ? C31 C32 C33 C34 0.1(3) . . . . ? C35 C34 C33 C32 0.3(3) . . . . ? C16 C17 C18 C11 126.15(19) . . . . ? C12 C17 C18 C11 -53.54(19) . . . . ? C16 C17 C18 C5 -121.90(19) . . . . ? C12 C17 C18 C5 58.41(19) . . . . ? C10 C11 C18 C17 -127.58(17) . . . . ? C6 C11 C18 C17 54.09(18) . . . . ? C10 C11 C18 C5 120.30(17) . . . . ? C6 C11 C18 C5 -58.02(17) . . . . ? C4 C5 C18 C17 -57.24(18) . . . . ? C31 C5 C18 C17 122.80(16) . . . . ? C4 C5 C18 C11 55.43(17) . . . . ? C31 C5 C18 C11 -124.53(16) . . . . ? C20 C21 C22 C23 -0.1(3) . . . . ? C22 C21 C20 C19 1.8(3) . . . . ? C22 C21 C20 C25 -178.87(18) . . . . ? C24 C19 C20 C21 -2.5(3) . . . . ? N1 C19 C20 C21 -179.87(15) . . . . ? C24 C19 C20 C25 178.17(17) . . . . ? N1 C19 C20 C25 0.8(3) . . . . ? C27 C25 C20 C21 -67.1(2) . . . . ? C26 C25 C20 C21 57.8(2) . . . . ? C27 C25 C20 C19 112.2(2) . . . . ? C26 C25 C20 C19 -122.9(2) . . . . ? C23 C24 C28 C29 -39.0(3) . . . . ? C19 C24 C28 C29 146.29(18) . . . . ? C23 C24 C28 C30 84.7(2) . . . . ? C19 C24 C28 C30 -89.9(2) . . . . ? C16 C15 C14 C13 -0.5(3) . . . . ? C12 C13 C14 C15 0.3(3) . . . . ? C11 C6 C7 C8 -0.7(3) . . . . ? C1 C6 C7 C8 176.36(15) . . . . ? C9 C8 C7 C6 0.4(3) . . . . ? C7 C8 C9 C10 0.6(3) . . . . ? C11 C10 C9 C8 -1.3(3) . . . . ? C21 C22 C23 C24 -1.1(3) . . . . ? C19 C24 C23 C22 0.4(3) . . . . ? C28 C24 C23 C22 -174.52(18) . . . . ? _refine_diff_density_max 0.572 _refine_diff_density_min -0.391 _refine_diff_density_rms 0.056 _shelx_res_file ; TITL naka413.res created by SHELXL-2018/1 at 19:14:31 on 17-Jan-2023 REM Yadorkari-X generated CELL 0.71073 10.5927 16.7994 17.1060 90.0000 100.0670 90.0000 ZERR 4.0 0.0015 0.0024 0.0024 0.0000 0.0020 0.0000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z REM SPGR P21/n monoclinic SFAC C H B N F O UNIT 144 144 4 4 16 4 SIZE 0.12 0.16 0.17 TEMP -173.0 L.S. 10 FMAP 2 PLAN -150 ACTA CONF LIST 4 WPDB MERG 2 OMIT -10.000000 51.000000 OMIT 1 0 1 OMIT -6 3 6 OMIT -1 0 1 OMIT -2 1 3 OMIT 0 9 6 OMIT 2 2 8 WGHT 0.051400 FVAR 0.29669 F3 5 0.944910 0.402478 0.674729 11.00000 0.03555 0.06126 = 0.04503 -0.00878 0.01007 0.00844 F1 5 1.155826 0.398434 0.670936 11.00000 0.03249 0.06170 = 0.07630 -0.01523 0.00186 -0.01096 C5 1 1.009526 0.037584 0.834601 11.00000 0.01917 0.02437 = 0.01336 -0.00331 0.00229 -0.00230 N1 4 0.761873 0.177647 0.760691 11.00000 0.01838 0.02618 = 0.01775 0.00143 0.00448 0.00250 F2 5 1.029652 0.296658 0.622178 11.00000 0.07177 0.03624 = 0.07429 -0.01359 0.02640 -0.01291 C3 1 0.798638 0.114953 0.804054 11.00000 0.01975 0.02593 = 0.01395 -0.00142 0.00305 -0.00023 AFIX 43 H3 2 0.745442 0.086580 0.833734 11.00000 -1.20000 AFIX 0 C11 1 1.179219 0.136797 0.841317 11.00000 0.01952 0.03091 = 0.01723 -0.00108 0.00796 -0.00466 C4 1 0.926897 0.094664 0.801333 11.00000 0.01707 0.02232 = 0.01565 -0.00011 0.00343 -0.00255 C35 1 0.842994 -0.127443 0.925231 11.00000 0.02927 0.02542 = 0.02249 -0.00387 0.00802 -0.00729 AFIX 43 H33 2 0.759731 -0.149893 0.920806 11.00000 -1.20000 AFIX 0 C6 1 1.092948 0.194598 0.807166 11.00000 0.02272 0.02708 = 0.01732 0.00033 0.00948 -0.00456 C1 1 0.979740 0.158290 0.750132 11.00000 0.01989 0.02226 = 0.01717 0.00172 0.00549 0.00037 C10 1 1.285620 0.156495 0.896837 11.00000 0.02146 0.04611 = 0.02002 -0.00082 0.00487 -0.00809 AFIX 43 H7 2 1.344987 0.116865 0.919367 11.00000 -1.20000 AFIX 0 C17 1 1.124012 0.053195 0.723540 11.00000 0.01650 0.02227 = 0.02122 0.00058 0.00676 -0.00327 C19 1 0.630616 0.205632 0.741100 11.00000 0.01879 0.02975 = 0.02094 0.00600 0.00663 0.00474 C24 1 0.595133 0.273660 0.779737 11.00000 0.02326 0.03233 = 0.02649 0.00254 0.00923 0.00265 C34 1 0.943588 -0.158341 0.979399 11.00000 0.03999 0.02507 = 0.02031 0.00306 0.00971 -0.00037 AFIX 43 H32 2 0.929495 -0.201874 1.012263 11.00000 -1.20000 AFIX 0 C16 1 1.184402 0.003349 0.677819 11.00000 0.02285 0.02550 = 0.02702 0.00209 0.00894 -0.00087 AFIX 43 H11 2 1.241976 -0.036566 0.701810 11.00000 -1.20000 AFIX 0 C15 1 1.159211 0.012727 0.595489 11.00000 0.03348 0.02766 = 0.02733 -0.00503 0.01498 -0.00084 AFIX 43 H10 2 1.200284 -0.020995 0.563051 11.00000 -1.20000 AFIX 0 C36 1 0.863645 -0.063921 0.877563 11.00000 0.02367 0.02558 = 0.01643 -0.00202 0.00308 -0.00146 AFIX 43 H34 2 0.794353 -0.043164 0.840334 11.00000 -1.20000 AFIX 0 C12 1 1.037750 0.110836 0.688554 11.00000 0.01795 0.02247 = 0.01984 -0.00138 0.00612 -0.00470 C13 1 1.013308 0.120109 0.606960 11.00000 0.02509 0.02554 = 0.02063 0.00145 0.00327 -0.00114 AFIX 43 H8 2 0.955186 0.159707 0.582889 11.00000 -1.20000 AFIX 0 C2 1 0.863579 0.209998 0.720022 11.00000 0.02272 0.02716 = 0.02183 0.00386 0.00910 0.00250 AFIX 23 H1 2 0.881257 0.266520 0.734266 11.00000 -1.20000 H2 2 0.838561 0.205641 0.661650 11.00000 -1.20000 AFIX 0 F4 5 1.012156 0.413573 0.558257 11.00000 0.10301 0.08429 = 0.04145 0.02718 0.02429 0.03852 C31 1 0.985778 -0.029885 0.883649 11.00000 0.02358 0.02196 = 0.01365 -0.00235 0.00490 0.00056 C32 1 1.086484 -0.062009 0.938244 11.00000 0.02248 0.03036 = 0.01849 -0.00133 0.00432 0.00087 AFIX 43 H30 2 1.170149 -0.040103 0.942909 11.00000 -1.20000 AFIX 0 C33 1 1.064754 -0.125499 0.985432 11.00000 0.03316 0.02850 = 0.01822 0.00272 0.00332 0.00545 AFIX 43 H31 2 1.133753 -0.146880 1.022457 11.00000 -1.20000 AFIX 0 C21 1 0.422746 0.192241 0.663977 11.00000 0.02644 0.04577 = 0.02618 0.00395 0.00093 0.00441 AFIX 43 H13 2 0.362904 0.165046 0.625255 11.00000 -1.20000 AFIX 0 C18 1 1.143197 0.052174 0.813780 11.00000 0.01608 0.02489 = 0.01991 0.00155 0.00434 -0.00007 AFIX 13 H12 2 1.207841 0.011842 0.837956 11.00000 -1.20000 AFIX 0 C22 1 0.383571 0.258232 0.700930 11.00000 0.02178 0.04930 = 0.03607 0.00926 0.00481 0.01168 AFIX 43 H14 2 0.297369 0.275996 0.687410 11.00000 -1.20000 AFIX 0 C25 1 0.590037 0.092345 0.639459 11.00000 0.02578 0.03783 = 0.02458 -0.00171 0.00215 0.00004 AFIX 13 H16 2 0.684285 0.085283 0.657862 11.00000 -1.20000 AFIX 0 C20 1 0.548369 0.164486 0.682179 11.00000 0.02506 0.03782 = 0.01798 0.00449 0.00475 0.00252 C8 1 1.218404 0.293311 0.884820 11.00000 0.04753 0.03575 = 0.02607 -0.00723 0.01556 -0.02016 AFIX 43 H5 2 1.232495 0.347369 0.900203 11.00000 -1.20000 AFIX 0 C28 1 0.686359 0.313251 0.846860 11.00000 0.02868 0.03647 = 0.03514 -0.00769 0.01164 0.00391 AFIX 13 H23 2 0.775886 0.301585 0.839040 11.00000 -1.20000 AFIX 0 C14 1 1.075278 0.070481 0.560857 11.00000 0.03479 0.03079 = 0.01822 -0.00076 0.00861 -0.00469 AFIX 43 H9 2 1.059608 0.076425 0.504765 11.00000 -1.20000 AFIX 0 C7 1 1.112254 0.273418 0.828320 11.00000 0.03724 0.02714 = 0.02311 -0.00101 0.01377 -0.00677 AFIX 43 H4 2 1.054206 0.313290 0.804764 11.00000 -1.20000 AFIX 0 C9 1 1.303473 0.236045 0.918876 11.00000 0.03141 0.05229 = 0.02157 -0.00582 0.00557 -0.02041 AFIX 43 H6 2 1.374995 0.250908 0.957757 11.00000 -1.20000 AFIX 0 C27 1 0.524417 0.017450 0.660743 11.00000 0.04500 0.04098 = 0.05618 0.00278 0.01946 0.00146 AFIX 137 H20 2 0.544952 0.008859 0.718230 11.00000 -1.50000 H21 2 0.554347 -0.028119 0.633220 11.00000 -1.50000 H22 2 0.431430 0.023078 0.644569 11.00000 -1.50000 AFIX 0 C23 1 0.468403 0.298861 0.757476 11.00000 0.03022 0.03707 = 0.03445 0.00391 0.01209 0.01143 AFIX 43 H15 2 0.439990 0.344841 0.781696 11.00000 -1.20000 AFIX 0 C30 1 0.668626 0.276662 0.925950 11.00000 0.04528 0.03369 = 0.03161 -0.00133 -0.00399 0.00592 AFIX 137 H27 2 0.584120 0.291270 0.937335 11.00000 -1.50000 H28 2 0.735418 0.296654 0.968369 11.00000 -1.50000 H29 2 0.674963 0.218584 0.922898 11.00000 -1.50000 AFIX 0 C29 1 0.670820 0.403545 0.848799 11.00000 0.06002 0.03788 = 0.03332 0.00000 0.01582 -0.00835 AFIX 137 H24 2 0.684506 0.426192 0.798147 11.00000 -1.50000 H25 2 0.733841 0.425782 0.892073 11.00000 -1.50000 H26 2 0.584139 0.416619 0.857420 11.00000 -1.50000 AFIX 0 B1 3 1.037620 0.377772 0.631514 11.00000 0.02887 0.03156 = 0.02676 0.00221 0.00263 -0.00050 C26 1 0.568080 0.105054 0.549583 11.00000 0.10031 0.04702 = 0.03027 -0.00363 0.01788 0.00984 AFIX 137 H17 2 0.475924 0.109511 0.529319 11.00000 -1.50000 H18 2 0.603078 0.059758 0.524252 11.00000 -1.50000 H19 2 0.611168 0.154038 0.537580 11.00000 -1.50000 AFIX 0 O1 6 0.625763 0.061643 0.922670 11.00000 0.04617 0.04304 = 0.05286 -0.00495 0.02620 -0.01025 H36 2 0.584346 0.007156 0.900700 11.00000 0.12580 H35 2 0.592284 0.076842 0.967510 11.00000 0.06768 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM REM R1 = 0.0497 for 4138 Fo > 4sig(Fo) and 0.0658 for all 5540 data REM 400 parameters refined using 0 restraints END WGHT 0.0514 0.0000 REM Highest difference peak 0.572, deepest hole -0.391, 1-sigma level 0.056 Q1 1 1.0854 0.4430 0.5846 11.00000 0.05 0.57 Q2 1 0.4462 0.3802 0.2662 11.00000 0.05 0.27 Q3 1 0.9621 0.3362 0.5810 11.00000 0.05 0.25 Q4 1 0.1053 0.2998 0.1935 11.00000 0.05 0.25 Q5 1 0.5733 0.0987 0.5945 11.00000 0.05 0.23 Q6 1 1.1218 0.3268 0.5540 11.00000 0.05 0.23 Q7 1 0.5801 0.4640 0.3214 11.00000 0.05 0.22 Q8 1 0.5390 0.3202 0.2753 11.00000 0.05 0.21 Q9 1 0.5003 0.3660 0.2187 11.00000 0.05 0.21 Q10 1 0.4795 0.4734 0.5724 11.00000 0.05 0.21 Q11 1 0.4421 0.4345 0.6031 11.00000 0.05 0.21 Q12 1 1.1031 0.4452 0.6575 11.00000 0.05 0.21 Q13 1 1.0247 0.3658 0.5424 11.00000 0.05 0.20 Q14 1 1.1221 0.3000 0.5766 11.00000 0.05 0.20 Q15 1 0.4831 0.3613 0.2533 11.00000 0.05 0.20 Q16 1 0.4657 0.4135 0.3417 11.00000 0.05 0.20 Q17 1 0.9098 0.3962 0.6148 11.00000 0.05 0.20 Q18 1 0.8365 0.3211 0.5343 11.00000 0.05 0.19 Q19 1 0.6227 0.3787 0.5320 11.00000 0.05 0.19 Q20 1 0.6071 0.3330 0.4531 11.00000 0.05 0.19 Q21 1 0.4851 0.3373 0.5329 11.00000 0.05 0.18 Q22 1 0.0743 0.3352 0.2250 11.00000 0.05 0.18 Q23 1 0.1445 0.2035 0.3090 11.00000 0.05 0.18 Q24 1 0.5913 0.3389 0.5684 11.00000 0.05 0.18 Q25 1 0.5396 0.3783 0.1550 11.00000 0.05 0.18 Q26 1 0.9711 0.4261 0.6256 11.00000 0.05 0.18 Q27 1 0.1247 0.2674 0.2548 11.00000 0.05 0.17 Q28 1 0.6965 0.1584 0.5586 11.00000 0.05 0.17 Q29 1 0.5818 0.4667 0.6023 11.00000 0.05 0.17 Q30 1 0.4589 0.4422 0.2948 11.00000 0.05 0.17 Q31 1 0.0194 0.2253 0.2993 11.00000 0.05 0.17 Q32 1 0.3115 0.3072 0.2403 11.00000 0.05 0.17 Q33 1 0.3040 0.3192 0.2246 11.00000 0.05 0.17 Q34 1 0.4255 0.3160 0.2197 11.00000 0.05 0.17 Q35 1 0.6370 0.4472 0.2645 11.00000 0.05 0.17 Q36 1 0.1966 0.3058 0.2450 11.00000 0.05 0.17 Q37 1 -0.0769 0.2419 0.2505 11.00000 0.05 0.16 Q38 1 0.3102 0.3028 0.1715 11.00000 0.05 0.16 Q39 1 0.7459 0.2381 0.4300 11.00000 0.05 0.16 Q40 1 0.4989 0.3743 0.4984 11.00000 0.05 0.16 Q41 1 0.1212 0.1110 0.5114 11.00000 0.05 0.16 Q42 1 0.5741 0.4253 0.6461 11.00000 0.05 0.16 Q43 1 0.2185 0.1223 0.5440 11.00000 0.05 0.16 Q44 1 0.5594 0.2737 0.3321 11.00000 0.05 0.15 Q45 1 0.1081 0.1962 0.4410 11.00000 0.05 0.15 Q46 1 0.3885 0.4072 0.2971 11.00000 0.05 0.15 Q47 1 0.5826 0.4185 0.2060 11.00000 0.05 0.15 Q48 1 0.7416 0.3452 0.4964 11.00000 0.05 0.15 Q49 1 0.7178 0.3380 0.4745 11.00000 0.05 0.15 Q50 1 0.5241 0.1579 0.5270 11.00000 0.05 0.15 Q51 1 1.1047 0.3581 0.7012 11.00000 0.05 0.15 Q52 1 0.2303 0.3946 0.3463 11.00000 0.05 0.14 Q53 1 1.1461 0.3833 0.6077 11.00000 0.05 0.14 Q54 1 0.3788 0.3844 0.4607 11.00000 0.05 0.14 Q55 1 0.6746 0.4810 0.1430 11.00000 0.05 0.14 Q56 1 -0.0447 0.1761 0.3321 11.00000 0.05 0.14 Q57 1 1.1782 0.4411 0.6066 11.00000 0.05 0.14 Q58 1 1.1964 0.3627 0.5747 11.00000 0.05 0.14 Q59 1 0.6786 0.2758 0.4751 11.00000 0.05 0.14 Q60 1 0.2017 0.2050 0.3903 11.00000 0.05 0.14 Q61 1 0.4610 0.0248 0.6942 11.00000 0.05 0.13 Q62 1 1.1150 0.3432 0.6812 11.00000 0.05 0.13 Q63 1 0.7265 0.3785 0.5535 11.00000 0.05 0.13 Q64 1 0.2538 0.2263 0.3664 11.00000 0.05 0.13 Q65 1 0.6775 0.4409 0.6726 11.00000 0.05 0.13 Q66 1 -0.0612 0.2064 0.2085 11.00000 0.05 0.13 Q67 1 0.6475 0.2319 0.3739 11.00000 0.05 0.13 Q68 1 0.3818 0.0638 0.5755 11.00000 0.05 0.13 Q69 1 0.3565 0.5591 0.5388 11.00000 0.05 0.13 Q70 1 1.2351 -0.0364 0.9552 11.00000 0.05 0.13 Q71 1 1.2121 0.1328 0.8877 11.00000 0.05 0.13 Q72 1 1.0329 0.0601 0.5025 11.00000 0.05 0.13 Q73 1 1.1705 0.3943 0.5546 11.00000 0.05 0.13 Q74 1 0.4147 0.0897 0.5298 11.00000 0.05 0.13 Q75 1 1.0233 0.0551 0.9561 11.00000 0.05 0.13 Q76 1 1.3356 0.1358 0.9610 11.00000 0.05 0.13 Q77 1 0.8191 -0.1451 0.9982 11.00000 0.05 0.13 Q78 1 0.8848 0.3882 0.7307 11.00000 0.05 0.13 Q79 1 0.3889 0.0697 0.5455 11.00000 0.05 0.13 Q80 1 1.2329 0.3983 0.6262 11.00000 0.05 0.13 Q81 1 1.1200 0.1694 0.8496 11.00000 0.05 0.13 Q82 1 1.0052 0.4371 0.4954 11.00000 0.05 0.13 Q83 1 0.6376 0.2796 0.8676 11.00000 0.05 0.13 Q84 1 1.1276 0.1163 0.4540 11.00000 0.05 0.12 Q85 1 1.1452 -0.0249 0.9542 11.00000 0.05 0.12 Q86 1 1.0724 -0.1264 1.0050 11.00000 0.05 0.12 Q87 1 0.8793 0.4204 0.5560 11.00000 0.05 0.12 Q88 1 1.4682 0.1140 0.9825 11.00000 0.05 0.12 Q89 1 1.1518 0.4754 0.5573 11.00000 0.05 0.12 Q90 1 0.6891 0.1137 0.6295 11.00000 0.05 0.12 Q91 1 1.1797 0.0413 0.6991 11.00000 0.05 0.12 Q92 1 1.0032 -0.1767 1.0824 11.00000 0.05 0.12 Q93 1 0.5577 0.1350 0.6558 11.00000 0.05 0.12 Q94 1 1.2214 0.5254 0.5594 11.00000 0.05 0.12 Q95 1 0.9030 0.5141 0.5723 11.00000 0.05 0.12 Q96 1 1.1557 0.0000 0.9496 11.00000 0.05 0.12 Q97 1 0.6939 0.2991 0.9795 11.00000 0.05 0.12 Q98 1 -0.0522 0.3370 0.3235 11.00000 0.05 0.12 Q99 1 0.7237 0.0889 0.9108 11.00000 0.05 0.12 Q100 1 1.1312 0.1409 0.9188 11.00000 0.05 0.12 Q101 1 0.2553 0.0617 0.5038 11.00000 0.05 0.12 Q102 1 1.1829 -0.1197 1.0506 11.00000 0.05 0.12 Q103 1 1.1581 0.4665 0.5314 11.00000 0.05 0.12 Q104 1 1.2477 0.2341 0.9811 11.00000 0.05 0.12 Q105 1 0.8894 -0.2274 1.0637 11.00000 0.05 0.12 Q106 1 0.6918 0.1100 0.8260 11.00000 0.05 0.12 Q107 1 1.3455 0.2278 0.9564 11.00000 0.05 0.12 Q108 1 1.2211 0.3420 0.5456 11.00000 0.05 0.12 Q109 1 0.7636 0.1258 0.7459 11.00000 0.05 0.12 Q110 1 1.2885 0.0768 0.5678 11.00000 0.05 0.11 Q111 1 1.3955 0.2431 0.8626 11.00000 0.05 0.11 Q112 1 0.7132 0.3000 0.8479 11.00000 0.05 0.11 Q113 1 1.2284 0.1031 0.9725 11.00000 0.05 0.11 Q114 1 1.1706 0.0870 0.5026 11.00000 0.05 0.11 Q115 1 0.4119 0.1516 0.5761 11.00000 0.05 0.11 Q116 1 0.8689 0.0158 0.9424 11.00000 0.05 0.11 Q117 1 0.8456 -0.0281 0.9722 11.00000 0.05 0.11 Q118 1 0.6974 0.0008 0.9612 11.00000 0.05 0.11 Q119 1 0.6786 0.0634 0.8615 11.00000 0.05 0.11 Q120 1 0.7079 0.2625 0.5277 11.00000 0.05 0.11 Q121 1 0.2800 0.2771 0.6427 11.00000 0.05 0.11 Q122 1 1.2317 0.0386 0.6530 11.00000 0.05 0.11 Q123 1 0.7963 0.1764 0.8067 11.00000 0.05 0.11 Q124 1 0.9624 0.1410 0.8866 11.00000 0.05 0.11 Q125 1 1.1591 0.5042 0.5166 11.00000 0.05 0.11 Q126 1 1.1636 0.0994 0.8286 11.00000 0.05 0.11 Q127 1 1.2262 -0.0387 1.0321 11.00000 0.05 0.11 Q128 1 0.3598 0.1189 0.6020 11.00000 0.05 0.11 Q129 1 1.1493 0.1644 0.8008 11.00000 0.05 0.11 Q130 1 0.7359 0.3594 0.8505 11.00000 0.05 0.11 Q131 1 0.8975 0.4484 0.5188 11.00000 0.05 0.11 Q132 1 0.4332 0.2449 0.8182 11.00000 0.05 0.11 Q133 1 1.2624 0.1957 0.9266 11.00000 0.05 0.11 Q134 1 0.3393 0.2726 0.7816 11.00000 0.05 0.11 Q135 1 0.6714 0.0674 1.0046 11.00000 0.05 0.10 Q136 1 0.4758 0.0966 0.5540 11.00000 0.05 0.10 Q137 1 1.2041 -0.1360 1.0021 11.00000 0.05 0.10 Q138 1 0.8016 0.3624 0.9548 11.00000 0.05 0.10 Q139 1 0.6219 0.1792 0.9437 11.00000 0.05 0.10 Q140 1 1.2644 0.2808 0.7999 11.00000 0.05 0.10 Q141 1 1.0348 0.2614 0.8873 11.00000 0.05 0.10 Q142 1 1.1083 0.0699 0.9183 11.00000 0.05 0.10 Q143 1 0.3783 0.1735 0.6101 11.00000 0.05 0.10 Q144 1 0.7619 0.3232 0.7963 11.00000 0.05 0.10 Q145 1 0.7720 0.1371 0.6122 11.00000 0.05 0.10 Q146 1 0.8626 -0.0969 0.9006 11.00000 0.05 0.10 Q147 1 1.1325 0.0527 0.5803 11.00000 0.05 0.10 Q148 1 0.7792 0.4158 0.6914 11.00000 0.05 0.10 Q149 1 0.4975 0.1935 0.6491 11.00000 0.05 0.10 Q150 1 1.0039 0.1396 0.4388 11.00000 0.05 0.10 ; _shelx_res_checksum 36786 _shelx_hkl_file ; 0 0 -1 0.10 0.10 0 0 -2 2329.50 57.69 0 0 -3 0.39 0.39 0 0 3 0.05 0.21 0 0 -4 1243.21 12.61 0 0 4 1197.57 7.30 0 0 -5 1.23 0.53 0 0 5 1.20 0.29 0 0 -6 66.43 1.94 0 0 6 60.08 1.10 0 0 -7 16.69 1.26 0 0 -8 605.84 6.35 0 0 8 647.95 3.80 0 0 -9 0.24 0.70 0 0 9 0.49 0.33 0 0 -10 18.99 1.69 0 0 10 20.11 0.86 0 0 -11 -0.15 0.78 0 0 -12 171.90 4.35 0 0 -13 3.62 1.18 0 0 -14 44.37 2.81 0 0 -14 56.51 3.23 0 0 -15 2.22 1.28 0 0 -15 1.38 1.39 0 0 -16 99.04 4.12 0 0 -16 116.43 4.87 0 0 -17 -0.02 1.48 0 0 -17 -0.24 1.35 0 0 -18 7.49 2.10 0 0 -19 0.13 1.43 0 0 -20 0.46 1.74 0 0 -21 -0.82 1.76 0 -1 0 -0.01 0.08 0 -1 1 543.53 4.78 0 1 -1 914.86 6.07 0 1 -1 704.29 5.71 0 1 1 773.06 5.75 0 -1 -2 69.69 1.24 0 -1 2 65.74 0.94 0 1 -2 97.66 1.46 0 1 2 105.58 1.13 0 -1 -3 0.13 0.40 0 -1 3 -0.10 0.27 0 1 -3 0.59 0.49 0 1 -3 0.14 0.46 0 1 3 0.22 0.26 0 -1 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203.51 2.49 2 -3 -7 232.57 4.43 2 3 -7 262.59 4.71 -2 -3 6 317.05 3.34 2 -3 -6 218.22 2.67 2 -3 -6 249.53 4.31 2 3 -6 292.43 4.71 2 -3 -5 0.76 0.39 2 -3 -5 0.76 0.58 2 3 -5 0.75 0.41 2 3 -5 0.56 0.73 2 -3 -4 142.21 2.31 2 -3 -4 156.39 3.04 2 3 -4 243.91 3.06 2 3 -4 181.48 3.36 2 -3 -3 803.19 7.78 2 -3 -3 865.21 6.55 2 3 -3 1350.92 12.71 2 3 -3 1050.95 11.20 2 -3 -2 261.22 3.27 2 3 -2 420.61 4.16 2 3 -2 342.36 4.03 2 -3 -1 388.08 4.07 2 3 -1 656.22 5.30 2 3 -1 542.27 4.75 -2 -3 0 1358.50 8.15 2 -3 0 831.55 7.67 2 3 0 1413.61 14.43 2 3 0 1195.70 12.18 -2 -3 -1 921.94 8.45 2 -3 1 550.65 5.11 -2 -3 -2 332.07 3.32 -2 3 -2 292.73 3.98 2 -3 2 192.57 3.17 2 3 2 313.18 3.98 -2 3 -3 10.50 1.12 2 -3 3 6.25 0.83 2 3 3 11.53 1.00 -2 3 -4 250.60 2.72 -2 3 -4 267.29 4.26 2 -3 4 173.19 3.19 2 3 4 283.94 3.98 -2 3 -5 2.78 0.60 -2 3 -5 2.78 0.88 2 -3 5 1.66 0.63 2 3 5 2.68 0.70 -2 3 -6 173.00 2.72 -2 3 -6 173.05 3.93 2 -3 6 115.46 2.77 2 3 6 196.75 3.51 -2 -3 -7 139.15 2.92 -2 3 -7 175.11 2.94 -2 3 -7 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32.75 3.32 2 4 -19 30.60 3.31 2 4 -19 39.05 3.51 2 -4 -18 3.82 1.80 2 4 -18 2.37 1.82 2 4 -18 2.65 1.68 2 -4 -17 1.00 1.45 2 4 -17 1.28 1.63 2 4 -17 1.78 1.52 2 -4 -16 67.19 3.82 2 4 -16 69.23 3.93 2 4 -16 79.14 4.01 2 -4 -15 -0.37 1.17 2 4 -15 -0.97 1.37 2 4 -15 0.95 1.25 2 -4 -14 108.95 4.34 2 4 -14 112.48 4.34 2 4 -14 134.46 4.59 2 -4 -13 0.89 1.01 2 4 -13 0.29 1.27 2 4 -13 0.08 0.99 2 -4 -12 1.21 0.96 2 4 -12 0.95 1.19 2 4 -12 0.76 0.97 2 -4 -11 60.90 2.92 2 4 -11 69.99 3.12 2 4 -11 83.73 3.20 -2 -4 10 2.74 0.57 2 -4 -10 2.82 1.02 2 4 -10 3.60 1.16 2 4 -10 4.68 1.08 -2 -4 9 62.38 1.69 2 -4 -9 52.33 1.47 2 -4 -9 62.44 2.70 2 4 -9 75.91 3.03 2 4 -9 91.61 2.87 -2 -4 8 165.08 2.71 2 -4 -8 139.34 2.38 2 -4 -8 152.98 3.89 2 4 -8 181.74 4.26 2 4 -8 215.89 3.96 -2 -4 7 57.95 1.71 2 -4 -7 44.91 1.48 2 -4 -7 49.10 2.31 2 4 -7 57.67 2.45 2 4 -7 69.18 2.21 -2 -4 6 222.70 3.21 2 -4 -6 172.03 2.73 2 -4 -6 181.49 3.87 2 4 -6 219.66 4.25 2 4 -6 257.43 3.58 -2 -4 5 81.36 2.02 2 -4 -5 56.23 1.69 2 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39.91 2.94 2 -5 -14 23.05 2.42 2 5 -14 28.56 2.73 2 5 -14 38.07 2.76 2 -5 -13 156.29 5.00 2 5 -13 162.70 5.06 2 5 -13 189.51 5.11 2 -5 -12 71.14 3.39 2 5 -12 82.00 3.61 2 5 -12 97.93 3.57 2 -5 -11 1.06 0.97 2 5 -11 0.02 1.06 2 5 -11 0.67 0.88 -2 -5 10 41.34 1.59 2 -5 -10 41.15 1.51 2 -5 -10 47.07 2.57 2 5 -10 50.96 2.76 2 5 -10 61.71 2.59 -2 -5 9 154.03 2.91 2 -5 -9 140.99 2.66 2 -5 -9 154.63 4.21 2 5 -9 173.42 4.43 2 5 -9 208.09 4.18 -2 -5 8 105.76 2.47 2 -5 -8 90.66 2.22 2 -5 -8 96.37 3.30 2 5 -8 111.73 3.46 2 5 -8 126.37 3.11 -2 -5 7 39.89 1.65 2 -5 -7 33.85 1.48 2 -5 -7 35.14 2.10 2 5 -7 39.23 2.17 2 5 -7 46.53 1.89 -2 -5 6 57.39 1.91 2 -5 -6 43.11 1.63 2 -5 -6 44.20 2.12 2 5 -6 58.29 2.53 2 5 -6 62.26 1.89 -2 -5 5 105.94 2.54 2 -5 -5 81.70 2.19 2 -5 -5 87.42 2.72 2 5 -5 100.07 3.00 2 5 -5 116.58 2.20 2 -5 -4 277.89 3.94 2 5 -4 351.44 5.09 2 5 -4 380.71 3.24 2 -5 -3 21.30 1.34 2 5 -3 33.59 1.60 2 5 -3 26.23 1.56 2 5 -3 28.77 0.86 2 -5 -2 3.06 0.70 2 5 -2 7.32 0.95 2 5 -2 4.41 0.91 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10 43.03 2.56 2 -11 -10 42.17 2.52 2 -11 -10 44.31 3.04 2 11 -10 52.78 3.34 -2 -11 9 -0.66 0.79 2 -11 -9 0.32 0.84 2 11 -9 -0.66 1.13 -2 -11 8 2.02 0.99 2 -11 -8 2.04 0.97 2 11 -8 1.93 1.22 -2 -11 7 -0.41 0.80 2 -11 -7 -0.57 0.76 2 11 -7 1.45 1.19 -2 -11 6 38.13 2.43 2 -11 -6 32.67 2.21 2 11 -6 40.19 2.75 -2 -11 5 5.14 1.21 2 -11 -5 2.24 1.07 2 11 -5 5.23 1.36 -2 -11 4 1.28 0.88 2 -11 -4 0.01 0.75 2 11 -4 0.89 0.95 -2 -11 3 71.46 3.18 2 -11 -3 53.88 2.74 -2 -11 2 85.92 3.44 2 -11 -2 67.70 3.05 -2 -11 1 7.54 1.39 2 -11 -1 5.90 1.35 -2 -11 0 6.15 1.34 2 -11 0 5.67 1.27 -2 -11 -1 6.00 1.31 2 -11 1 6.29 1.31 -2 -11 -2 34.05 2.38 2 -11 2 31.15 2.24 -2 -11 -3 5.56 1.28 2 -11 3 3.40 1.18 -2 -11 -4 95.59 3.66 2 -11 4 68.97 3.17 -2 -11 -5 2.39 1.03 2 -11 5 1.23 0.93 -2 -11 -6 136.76 4.43 2 -11 6 87.05 3.60 -2 -11 -7 42.42 2.69 2 -11 7 31.44 2.34 -2 -11 -8 3.94 1.21 2 -11 8 3.39 1.28 -2 -11 -9 45.65 2.81 -2 11 -9 43.69 2.98 2 -11 9 30.84 2.38 -2 -11 -10 19.91 2.10 -2 11 -10 17.29 2.05 -2 11 -10 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12.42 1.77 -2 -12 3 24.89 2.13 2 -12 -3 18.19 1.98 -2 -12 2 49.94 2.81 2 -12 -2 37.71 2.58 -2 -12 1 0.34 0.85 2 -12 -1 0.36 0.89 -2 -12 0 13.10 1.87 2 -12 0 10.78 1.70 -2 -12 -1 16.80 1.86 2 -12 1 19.64 1.96 -2 -12 -2 8.96 1.59 2 -12 2 10.24 1.67 -2 -12 -3 -0.32 0.80 2 -12 3 0.53 0.93 -2 -12 -4 60.95 3.14 2 -12 4 45.04 2.83 -2 -12 -5 75.50 3.49 2 -12 5 54.84 3.03 -2 -12 -6 10.81 1.82 2 -12 6 8.04 1.65 -2 -12 -7 168.14 5.15 2 -12 7 119.00 4.39 -2 -12 -8 116.12 4.37 2 -12 8 79.35 3.68 -2 -12 -9 1.65 1.13 2 -12 9 0.12 1.06 -2 -12 -10 0.71 1.01 -2 12 -10 -0.77 1.20 2 -12 10 -0.55 0.88 -2 -12 -11 0.25 0.99 -2 12 -11 -0.91 1.27 2 -12 11 0.39 1.10 -2 -12 -12 15.19 2.37 -2 12 -12 19.61 2.65 -2 -12 -13 6.63 1.87 -2 12 -13 9.49 2.18 -2 -12 -14 2.07 1.62 -2 12 -14 5.80 2.01 -2 12 -15 26.68 3.16 -2 12 -16 2.35 1.84 -2 12 -17 19.42 3.16 2 -13 -17 2.15 1.86 2 13 -17 1.08 1.79 2 -13 -16 2.35 1.77 2 13 -16 2.90 1.89 2 -13 -15 -0.04 1.34 2 13 -15 1.47 1.67 2 -13 -14 4.42 1.88 2 13 -14 4.09 1.84 2 -13 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1.46 -2 -13 -10 18.26 2.20 2 -13 10 12.01 2.08 -2 -13 -11 0.30 1.02 2 -13 11 0.38 1.15 -2 -13 -12 0.78 1.39 -2 13 -12 4.38 1.86 -2 -13 -13 6.77 1.94 -2 13 -13 8.65 2.21 -2 -13 -14 2.47 1.64 -2 13 -14 3.01 1.88 -2 13 -15 0.56 1.68 2 -14 -16 -0.83 1.39 2 14 -16 1.42 1.78 2 -14 -15 5.04 2.09 2 14 -15 6.13 2.13 2 -14 -14 13.12 2.60 2 14 -14 18.84 2.89 2 -14 -13 0.30 1.27 2 14 -13 1.22 1.58 2 -14 -12 3.06 1.69 2 14 -12 3.02 1.72 2 -14 -11 53.89 3.81 2 14 -11 66.97 4.00 -2 -14 10 8.09 1.76 2 -14 -10 8.84 1.77 2 14 -10 11.48 2.27 -2 -14 9 45.42 3.06 2 -14 -9 43.54 2.98 2 14 -9 55.75 3.58 -2 -14 8 21.29 2.22 2 -14 -8 16.56 2.25 2 14 -8 22.26 2.64 -2 -14 7 8.24 1.74 2 -14 -7 7.63 1.74 2 14 -7 7.20 1.91 -2 -14 6 60.84 3.45 2 -14 -6 54.80 3.26 -2 -14 5 0.58 1.05 2 -14 -5 -0.15 0.93 -2 -14 4 40.92 2.85 2 -14 -4 39.42 2.79 -2 -14 3 44.65 2.94 2 -14 -3 35.71 2.76 -2 -14 2 1.77 1.19 2 -14 -2 2.01 1.19 -2 -14 1 24.37 2.32 2 -14 -1 19.03 2.14 -2 -14 0 11.42 1.94 2 -14 0 7.43 1.64 -2 -14 -1 85.58 4.00 2 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6.94 1.56 -4 -10 -9 65.52 3.24 -4 10 -9 59.75 3.55 4 -10 9 36.97 2.68 4 10 9 68.45 3.46 -4 -10 -10 31.18 2.55 -4 10 -10 26.28 2.67 4 -10 10 17.76 2.18 4 10 10 30.13 2.59 -4 -10 -11 7.02 1.71 -4 10 -11 6.44 1.94 4 -10 11 2.39 1.33 4 10 11 5.39 1.56 -4 -10 -12 0.64 1.24 -4 10 -12 0.39 1.36 -4 -10 -13 13.28 2.34 -4 10 -13 12.97 2.53 -4 -10 -14 18.29 2.73 -4 10 -14 18.37 2.88 -4 -10 -15 1.37 1.64 -4 10 -15 1.09 1.79 -4 -10 -16 1.37 1.65 -4 10 -16 2.51 2.00 4 -11 -18 1.88 1.75 4 11 -18 2.64 2.03 4 -11 -17 4.77 2.06 4 11 -17 5.69 2.25 4 -11 -16 11.93 2.54 4 11 -16 18.96 3.01 4 -11 -15 12.48 2.46 4 11 -15 11.09 2.43 4 -11 -14 40.11 3.47 4 11 -14 44.88 3.54 4 -11 -13 1.56 1.51 4 11 -13 0.01 1.49 4 -11 -12 89.93 4.56 4 11 -12 103.09 4.85 4 -11 -11 7.43 1.80 4 11 -11 10.02 2.19 -4 -11 10 23.66 2.10 4 -11 -10 17.24 2.38 4 11 -10 23.66 2.72 -4 -11 9 59.71 3.06 4 -11 -9 40.31 2.51 4 -11 -9 45.83 3.17 4 11 -9 57.53 3.57 -4 -11 8 -0.36 0.87 4 -11 -8 0.52 0.92 4 -11 -8 -0.01 1.13 4 11 -8 0.27 1.16 -4 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7 -13 19.48 2.64 5 -7 -12 58.58 3.53 5 7 -12 66.69 3.73 5 -7 -11 22.70 2.30 5 7 -11 24.26 2.66 5 -7 -10 77.40 3.65 5 7 -10 84.40 3.88 5 -7 -9 30.82 1.93 5 -7 -9 40.33 2.75 5 7 -9 56.64 2.51 5 7 -9 43.25 2.97 5 -7 -8 7.76 1.26 5 -7 -8 8.00 1.59 5 7 -8 16.55 1.60 5 7 -8 9.89 1.74 5 -7 -7 18.43 1.62 5 -7 -7 22.57 1.99 5 7 -7 37.06 2.16 5 7 -7 29.01 2.31 5 -7 -6 75.18 2.88 5 -7 -6 93.24 3.51 5 7 -6 142.97 3.94 5 7 -6 107.11 3.82 5 -7 -5 -0.53 0.63 5 -7 -5 0.00 0.77 5 7 -5 0.04 0.76 5 7 -5 0.10 0.95 5 -7 -4 43.26 2.34 5 -7 -4 49.11 2.52 5 7 -4 72.64 2.96 5 7 -4 59.55 2.86 5 -7 -3 11.76 1.42 5 -7 -3 13.44 1.60 5 7 -3 21.09 1.77 5 7 -3 16.81 1.80 5 -7 -2 63.25 2.76 5 -7 -2 79.45 2.80 5 7 -2 111.52 3.62 5 7 -2 93.44 3.27 5 -7 -1 0.45 0.73 5 7 -1 0.95 0.80 5 7 -1 0.77 0.85 5 -7 0 115.74 3.75 5 7 0 201.74 4.90 5 7 0 164.78 4.08 5 -7 1 75.39 3.12 5 7 1 126.28 3.97 -5 -7 -2 6.87 0.89 5 -7 2 4.75 1.23 5 7 2 5.39 1.24 -5 -7 -3 13.55 1.26 5 -7 3 7.43 1.43 5 7 3 14.40 1.66 -5 -7 -4 33.85 1.84 5 -7 4 21.57 1.94 5 7 4 35.14 2.34 -5 -7 -5 8.37 1.25 5 -7 5 4.25 1.19 5 7 5 8.51 1.50 -5 -7 -6 0.28 0.85 -5 7 -6 1.22 1.19 5 -7 6 0.69 0.90 5 7 6 0.00 0.82 -5 -7 -7 0.10 0.88 -5 7 -7 0.54 1.09 5 -7 7 0.22 0.88 5 7 7 0.17 0.91 -5 -7 -8 33.60 2.43 -5 7 -8 27.64 2.65 5 -7 8 19.04 2.08 5 7 8 31.52 2.38 -5 -7 -9 22.42 2.17 -5 7 -9 17.98 2.46 5 -7 9 12.35 1.88 5 7 9 19.46 2.14 -5 -7 -10 6.57 1.64 -5 7 -10 5.72 1.71 5 -7 10 4.18 1.36 5 7 10 7.09 1.63 -5 -7 -11 113.52 4.56 -5 7 -11 103.65 4.72 5 -7 11 72.68 3.60 5 7 11 126.71 4.62 -5 -7 -12 20.11 2.59 -5 7 -12 18.88 2.70 5 -7 12 13.69 2.05 -5 -7 -13 36.56 3.25 -5 7 -13 37.01 3.27 -5 -7 -14 13.39 2.46 -5 7 -14 12.47 2.58 -5 -7 -15 -1.01 1.44 -5 7 -15 0.03 1.65 -5 -7 -16 6.86 2.24 -5 7 -16 7.38 2.37 -5 -7 -17 5.45 2.24 -5 7 -17 3.88 2.13 5 -8 -19 2.17 1.90 5 8 -19 2.16 2.09 5 -8 -18 4.27 2.00 5 8 -18 2.74 1.99 5 -8 -17 30.53 3.32 5 8 -17 35.86 3.61 5 -8 -16 1.42 1.65 5 8 -16 3.84 1.93 5 -8 -15 0.40 1.43 5 8 -15 1.59 1.75 5 -8 -14 65.54 4.02 5 8 -14 67.95 4.15 5 -8 -13 -0.06 1.12 5 8 -13 1.82 1.62 5 -8 -12 96.17 4.38 5 8 -12 101.35 4.54 5 -8 -11 39.39 2.98 5 8 -11 45.40 3.17 5 -8 -10 0.12 1.12 5 8 -10 -0.43 1.26 -5 -8 9 23.27 1.92 5 -8 -9 13.50 1.52 5 -8 -9 17.27 2.02 5 8 -9 20.41 2.26 5 -8 -8 53.82 2.55 5 -8 -8 69.29 3.41 5 8 -8 100.94 3.46 5 8 -8 80.68 3.77 5 -8 -7 15.16 1.58 5 -8 -7 21.90 2.05 5 8 -7 31.35 2.13 5 8 -7 24.43 2.36 5 -8 -6 8.69 1.38 5 -8 -6 11.81 1.74 5 8 -6 19.01 1.84 5 8 -6 12.59 1.90 5 -8 -5 0.38 0.73 5 -8 -5 0.09 0.87 5 8 -5 0.48 0.80 5 8 -5 1.45 1.12 5 -8 -4 104.82 3.58 5 -8 -4 131.37 3.96 5 8 -4 195.07 4.82 5 8 -4 153.90 4.48 5 -8 -3 3.04 1.01 5 -8 -3 5.70 1.24 5 8 -3 5.23 1.20 5 8 -3 6.11 1.40 5 -8 -2 162.87 4.47 5 8 -2 291.77 5.98 5 8 -2 237.16 5.26 5 -8 -1 13.93 1.60 5 8 -1 27.67 2.17 5 8 -1 27.68 2.08 5 -8 0 40.73 2.43 5 8 0 72.80 3.18 5 -8 1 50.84 2.72 5 8 1 85.57 3.45 5 -8 2 166.84 4.75 5 8 2 300.42 6.33 5 -8 3 56.74 2.92 5 8 3 103.47 3.88 5 -8 4 2.30 1.06 5 8 4 3.50 1.16 -5 -8 -5 34.96 2.04 5 -8 5 23.27 2.16 5 8 5 35.56 2.54 -5 -8 -6 42.38 2.32 5 -8 6 21.75 2.06 5 8 6 44.98 2.76 -5 -8 -7 9.29 1.52 -5 8 -7 8.13 1.81 5 -8 7 4.43 1.31 5 8 7 11.46 1.84 -5 -8 -8 16.53 1.98 -5 8 -8 16.52 2.32 5 -8 8 10.51 1.84 5 8 8 20.37 2.20 -5 -8 -9 6.88 1.60 -5 8 -9 8.65 1.87 5 -8 9 4.98 1.43 5 8 9 8.03 1.67 -5 -8 -10 -0.20 1.17 -5 8 -10 0.17 1.38 5 -8 10 -0.42 1.03 5 8 10 -0.86 0.99 -5 -8 -11 1.40 1.31 -5 8 -11 -0.19 1.39 5 -8 11 1.13 1.20 5 8 11 0.93 1.23 -5 -8 -12 13.52 2.29 -5 8 -12 11.43 2.34 5 -8 12 8.35 1.77 -5 -8 -13 1.40 1.54 -5 8 -13 2.79 1.79 -5 -8 -14 0.57 1.56 -5 8 -14 4.68 1.99 -5 -8 -15 9.33 2.31 -5 8 -15 7.89 2.39 -5 -8 -16 4.29 2.05 -5 8 -16 3.47 2.11 -5 -8 -17 11.09 2.67 -5 8 -17 9.93 2.66 5 -9 -19 7.03 2.43 5 9 -19 5.58 2.36 5 -9 -18 2.43 1.94 5 9 -18 6.13 2.29 5 -9 -17 2.37 1.82 5 9 -17 3.68 2.02 5 -9 -16 2.19 1.66 5 9 -16 3.05 1.91 5 -9 -15 3.43 1.67 5 9 -15 3.91 1.91 5 -9 -14 16.03 2.57 5 9 -14 25.05 2.98 5 -9 -13 0.37 1.31 5 9 -13 0.29 1.39 5 -9 -12 0.58 1.32 5 9 -12 0.72 1.46 5 -9 -11 1.86 1.27 5 9 -11 1.24 1.52 5 -9 -10 8.81 1.87 5 9 -10 9.33 1.90 -5 -9 9 10.95 1.60 5 -9 -9 6.81 1.36 5 -9 -9 6.36 1.58 5 9 -9 9.10 1.86 -5 -9 8 125.46 4.01 5 -9 -8 80.89 3.20 5 -9 -8 100.92 4.13 5 9 -8 113.61 4.49 5 -9 -7 5.29 1.24 5 -9 -7 8.46 1.65 5 9 -7 12.03 1.71 5 9 -7 10.48 1.86 5 -9 -6 10.65 1.58 5 -9 -6 13.18 1.86 5 9 -6 22.67 1.95 5 9 -6 19.07 2.25 5 -9 -5 5.31 1.20 5 -9 -5 7.78 1.49 5 9 -5 10.89 1.62 5 9 -5 9.67 1.73 5 -9 -4 65.67 2.98 5 -9 -4 94.00 3.55 5 9 -4 132.00 4.23 5 9 -4 105.31 3.95 5 -9 -3 79.67 3.29 5 9 -3 154.53 4.53 5 9 -3 132.18 4.28 5 -9 -2 33.63 2.28 5 9 -2 67.01 3.12 5 9 -2 52.20 2.84 5 -9 -1 9.15 1.51 5 9 -1 21.58 1.99 5 9 -1 19.48 1.97 5 -9 0 10.78 1.63 5 9 0 22.47 2.11 5 -9 1 1.24 0.92 5 9 1 1.36 1.01 5 -9 2 21.53 2.01 5 9 2 39.12 2.56 5 -9 3 72.95 3.37 5 9 3 125.26 4.34 5 -9 4 1.80 1.04 5 9 4 2.23 1.08 5 -9 5 0.33 0.92 5 9 5 1.65 1.07 5 -9 6 -0.26 0.88 5 9 6 -1.06 0.82 5 -9 7 73.79 3.58 5 9 7 142.99 4.88 -5 9 -8 -0.55 1.30 5 -9 8 -0.62 0.90 5 9 8 0.37 1.12 -5 -9 -9 40.86 2.77 -5 9 -9 36.82 3.14 5 -9 9 23.72 2.40 5 9 9 46.07 3.06 -5 -9 -10 30.60 2.65 -5 9 -10 25.34 2.84 5 -9 10 22.60 2.40 5 9 10 36.34 2.84 -5 -9 -11 2.43 1.49 -5 9 -11 5.73 1.90 5 -9 11 2.90 1.38 5 9 11 5.38 1.62 -5 -9 -12 -0.33 1.35 -5 9 -12 0.19 1.53 5 -9 12 1.51 1.28 -5 -9 -13 11.60 2.24 -5 9 -13 10.79 2.48 -5 -9 -14 1.63 1.65 -5 9 -14 1.07 1.60 -5 -9 -15 5.93 2.07 -5 9 -15 3.94 2.09 -5 -9 -16 18.37 3.03 -5 9 -16 14.98 3.03 5 -10 -18 -0.52 1.69 5 10 -18 3.44 2.09 5 -10 -17 9.28 2.52 5 10 -17 8.12 2.40 5 -10 -16 27.32 3.25 5 10 -16 28.87 3.19 5 -10 -15 2.27 1.53 5 10 -15 3.29 1.89 5 -10 -14 8.67 2.16 5 10 -14 12.63 2.49 5 -10 -13 13.03 2.41 5 10 -13 15.64 2.56 5 -10 -12 -0.64 1.07 5 10 -12 1.16 1.52 5 -10 -11 0.60 1.27 5 10 -11 -0.81 1.21 5 -10 -10 10.48 1.99 5 10 -10 9.75 2.11 -5 -10 9 2.89 1.11 5 -10 -9 0.91 0.94 5 -10 -9 2.16 1.31 5 10 -9 2.15 1.51 -5 -10 8 85.33 3.54 5 -10 -8 57.44 2.88 5 -10 -8 69.97 3.55 5 10 -8 75.38 3.78 -5 -10 7 3.00 1.19 5 -10 -7 2.53 1.01 5 -10 -7 2.07 1.23 5 10 -7 1.20 1.36 5 -10 -6 0.25 0.88 5 -10 -6 0.77 1.06 5 10 -6 1.46 1.08 5 10 -6 0.98 1.12 5 -10 -5 19.77 1.97 5 -10 -5 28.35 2.36 5 10 -5 39.84 2.56 5 10 -5 30.29 2.59 5 -10 -4 35.59 2.39 5 10 -4 69.92 3.33 5 10 -4 54.75 3.13 5 -10 -3 180.15 5.04 5 10 -3 337.91 6.88 5 10 -3 273.49 6.26 5 -10 -2 137.09 4.46 5 10 -2 265.92 6.20 5 10 -2 221.15 5.59 5 -10 -1 86.85 3.64 5 10 -1 168.31 4.99 5 -10 0 0.61 0.89 5 10 0 -0.14 0.83 5 -10 1 0.25 0.86 5 10 1 0.32 0.86 5 -10 2 61.19 3.24 5 10 2 107.90 4.15 5 -10 3 -0.21 0.96 5 10 3 1.37 1.05 5 -10 4 134.27 4.74 5 10 4 228.86 6.04 5 -10 5 1.78 1.13 5 10 5 3.79 1.32 5 -10 6 0.48 1.06 5 10 6 -0.24 0.96 5 -10 7 18.02 2.37 5 10 7 26.76 2.42 5 -10 8 20.60 2.36 5 10 8 35.84 2.77 5 -10 9 45.90 3.08 5 10 9 86.92 4.05 -5 10 -10 4.22 1.79 5 -10 10 2.17 1.35 5 10 10 5.54 1.66 -5 10 -11 10.86 2.34 5 -10 11 6.26 1.72 5 10 11 13.34 2.21 -5 10 -12 23.35 2.84 5 -10 12 15.27 2.37 -5 10 -13 2.97 1.76 -5 10 -14 30.87 3.33 -5 10 -15 1.06 1.92 -5 10 -16 -0.01 1.89 5 -11 -18 0.34 1.82 5 11 -18 0.86 1.88 5 -11 -17 0.15 1.64 5 11 -17 1.97 1.91 5 -11 -16 1.75 1.74 5 11 -16 1.34 1.86 5 -11 -15 2.72 1.79 5 11 -15 3.48 1.97 5 -11 -14 39.83 3.52 5 11 -14 44.06 3.75 5 -11 -13 0.00 1.24 5 11 -13 0.57 1.45 5 -11 -12 16.94 2.58 5 11 -12 19.04 2.76 5 -11 -11 9.01 1.96 5 11 -11 9.06 2.06 5 -11 -10 1.66 1.36 5 11 -10 0.30 1.46 -5 -11 9 54.66 3.03 5 -11 -9 38.05 2.54 5 -11 -9 40.97 3.00 5 11 -9 48.12 3.43 -5 -11 8 59.45 3.09 5 -11 -8 36.85 2.53 5 -11 -8 40.98 3.01 5 11 -8 54.20 3.50 -5 -11 7 0.90 1.00 5 -11 -7 -0.32 0.88 5 -11 -7 0.09 1.08 5 11 -7 -0.29 1.25 -5 -11 6 0.04 0.93 5 -11 -6 0.36 0.93 5 -11 -6 0.80 1.11 5 11 -6 0.89 1.19 5 -11 -5 34.45 2.52 5 -11 -5 44.30 2.88 5 11 -5 53.13 3.27 5 -11 -4 1.79 1.08 5 11 -4 6.75 1.56 5 11 -4 5.26 1.51 5 -11 -3 5.84 1.43 5 11 -3 10.99 1.81 5 11 -3 8.18 1.77 5 -11 -2 -0.34 0.88 5 11 -2 0.87 1.10 5 -11 -1 0.12 0.88 5 11 -1 -0.73 0.87 5 -11 0 2.05 1.20 5 11 0 6.27 1.58 5 -11 1 5.35 1.42 5 11 1 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1.29 -6 8 -10 14.13 2.51 6 -8 10 9.52 1.95 6 8 10 15.57 2.30 -6 8 -11 34.40 3.30 6 -8 11 25.06 2.48 6 8 11 46.88 3.27 -6 -8 -12 5.53 1.83 -6 8 -12 6.56 2.11 6 -8 12 3.31 1.57 6 8 12 7.62 1.86 -6 -8 -13 0.17 1.47 -6 8 -13 1.51 1.75 -6 -8 -14 3.85 1.87 -6 8 -14 1.47 1.80 -6 -8 -15 -0.12 1.59 -6 8 -15 -0.15 1.79 -6 -8 -16 1.35 1.93 6 -9 -18 -0.10 1.59 6 9 -18 2.87 2.08 6 -9 -17 7.65 2.37 6 9 -17 10.17 2.59 6 -9 -16 2.62 1.91 6 9 -16 5.68 2.11 6 -9 -15 0.69 1.55 6 9 -15 1.65 1.83 6 -9 -14 15.48 2.58 6 9 -14 16.16 2.73 6 -9 -13 16.49 2.56 6 9 -13 17.26 2.72 6 -9 -12 32.98 3.03 6 9 -12 42.32 3.44 6 -9 -11 1.74 1.43 6 9 -11 5.21 1.88 6 -9 -10 3.26 1.46 6 9 -10 4.65 1.74 6 -9 -9 4.54 1.24 6 -9 -9 5.65 1.59 6 9 -9 9.29 1.60 6 9 -9 6.46 1.81 6 -9 -8 0.46 0.89 6 -9 -8 0.54 1.01 6 9 -8 0.09 0.94 6 9 -8 1.89 1.43 6 -9 -7 30.92 2.29 6 -9 -7 38.41 2.67 6 9 -7 57.04 3.02 6 9 -7 44.71 3.12 6 -9 -6 91.14 3.59 6 -9 -6 120.40 4.26 6 9 -6 165.77 4.88 6 9 -6 136.01 4.72 6 -9 -5 34.70 2.44 6 -9 -5 39.39 2.63 6 9 -5 65.32 3.19 6 9 -5 59.46 3.32 6 -9 -4 6.69 1.39 6 -9 -4 9.20 1.58 6 9 -4 13.00 1.85 6 -9 -3 36.11 2.55 6 -9 -3 46.09 2.63 6 9 -3 67.79 3.34 6 9 -3 57.69 3.11 6 -9 -2 62.14 3.16 6 -9 -2 76.63 3.13 6 9 -2 112.82 4.22 6 9 -2 102.21 3.88 6 -9 -1 56.30 3.12 6 -9 -1 75.55 3.07 6 9 -1 106.07 4.09 6 9 -1 103.11 3.84 6 -9 0 11.32 1.77 6 9 0 21.72 2.15 6 -9 1 38.80 2.65 6 9 1 74.50 3.53 6 -9 2 17.92 1.99 6 9 2 33.47 2.56 6 -9 3 0.66 1.01 6 9 3 1.69 1.12 6 -9 4 15.43 2.12 6 9 4 27.36 2.44 6 -9 5 5.37 1.49 6 9 5 8.11 1.67 6 -9 6 0.69 1.06 6 9 6 0.48 1.09 6 -9 7 3.97 1.52 6 9 7 8.41 1.83 6 -9 8 0.17 1.12 6 9 8 0.64 1.21 6 -9 9 1.85 1.33 6 9 9 6.22 1.69 -6 9 -10 6.13 2.01 6 -9 10 3.56 1.56 6 9 10 5.55 1.73 -6 9 -11 55.02 4.01 6 -9 11 31.82 2.80 6 9 11 63.76 3.79 -6 9 -12 5.05 2.06 6 -9 12 2.46 1.47 -6 9 -13 52.64 4.14 -6 9 -14 5.62 2.25 -6 9 -15 -0.58 1.77 6 -10 -18 0.19 1.84 6 10 -18 1.97 1.92 6 -10 -17 1.21 1.84 6 10 -17 1.33 1.81 6 -10 -16 7.94 2.31 6 10 -16 11.08 2.63 6 -10 -15 0.47 1.44 6 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5.12 1.58 6 -10 5 0.52 1.11 6 10 5 -0.24 1.09 6 -10 6 12.66 2.14 6 10 6 24.12 2.54 6 -10 7 0.58 1.13 6 10 7 2.23 1.36 6 -10 8 2.70 1.34 6 10 8 2.29 1.38 6 -10 9 1.23 1.30 6 10 9 6.03 1.69 6 -10 10 16.14 2.42 6 10 10 27.53 2.78 -6 10 -11 2.65 1.81 6 -10 11 1.54 1.48 6 10 11 4.09 1.71 -6 10 -12 8.08 2.35 6 -10 12 8.08 1.93 -6 10 -13 8.66 2.39 -6 10 -14 10.32 2.68 6 -11 -17 1.48 1.96 6 11 -17 4.36 2.19 6 -11 -16 0.33 1.67 6 11 -16 1.58 1.90 6 -11 -15 38.06 3.68 6 11 -15 39.19 3.78 6 -11 -14 8.71 2.27 6 11 -14 8.56 2.37 6 -11 -13 1.61 1.61 6 11 -13 2.62 1.81 6 -11 -12 26.44 2.92 6 11 -12 32.45 3.12 6 -11 -11 15.78 2.52 6 11 -11 13.89 2.50 6 -11 -10 3.58 1.61 6 11 -10 4.14 1.70 -6 -11 9 21.79 2.25 6 -11 -9 12.84 1.90 6 -11 -9 16.45 2.44 6 11 -9 16.73 2.50 -6 -11 8 110.60 4.31 6 -11 -8 63.86 3.31 6 -11 -8 83.48 4.13 6 11 -8 93.69 4.52 6 -11 -7 -0.17 0.86 6 -11 -7 -0.19 1.12 6 11 -7 1.72 1.16 6 11 -7 2.86 1.54 6 -11 -6 24.11 2.31 6 -11 -6 35.43 2.77 6 11 -6 52.67 3.20 6 11 -6 37.65 2.92 6 -11 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1.21 1.54 6 12 -12 2.19 1.77 6 -12 -11 1.82 1.53 6 12 -11 0.38 1.54 6 -12 -10 2.59 1.56 6 12 -10 3.44 1.77 -6 -12 9 -0.31 1.02 6 -12 -9 -0.07 1.02 6 -12 -9 0.18 1.27 6 12 -9 1.68 1.55 -6 -12 8 1.00 1.14 6 -12 -8 0.63 1.07 6 -12 -8 0.21 1.23 6 12 -8 -0.51 1.22 -6 -12 7 7.30 1.72 6 -12 -7 5.98 1.57 6 -12 -7 7.39 1.73 6 12 -7 7.97 1.92 6 -12 -6 27.31 2.50 6 -12 -6 33.42 2.81 6 12 -6 45.10 3.34 6 -12 -5 75.16 3.80 6 -12 -5 92.15 4.15 6 12 -5 148.23 5.23 6 12 -5 116.35 4.85 6 -12 -4 19.58 2.19 6 -12 -4 23.34 2.42 6 12 -4 53.53 3.31 6 -12 -3 43.75 3.08 6 12 -3 90.98 4.19 6 12 -3 76.75 3.96 6 -12 -2 0.07 1.14 6 12 -2 2.50 1.37 6 -12 -1 71.18 3.75 6 12 -1 133.03 5.03 6 -12 0 32.28 2.80 6 12 0 64.93 3.67 6 -12 1 70.99 3.81 6 12 1 133.45 5.10 6 -12 2 4.06 1.54 6 12 2 5.19 1.61 6 -12 3 2.39 1.34 6 12 3 5.03 1.60 6 -12 4 -0.36 1.12 6 12 4 -0.40 1.15 6 -12 5 74.26 4.11 6 12 5 137.19 5.39 6 -12 6 0.26 1.24 6 12 6 0.81 1.31 6 -12 7 8.18 1.92 6 12 7 12.65 2.25 6 -12 8 -0.32 1.27 6 12 8 0.32 1.31 6 -12 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12.15 2.17 6 -14 -4 10.54 2.06 6 -14 -3 0.52 1.10 6 -14 -2 10.74 2.05 6 -14 -1 5.44 1.71 6 14 -1 10.05 2.08 6 -14 0 0.34 1.18 6 14 0 -0.63 1.20 6 -14 1 1.29 1.27 6 14 1 -0.23 1.14 6 -14 2 2.43 1.40 6 14 2 4.78 1.66 6 -14 3 15.06 2.42 6 14 3 29.55 2.90 6 -14 4 2.67 1.46 6 14 4 3.40 1.59 6 -14 5 0.15 1.30 6 14 5 0.51 1.31 6 -14 6 0.29 1.38 6 14 6 3.52 1.64 6 -14 7 3.37 1.60 6 14 7 5.38 1.89 6 -14 8 -1.76 1.17 6 14 8 1.39 1.49 6 -14 9 0.48 1.38 6 14 9 -0.10 1.35 6 -14 10 2.44 1.61 6 14 10 1.80 1.63 6 -14 11 5.72 1.99 6 14 11 11.60 2.53 6 -15 -13 0.46 1.69 6 15 -13 2.78 2.02 6 -15 -12 3.99 2.00 6 15 -12 4.23 2.10 6 -15 -11 4.75 2.02 6 15 -11 7.38 2.22 6 -15 -10 5.52 2.03 6 15 -10 5.62 2.11 -6 -15 9 10.27 2.12 6 -15 -9 9.30 2.23 6 15 -9 8.51 2.30 -6 -15 8 3.63 1.61 6 -15 -8 2.94 1.47 6 -15 -8 3.64 1.69 6 15 -8 3.85 1.91 -6 -15 7 12.34 2.25 6 -15 -7 4.24 1.57 6 -15 -7 8.59 2.09 6 15 -7 10.57 2.39 -6 -15 6 2.90 1.44 6 -15 -6 2.55 1.47 6 -15 -6 1.50 1.52 6 15 -6 3.25 1.82 -6 -15 5 21.89 2.70 6 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3.47 1.89 8 -5 11 3.91 1.60 8 5 11 3.92 1.58 -8 -5 -12 1.66 1.66 -8 5 -12 1.08 1.81 8 -5 12 1.49 1.46 8 5 12 1.38 1.51 -8 -5 -13 -0.76 1.51 -8 5 -13 -0.36 1.70 -8 -5 -14 -1.05 1.69 -8 5 -14 -0.92 1.76 8 -6 -18 5.49 2.39 8 6 -18 5.26 2.41 8 -6 -17 23.13 3.42 8 6 -17 23.03 3.49 8 -6 -16 34.66 3.59 8 6 -16 32.33 3.65 8 -6 -15 0.27 1.56 8 6 -15 0.43 1.65 8 -6 -14 0.37 1.54 8 6 -14 -0.96 1.67 8 -6 -13 32.25 3.18 8 6 -13 34.76 3.42 8 -6 -12 2.63 1.66 8 6 -12 2.59 1.83 8 -6 -11 84.28 4.32 8 6 -11 88.00 4.56 8 -6 -10 21.46 2.54 8 6 -10 22.65 2.83 8 -6 -9 12.34 2.11 8 6 -9 11.35 1.81 8 6 -9 10.54 2.09 8 -6 -8 8.73 1.62 8 -6 -8 11.31 1.97 8 6 -8 18.40 2.04 8 6 -8 13.45 2.25 8 -6 -7 0.44 0.95 8 -6 -7 0.34 1.11 8 6 -7 0.33 1.00 8 6 -7 -0.43 1.27 8 -6 -6 26.70 2.30 8 -6 -6 35.68 2.65 8 6 -6 45.48 2.84 8 6 -6 40.51 2.91 8 -6 -5 9.88 1.76 8 -6 -5 13.41 1.86 8 6 -5 20.78 2.16 8 6 -5 17.88 2.20 8 -6 -4 1.22 1.05 8 -6 -4 0.84 1.05 8 6 -4 1.42 1.22 8 -6 -3 41.04 2.81 8 -6 -3 56.08 2.73 8 6 -3 64.60 3.33 8 6 -3 63.15 3.18 8 -6 -2 3.38 1.26 8 -6 -1 33.38 2.58 8 6 -1 55.34 3.19 8 6 -1 48.45 2.65 8 6 0 4.19 1.34 8 -6 1 20.24 2.18 8 6 1 29.24 2.51 8 -6 2 10.25 1.82 8 6 2 9.89 1.83 8 -6 3 14.94 2.22 8 6 3 24.29 2.42 8 -6 4 7.14 1.75 8 6 4 12.67 2.09 8 -6 5 11.64 2.01 8 6 5 15.68 2.29 8 -6 6 13.83 2.21 8 6 6 20.52 2.49 8 -6 7 6.80 1.79 8 6 7 7.03 1.78 8 -6 8 0.28 1.18 8 6 8 0.73 1.23 -8 6 -9 28.15 3.00 8 -6 9 17.57 2.54 8 6 9 30.43 2.86 -8 6 -10 0.91 1.48 8 -6 10 -0.29 1.24 8 6 10 0.15 1.22 -8 6 -11 3.37 1.98 8 -6 11 2.38 1.54 8 6 11 4.43 1.73 -8 6 -12 0.05 1.71 8 -6 12 0.63 1.41 8 6 12 0.01 1.35 -8 6 -13 -0.81 1.72 8 -7 -18 18.14 3.29 8 7 -18 15.60 3.08 8 -7 -17 17.19 3.11 8 7 -17 18.57 3.29 8 -7 -16 1.13 1.79 8 7 -16 0.90 1.82 8 -7 -15 16.32 2.76 8 7 -15 18.73 3.11 8 -7 -14 3.66 1.86 8 7 -14 1.32 1.79 8 -7 -13 7.53 2.13 8 7 -13 11.09 2.48 8 -7 -12 4.10 1.75 8 7 -12 5.66 2.03 8 -7 -11 2.17 1.50 8 7 -11 2.27 1.75 8 -7 -10 46.41 3.31 8 7 -10 52.29 3.67 8 -7 -9 31.74 2.81 8 7 -9 42.30 2.79 8 7 -9 31.26 3.03 8 -7 -8 1.52 1.07 8 -7 -8 0.36 1.25 8 7 -8 1.61 1.10 8 7 -8 1.00 1.38 8 -7 -7 33.24 2.52 8 -7 -7 46.72 2.99 8 7 -7 61.17 3.26 8 7 -7 46.60 3.24 8 -7 -6 18.69 2.11 8 -7 -6 22.85 2.26 8 7 -6 40.26 2.70 8 7 -6 30.56 2.72 8 -7 -5 50.73 2.98 8 -7 -5 73.29 3.43 8 7 -5 89.73 3.87 8 7 -5 82.63 3.80 8 -7 -4 11.20 1.90 8 -7 -4 12.15 1.82 8 7 -4 23.97 2.27 8 7 -4 23.86 2.39 8 -7 -3 72.97 3.59 8 7 -3 131.14 4.76 8 7 -3 115.76 4.15 8 7 -2 23.77 2.33 8 7 -2 28.01 2.35 8 -7 -1 44.25 2.96 8 7 -1 67.51 3.55 8 7 -1 60.35 3.05 8 7 0 2.59 1.32 8 -7 1 6.81 1.63 8 7 1 10.01 1.88 8 -7 2 1.57 1.17 8 7 2 0.86 1.11 8 -7 3 13.11 2.10 8 7 3 20.43 2.32 8 -7 4 0.92 1.15 8 7 4 2.03 1.30 8 -7 5 0.77 1.19 8 7 5 1.02 1.33 8 -7 6 14.98 2.39 8 7 6 17.79 2.47 8 -7 7 5.13 1.74 8 7 7 7.14 1.82 8 -7 8 15.94 2.51 8 7 8 22.87 2.69 8 -7 9 0.57 1.23 8 7 9 3.10 1.56 -8 7 -10 1.79 1.69 8 -7 10 2.44 1.53 8 7 10 3.43 1.60 -8 7 -11 1.50 1.75 8 -7 11 0.24 1.32 8 7 11 2.56 1.52 -8 7 -12 1.23 1.79 8 -7 12 1.29 1.43 8 7 12 1.67 1.61 -8 7 -13 7.30 2.50 8 -8 -17 4.74 2.20 8 8 -17 4.20 2.17 8 -8 -16 3.47 2.01 8 8 -16 4.97 2.23 8 -8 -15 0.15 1.66 8 8 -15 3.18 2.06 8 -8 -14 10.89 2.45 8 8 -14 11.73 2.63 8 -8 -13 -0.51 1.31 8 8 -13 0.18 1.51 8 -8 -12 4.66 1.84 8 8 -12 5.11 2.02 8 -8 -11 9.84 2.17 8 8 -11 13.41 2.50 8 -8 -10 6.33 1.85 8 8 -10 8.02 2.01 8 -8 -9 2.82 1.55 8 8 -9 2.32 1.27 8 8 -9 2.24 1.68 8 -8 -8 4.33 1.41 8 -8 -8 4.21 1.55 8 8 -8 6.68 1.64 8 8 -8 8.31 2.02 8 -8 -7 17.32 2.09 8 -8 -7 22.43 2.36 8 8 -7 28.21 2.40 8 8 -7 23.64 2.66 8 -8 -6 7.15 1.64 8 -8 -6 8.35 1.77 8 8 -6 10.67 1.86 8 8 -6 8.79 1.91 8 -8 -5 1.79 1.12 8 -8 -5 1.00 1.20 8 8 -5 3.70 1.38 8 8 -5 3.38 1.54 8 -8 -4 17.57 2.33 8 -8 -4 18.56 2.02 8 8 -4 30.41 2.55 8 8 -4 21.55 2.38 8 -8 -3 12.09 2.07 8 8 -3 22.04 2.40 8 8 -3 15.85 2.21 8 -8 -2 22.90 2.35 8 8 -2 40.64 2.92 8 8 -2 37.05 2.67 8 8 -1 -0.48 1.00 8 8 -1 1.98 1.25 8 -8 0 50.59 3.23 8 8 0 83.58 4.05 8 8 1 12.29 2.09 8 -8 2 4.58 1.53 8 8 2 3.15 1.43 8 -8 3 12.30 2.17 8 8 3 19.47 2.32 8 -8 4 1.43 1.29 8 8 4 1.38 1.25 8 -8 5 23.02 2.50 8 8 5 35.73 2.98 8 -8 6 0.62 1.31 8 8 6 0.55 1.27 8 -8 7 7.10 1.92 8 8 7 12.44 2.34 8 -8 8 -0.15 1.24 8 8 8 1.51 1.42 8 -8 9 0.11 1.20 8 8 9 0.43 1.29 8 -8 10 0.96 1.46 8 8 10 0.94 1.32 8 -8 11 5.86 1.86 8 8 11 8.12 2.07 -8 8 -12 3.39 2.08 8 -8 12 3.94 1.75 8 8 12 8.67 2.20 -8 8 -13 0.36 1.90 8 -9 -17 4.11 2.22 8 9 -17 1.22 1.89 8 -9 -16 1.70 1.95 8 9 -16 3.75 2.18 8 -9 -15 7.25 2.26 8 9 -15 4.38 2.04 8 -9 -14 -0.11 1.55 8 9 -14 -0.17 1.55 8 -9 -13 1.38 1.65 8 9 -13 2.66 1.87 8 -9 -12 0.33 1.48 8 9 -12 0.82 1.70 8 -9 -11 27.46 2.82 8 9 -11 29.59 3.17 8 -9 -10 38.83 3.22 8 9 -10 47.62 3.66 8 -9 -9 0.66 1.33 8 9 -9 1.86 1.28 8 9 -9 0.81 1.51 8 -9 -8 0.96 1.14 8 -9 -8 0.04 1.24 8 9 -8 0.68 1.14 8 9 -8 1.69 1.53 8 -9 -7 3.56 1.36 8 -9 -7 3.36 1.52 8 9 -7 6.97 1.72 8 9 -7 4.36 1.72 8 -9 -6 -0.40 0.93 8 -9 -6 0.17 1.12 8 9 -6 -0.23 1.09 8 9 -6 0.62 1.36 8 -9 -5 20.83 2.34 8 -9 -5 29.81 2.59 8 9 -5 36.72 2.79 8 9 -5 30.75 2.78 8 -9 -4 17.89 2.39 8 -9 -4 20.97 2.27 8 9 -4 37.06 2.84 8 9 -4 34.64 2.84 8 -9 -3 67.04 3.71 8 9 -3 111.22 4.60 8 9 -3 103.41 4.31 8 -9 -2 1.75 1.28 8 -9 -1 25.12 2.50 8 9 -1 35.25 2.85 8 9 -1 34.43 2.67 8 -9 0 47.51 3.23 8 9 0 62.05 3.73 8 9 1 17.28 2.44 8 9 2 4.07 1.61 8 -9 3 14.85 2.31 8 9 3 23.97 2.55 8 -9 4 3.47 1.51 8 9 4 5.53 1.71 8 -9 5 3.36 1.63 8 9 5 7.07 1.84 8 -9 6 2.52 1.47 8 9 6 4.23 1.62 8 -9 7 -0.13 1.17 8 9 7 1.79 1.49 8 -9 8 2.00 1.48 8 9 8 6.49 1.90 8 -9 9 1.07 1.44 8 9 9 0.34 1.27 8 -9 10 1.09 1.38 8 9 10 0.34 1.47 8 -9 11 1.46 1.57 8 9 11 0.20 1.51 8 -9 12 0.94 1.58 8 9 12 -0.17 1.55 8 -10 -16 32.44 3.69 8 10 -16 32.52 3.79 8 -10 -15 -0.16 1.69 8 10 -15 2.25 1.92 8 -10 -14 6.39 2.25 8 10 -14 9.99 2.53 8 -10 -13 4.51 1.97 8 10 -13 4.62 2.15 8 -10 -12 18.89 2.90 8 10 -12 16.90 2.90 8 -10 -11 3.02 1.75 8 10 -11 3.89 1.91 8 -10 -10 15.58 2.52 8 10 -10 25.50 3.02 8 -10 -9 1.90 1.46 8 10 -9 4.17 1.51 8 10 -9 4.08 1.84 8 -10 -8 11.88 2.03 8 -10 -8 13.56 2.27 8 10 -8 18.95 2.22 8 10 -8 15.18 2.46 8 -10 -7 0.11 1.10 8 -10 -7 0.82 1.30 8 10 -7 2.13 1.36 8 10 -7 3.42 1.68 8 -10 -6 39.45 2.98 8 -10 -6 52.11 3.35 8 10 -6 77.52 3.99 8 10 -6 58.54 3.69 8 -10 -5 11.65 2.00 8 -10 -5 13.49 2.08 8 10 -5 30.20 2.67 8 10 -5 16.52 2.43 8 -10 -4 0.87 1.13 8 -10 -4 0.94 1.21 8 10 -4 3.26 1.43 8 10 -4 2.48 1.51 8 -10 -3 4.96 1.58 8 10 -3 10.39 2.07 8 10 -3 10.68 2.07 8 -10 -2 112.18 4.79 8 10 -2 203.40 6.31 8 10 -2 168.38 5.42 8 10 -1 6.50 1.77 8 -10 0 55.52 3.61 8 10 0 94.48 4.50 8 10 1 3.02 1.58 8 -10 2 0.05 1.08 8 10 2 -0.15 1.15 8 -10 3 19.27 2.38 8 10 3 35.60 3.03 8 -10 4 14.46 2.36 8 10 4 27.87 2.81 8 -10 5 8.48 1.99 8 10 5 14.34 2.37 8 -10 6 7.31 1.98 8 10 6 17.73 2.73 8 -10 7 1.05 1.37 8 10 7 1.93 1.56 8 -10 8 14.62 2.54 8 10 8 23.58 2.88 8 -10 9 0.88 1.33 8 10 9 0.63 1.51 8 -10 10 1.38 1.52 8 10 10 0.29 1.39 8 -10 11 1.35 1.63 8 10 11 0.02 1.45 8 -10 12 6.56 2.22 8 -11 -15 10.06 2.60 8 11 -15 10.16 2.72 8 -11 -14 0.63 1.68 8 11 -14 -0.27 1.77 8 -11 -13 20.56 3.07 8 11 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1.78 8 12 4 9.28 2.21 8 -12 5 7.92 2.12 8 12 5 14.44 2.60 8 -12 6 10.02 2.28 8 12 6 22.84 2.79 8 -12 7 4.83 1.89 8 12 7 10.13 2.37 8 -12 8 0.61 1.44 8 12 8 1.30 1.54 8 -12 9 -0.66 1.29 8 12 9 0.43 1.52 8 -12 10 1.91 1.74 8 12 10 2.31 1.79 8 -13 -13 -0.84 1.41 8 13 -13 0.89 1.77 8 -13 -12 0.19 1.64 8 13 -12 -0.23 1.53 8 -13 -11 8.64 2.31 8 13 -11 8.49 2.46 8 -13 -10 32.36 3.31 8 13 -10 35.72 3.46 -8 -13 9 14.50 2.46 8 -13 -9 11.64 2.42 8 13 -9 14.36 2.65 8 -13 -8 2.15 1.44 8 -13 -8 4.53 1.80 8 13 -8 4.45 2.02 8 -13 -7 7.30 1.92 8 -13 -7 10.31 2.17 8 13 -7 16.49 2.67 8 13 -7 12.65 2.52 8 -13 -6 0.69 1.33 8 -13 -6 1.11 1.45 8 13 -6 1.38 1.40 8 13 -6 1.81 1.67 8 -13 -5 11.76 2.27 8 -13 -5 14.39 2.33 8 13 -5 22.24 2.94 8 13 -5 19.12 2.80 8 -13 -4 0.38 1.32 8 13 -4 2.28 1.45 8 13 -4 5.41 1.90 8 -13 -3 -0.29 1.15 8 13 -3 2.11 1.48 8 -13 -2 9.30 2.04 8 13 -2 15.35 2.53 8 -13 -1 2.21 1.34 8 13 -1 -0.30 1.23 8 -13 0 3.17 1.58 8 13 0 7.67 2.00 8 -13 1 0.94 1.42 8 13 1 1.29 1.57 8 -13 2 10.11 2.19 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3.27 10 -3 -14 3.82 2.15 10 3 -14 4.17 2.26 10 -3 -13 25.48 3.37 10 3 -13 22.85 3.25 10 -3 -12 -0.01 1.70 10 3 -12 -0.17 1.73 10 -3 -11 11.26 2.40 10 3 -11 13.04 2.61 10 -3 -10 10.06 2.25 10 3 -10 9.95 2.34 10 -3 -9 0.10 1.45 10 3 -9 1.04 1.63 10 -3 -8 0.06 1.07 10 -3 -8 -0.81 1.35 10 3 -8 0.64 1.15 10 3 -8 0.89 1.56 10 -3 -7 32.30 2.68 10 -3 -7 40.90 3.13 10 3 -7 40.42 2.85 10 3 -7 40.32 3.10 10 -3 -6 3.70 1.42 10 3 -6 4.34 1.55 10 3 -6 3.62 1.57 10 -3 -5 15.70 2.29 10 3 -5 20.06 2.28 10 -3 -4 -0.21 1.04 10 3 -4 0.18 1.08 10 -3 -3 9.99 1.92 10 3 -3 15.60 2.30 10 -3 -2 5.32 1.59 10 3 -2 4.45 1.58 10 -3 -1 1.40 1.36 10 3 -1 1.61 1.35 10 -3 0 37.23 3.03 10 3 0 49.36 3.46 10 -3 1 15.51 2.42 10 3 1 21.92 2.49 10 -3 2 10.59 2.05 10 3 2 10.37 2.07 10 -3 3 -0.35 1.10 10 3 3 0.21 1.27 10 -3 4 22.39 2.70 10 3 4 29.52 2.86 10 -3 5 8.37 1.99 10 3 5 8.94 2.08 10 -3 6 0.29 1.28 10 3 6 0.47 1.33 10 -3 7 3.67 1.69 10 3 7 4.55 1.73 10 -3 8 16.72 2.75 10 3 8 16.46 2.74 10 -3 9 9.30 2.21 10 3 9 9.87 2.36 10 -3 10 34.53 3.50 10 3 10 45.56 3.88 -10 3 -11 3.08 2.13 10 -3 11 1.90 1.74 10 3 11 4.27 1.95 10 -4 -16 10.61 2.86 10 4 -16 12.00 2.95 10 -4 -15 6.12 2.40 10 4 -15 8.18 2.67 10 -4 -14 4.18 2.14 10 4 -14 5.53 2.25 10 -4 -13 0.98 1.78 10 4 -13 2.03 1.97 10 -4 -12 2.26 1.80 10 4 -12 1.05 1.85 10 -4 -11 -0.45 1.50 10 4 -11 0.18 1.76 10 -4 -10 4.22 1.80 10 4 -10 4.86 2.00 10 -4 -9 -0.35 1.33 10 4 -9 -0.18 1.49 10 -4 -8 25.37 2.46 10 -4 -8 31.60 2.98 10 4 -8 34.74 2.77 10 4 -8 32.37 3.01 10 -4 -7 -0.39 1.09 10 4 -7 0.78 1.12 10 4 -7 -0.27 1.42 10 -4 -6 35.91 2.88 10 4 -6 46.40 3.19 10 4 -6 48.74 3.20 10 -4 -5 26.22 2.61 10 4 -5 41.88 3.02 10 -4 -4 9.06 1.89 10 4 -4 15.94 2.29 10 -4 -3 36.36 3.02 10 4 -3 43.25 3.14 10 -4 -2 27.92 2.69 10 4 -2 37.17 3.07 10 -4 -1 95.00 4.49 10 4 -1 116.87 4.99 10 -4 0 34.82 3.05 10 4 0 37.89 3.07 10 -4 1 6.12 1.72 10 4 1 6.70 1.83 10 -4 2 2.69 1.44 10 4 2 2.41 1.42 10 -4 3 0.16 1.17 10 4 3 0.65 1.28 10 -4 4 9.67 2.07 10 4 4 10.18 2.13 10 -4 5 7.13 1.97 10 4 5 10.34 2.19 10 -4 6 14.20 2.46 10 4 6 19.87 2.85 10 -4 7 -0.05 1.34 10 4 7 0.99 1.45 10 -4 8 3.33 1.68 10 4 8 3.53 1.75 10 -4 9 19.45 2.97 10 4 9 23.57 2.90 10 -4 10 0.39 1.54 10 4 10 0.54 1.52 10 -4 11 7.50 2.24 10 4 11 6.29 2.17 10 -5 -16 8.64 2.67 10 5 -16 9.60 2.79 10 -5 -15 11.43 2.62 10 5 -15 9.83 2.75 10 -5 -14 2.05 1.89 10 5 -14 2.56 2.13 10 -5 -13 2.03 1.76 10 5 -13 0.39 1.82 10 -5 -12 -0.61 1.48 10 5 -12 0.58 1.86 10 -5 -11 112.36 5.15 10 5 -11 119.87 5.48 10 -5 -10 3.12 1.71 10 5 -10 3.62 1.94 10 -5 -9 29.30 3.07 10 5 -9 33.11 3.17 10 -5 -8 0.67 1.18 10 -5 -8 -0.87 1.35 10 5 -8 1.10 1.21 10 5 -8 1.39 1.55 10 -5 -7 1.60 1.34 10 5 -7 3.51 1.41 10 5 -7 4.47 1.76 10 -5 -6 17.61 2.17 10 5 -6 29.10 2.71 10 5 -6 28.99 2.84 10 -5 -5 6.84 1.81 10 5 -5 11.94 2.09 10 -5 -4 -0.19 1.09 10 5 -4 0.90 1.32 10 -5 -3 17.67 2.46 10 5 -3 20.95 2.53 10 -5 -2 29.21 2.77 10 5 -2 40.00 3.09 10 -5 -1 17.06 2.49 10 5 -1 23.27 2.57 10 -5 0 45.02 3.42 10 5 0 67.68 3.95 10 -5 1 2.13 1.38 10 5 1 3.25 1.60 10 -5 2 1.64 1.33 10 5 2 1.01 1.33 10 -5 3 6.71 1.93 10 5 3 6.82 1.92 10 -5 4 4.08 1.62 10 5 4 3.85 1.63 10 -5 5 -0.71 1.14 10 5 5 0.58 1.27 10 -5 6 0.44 1.33 10 5 6 0.16 1.41 10 -5 7 2.14 1.51 10 5 7 4.74 1.83 10 -5 8 7.57 2.11 10 5 8 12.07 2.49 10 -5 9 28.82 3.14 10 5 9 41.97 3.64 10 -5 10 13.54 2.64 10 5 10 18.39 2.96 10 -5 11 13.36 2.74 10 5 11 21.68 3.23 10 -6 -16 3.23 2.01 10 6 -16 3.43 2.37 10 -6 -15 -1.43 1.66 10 6 -15 -0.28 2.02 10 -6 -14 9.50 2.58 10 6 -14 10.95 2.70 10 -6 -13 -0.14 1.63 10 6 -13 0.89 1.88 10 -6 -12 -0.37 1.60 10 6 -12 -0.22 1.72 10 -6 -11 -0.67 1.50 10 6 -11 1.55 1.77 10 -6 -10 1.34 1.61 10 6 -10 2.76 1.75 10 -6 -9 -0.51 1.46 10 6 -9 1.37 1.65 10 -6 -8 -0.06 1.14 10 -6 -8 -0.26 1.36 10 6 -8 -0.25 1.17 10 6 -8 0.72 1.52 10 -6 -7 1.99 1.38 10 6 -7 5.35 1.64 10 6 -7 3.88 1.71 10 -6 -6 25.90 2.64 10 6 -6 38.30 3.04 10 6 -6 32.91 2.90 10 -6 -5 23.37 2.62 10 6 -5 31.68 2.86 10 -6 -4 31.51 2.90 10 6 -4 51.98 3.42 10 -6 -3 6.25 1.81 10 6 -3 6.94 1.81 10 -6 -2 1.56 1.34 10 6 -2 3.26 1.57 10 -6 -1 5.05 1.78 10 6 -1 7.97 1.90 10 -6 0 0.55 1.25 10 6 0 1.22 1.30 10 -6 1 89.85 4.57 10 6 1 117.53 5.17 10 -6 2 25.67 2.74 10 6 2 40.68 3.37 10 -6 3 1.12 1.33 10 6 3 2.08 1.56 10 -6 4 0.37 1.22 10 6 4 0.36 1.26 10 -6 5 10.94 2.23 10 6 5 16.50 2.70 10 -6 6 5.11 1.78 10 6 6 9.18 2.20 10 -6 7 4.40 1.78 10 6 7 7.49 2.19 10 -6 8 0.00 1.43 10 6 8 -0.44 1.30 10 -6 9 2.48 1.70 10 6 9 5.96 2.10 10 -6 10 0.13 1.54 10 6 10 1.06 1.69 10 -7 -15 -0.39 1.84 10 7 -15 0.14 1.97 10 -7 -14 18.19 3.14 10 7 -14 18.63 3.20 10 -7 -13 10.74 2.52 10 7 -13 10.56 2.63 10 -7 -12 0.20 1.68 10 7 -12 2.40 1.91 10 -7 -11 7.61 2.17 10 7 -11 7.42 2.28 10 -7 -10 0.04 1.56 10 7 -10 0.56 1.66 10 -7 -9 -0.21 1.48 10 7 -9 0.84 1.64 10 -7 -8 0.86 1.16 10 -7 -8 -0.25 1.31 10 7 -8 -0.06 1.11 10 7 -8 1.86 1.58 10 -7 -7 1.36 1.30 10 7 -7 4.38 1.63 10 7 -7 2.94 1.69 10 -7 -6 2.26 1.48 10 7 -6 6.28 1.72 10 7 -6 4.28 1.74 10 -7 -5 2.03 1.45 10 7 -5 3.68 1.56 10 7 -5 3.39 1.68 10 -7 -4 1.68 1.38 10 7 -4 1.26 1.41 10 -7 -3 83.04 4.32 10 7 -3 131.91 5.39 10 7 -2 1.34 1.32 10 -7 -1 17.90 2.60 10 7 -1 23.09 2.73 10 -7 0 2.58 1.44 10 7 0 1.21 1.43 10 -7 1 20.44 2.81 10 7 1 33.68 3.06 10 -7 2 3.70 1.61 10 7 2 3.21 1.65 10 -7 3 3.30 1.64 10 7 3 1.61 1.51 10 -7 4 22.95 2.75 10 7 4 34.81 3.29 10 -7 5 2.18 1.53 10 7 5 2.13 1.57 10 -7 6 12.46 2.47 10 7 6 22.44 2.80 10 -7 7 10.60 2.42 10 7 7 17.08 2.82 10 -7 8 6.47 2.05 10 7 8 8.11 2.22 10 -7 9 -0.03 1.49 10 7 9 0.45 1.48 10 -7 10 9.49 2.45 10 7 10 16.03 2.92 10 -8 -15 0.20 1.97 10 8 -15 1.86 2.09 10 -8 -14 9.10 2.59 10 8 -14 11.43 2.81 10 -8 -13 14.02 2.83 10 8 -13 19.96 3.23 10 -8 -12 0.12 1.62 10 8 -12 1.51 1.88 10 -8 -11 20.64 2.99 10 8 -11 22.97 3.21 10 -8 -10 -0.10 1.44 10 8 -10 0.73 1.67 10 -8 -9 0.39 1.45 10 8 -9 2.88 1.79 10 -8 -8 5.01 1.71 10 8 -8 8.46 1.94 10 8 -8 7.75 2.17 10 -8 -7 2.52 1.51 10 8 -7 4.23 1.68 10 8 -7 3.54 1.73 10 -8 -6 5.07 1.72 10 8 -6 7.47 1.88 10 8 -6 6.58 2.01 10 -8 -5 10.00 2.18 10 8 -5 17.03 2.52 10 8 -5 14.91 2.39 10 -8 -4 16.52 2.53 10 8 -4 26.66 2.88 10 -8 -3 2.46 1.52 10 8 -3 3.22 1.65 10 -8 -2 19.43 2.74 10 8 -2 31.87 3.00 10 -8 -1 13.65 2.40 10 8 -1 23.57 2.83 10 8 0 1.23 1.43 10 -8 1 0.64 1.32 10 8 1 -1.52 0.96 10 -8 2 3.38 1.59 10 8 2 6.93 1.92 10 -8 3 2.96 1.58 10 8 3 4.73 1.76 10 -8 4 0.18 1.39 10 8 4 1.73 1.49 10 -8 5 11.65 2.44 10 8 5 16.44 2.72 10 -8 6 0.39 1.46 10 8 6 -0.60 1.41 10 -8 7 4.54 1.87 10 8 7 5.77 2.06 10 -8 8 0.45 1.56 10 8 8 0.20 1.59 10 -8 9 1.88 1.77 10 8 9 4.02 1.94 10 -9 -14 16.54 3.13 10 9 -14 21.36 3.40 10 -9 -13 -0.79 1.71 10 9 -13 1.18 1.96 10 -9 -12 3.02 1.99 10 9 -12 6.04 2.29 10 -9 -11 2.17 1.79 10 9 -11 2.92 1.94 10 -9 -10 11.81 2.47 10 9 -10 16.36 2.85 10 -9 -9 4.92 1.83 10 9 -9 6.24 2.12 10 -9 -8 2.97 1.46 10 9 -8 7.26 1.89 10 9 -8 7.04 2.12 10 -9 -7 0.78 1.36 10 9 -7 0.24 1.32 10 9 -7 2.02 1.66 10 -9 -6 3.29 1.60 10 9 -6 6.29 1.86 10 9 -6 5.93 1.91 10 -9 -5 6.26 1.83 10 9 -5 7.78 1.97 10 9 -5 5.77 1.92 10 -9 -4 8.40 2.04 10 9 -4 19.05 2.79 10 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9.90 2.42 10 -11 4 8.74 2.27 10 11 4 16.10 2.90 10 -11 5 12.70 2.61 10 11 5 20.47 3.18 10 -11 6 6.85 2.24 10 11 6 12.93 2.70 10 11 7 -0.13 1.55 10 -12 -11 1.32 1.81 10 12 -11 0.11 1.91 10 -12 -10 9.87 2.49 10 12 -10 10.02 2.60 10 12 -9 1.23 1.80 10 12 -8 0.76 1.45 10 12 -8 1.10 1.73 10 -12 -7 70.24 4.43 10 12 -7 129.78 5.83 10 12 -7 101.87 5.29 10 -12 -6 15.81 2.77 10 12 -6 28.78 3.24 10 12 -6 20.06 3.01 10 -12 -5 0.36 1.42 10 12 -5 1.74 1.72 10 12 -5 1.74 1.80 10 -12 -4 5.95 2.01 10 12 -4 13.25 2.60 10 -12 -3 26.95 3.07 10 12 -3 54.72 4.03 10 12 -2 6.48 2.04 10 -12 -1 1.19 1.52 10 12 -1 3.15 1.71 10 -12 0 -0.28 1.33 10 12 0 0.17 1.48 10 -12 1 8.42 2.23 10 12 1 14.99 2.80 10 -12 2 13.48 2.74 10 12 2 18.18 2.97 10 -12 3 2.96 1.76 10 12 3 4.94 1.96 10 -12 4 0.46 1.49 10 12 4 2.76 1.84 10 -12 5 8.93 2.36 10 12 5 12.79 2.67 10 13 -9 1.88 1.92 10 13 -8 14.34 2.72 10 13 -8 11.58 2.72 10 -13 -7 0.46 1.56 10 13 -7 0.38 1.60 10 13 -7 0.15 1.71 10 -13 -6 23.46 3.29 10 13 -6 35.13 3.58 10 13 -6 29.13 3.37 10 -13 -5 31.27 3.27 10 13 -5 54.70 4.23 10 13 -5 44.94 3.87 10 -13 -4 0.39 1.48 10 13 -4 -1.30 1.33 10 -13 -3 1.50 1.58 10 13 -3 0.80 1.57 10 -13 -2 0.72 1.60 10 13 -2 -0.17 1.53 10 -13 -1 26.86 3.14 10 13 -1 46.66 3.91 10 13 0 26.48 3.55 10 13 1 14.24 2.73 10 -13 2 0.93 1.47 10 13 2 -0.11 1.46 10 -13 3 5.72 2.21 10 13 3 11.28 2.57 10 -14 -7 3.28 1.97 10 14 -7 8.48 2.30 10 14 -7 6.88 2.40 10 -14 -6 0.71 1.67 10 14 -6 0.70 1.59 10 14 -6 0.83 1.97 10 -14 -5 -0.83 1.48 10 14 -5 -0.55 1.55 10 -14 -4 1.68 1.81 10 14 -4 1.52 1.70 10 -14 -3 2.04 1.80 10 14 -3 3.84 1.97 10 -14 -2 1.07 1.64 10 14 -2 3.95 1.95 10 -14 -1 2.21 1.73 10 14 -1 3.72 1.93 10 -14 0 0.60 1.57 10 14 0 -0.71 1.63 11 0 -15 3.41 2.55 11 0 -14 0.19 2.13 11 0 -13 0.75 2.21 11 0 -12 -1.21 1.87 11 0 -11 6.23 2.31 11 0 -10 -0.81 1.66 11 0 -9 -1.14 1.59 11 0 -8 0.05 1.17 11 0 -7 0.66 1.27 11 0 -6 -0.12 1.08 11 0 -5 0.52 1.18 11 0 -4 -1.47 1.06 11 0 -3 18.27 2.57 11 0 -2 0.73 1.34 11 0 -1 5.75 1.76 11 0 0 0.00 1.19 11 0 1 15.97 2.51 11 0 2 0.10 1.22 11 0 3 11.75 2.28 11 0 4 0.01 1.21 11 0 5 0.61 1.38 11 0 6 0.30 1.40 11 0 7 -0.56 1.31 11 0 8 1.27 1.55 11 0 9 19.70 3.09 11 -1 -15 48.42 4.53 11 1 -15 48.88 4.54 11 -1 -14 9.05 2.78 11 1 -14 11.65 2.97 11 -1 -13 61.79 4.54 11 1 -13 66.82 4.71 11 -1 -12 37.81 3.77 11 1 -12 31.26 3.59 11 -1 -11 -0.50 1.91 11 1 -11 0.68 1.91 11 -1 -10 -1.34 1.79 11 1 -10 -0.10 1.74 11 1 -9 5.76 2.08 11 -1 -8 21.67 2.46 11 1 -8 22.54 2.49 11 -1 -7 2.45 1.37 11 1 -7 2.58 1.45 11 -1 -6 8.48 1.92 11 1 -6 10.36 2.06 11 -1 -5 -0.03 1.12 11 1 -5 0.06 1.14 11 -1 -4 32.49 2.98 11 1 -4 36.16 3.10 11 -1 -3 0.23 1.27 11 1 -3 0.54 1.24 11 -1 -2 -0.26 1.23 11 1 -2 -0.75 1.11 11 -1 -1 2.89 1.49 11 1 -1 2.79 1.56 11 -1 0 18.09 2.64 11 1 0 18.85 2.69 11 -1 1 8.12 2.06 11 1 1 8.03 1.96 11 -1 2 0.80 1.31 11 1 2 -0.40 1.24 11 -1 3 0.18 1.21 11 1 3 0.58 1.28 11 -1 4 4.62 1.76 11 1 4 4.06 1.72 11 -1 5 4.31 1.81 11 1 5 3.47 1.72 11 -1 6 0.82 1.49 11 1 6 0.95 1.53 11 -1 7 -0.25 1.44 11 1 7 0.26 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